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Mineral Hills Environmental Site Assessments (two)
fi ~I ~L...~ !j f-- TABLE OF CONTENTS righe&Bond SECTION 1 INTRODUCTION SECTION 2 GENERAL SITE DESCRIPTION 2.1 Existing Conditions 2-1 2.1.1 Property Description and Site Use 2-1 2.1.2 Surrounding Property Description 2-1 2.2 Area Mapping 2-2 2.2.1 Topography and Drainage 2-2 2.2.2 Site Hydrology 2-2 2.2.3 Surficial and Bedrock Geology 2-2 2.2.4 Surrounding Resource Areas 2-3 2.3 Site Reconnaissance 2-3 2:3.1 North Parcel (Lot 2) ..................................................2-3 2.3.2 South Parcel (Lot 4) .2-4 2.4 Site History .2-4 SECTION 3 ENVIRONMENTAL REVIEW I~PI 3.1 Database Search ............3-1 3.2 DEP File Review ................................................................3-2 3.3 Fire Department Records ...................................................3-3 SECTION 4 LIMITED SOIL INVESTIGATION 4.1 Soil Sample Collection .......................................................4-1. 4.2 Soil and Groundwater Classification ..................................4-1 4.3 Soil Analytical Results .......................................................4-2 4 1~ SECTION 5 CONCLUSION !-j SECTION 6 LIMITATIONS SECTION 7 REFERENCES I APPENDIX A FIGURES FIGURE 1 SITE Locus. FIGURE 2 MASsGIS MAP FIGURE 3 FLOOD ZONE MAP l l SITE PLAN ~ ~j 1TJ ~ - I J _ Irighe&B®nd TABLE OF CONTENTS APPENDIX B ASSESSOR'S INFORMATION PROPERTY CARDS ASSESSOR'S MAPS APPENDIX C SITE PHOTOGRAPHS I' APPENDIX D ENVIRONMENTAL FiRSTSEARCHTm REPORT APPENDIX E LABORATORY ANALYSIS TABLE OF RESULTS ANALYTICAL LABORATORY REPORT SECTION 1 INTRODUCTION ' Teghe&B®nd Tighe & Bond has completed a Phase I Environmental Site Assessment for Quarry Alternatives, Inc., for the former quarry at Turkey Hill located at the western end of Turkey Hill Road in the Village of Florence, City of Northampton, Hampshire County, Massachusetts (the site). The investigation was performed in general compliance with the American Society for Testing Materials (ASTM), Standard E 1527-00 for Phase I Environmental Site Assessments and Massachusetts General Laws (MGL) Chapter 21E to evaluate and determine whether there is the potential for a release or threat of release of oil or hazardous materials (OHM) to have occurred at the site. The tasks performed to evaluate the site for evidence of a.release of OHM included: • A reconnaissance inspection of the site; • An environmental database search, site history research and review of local, state and Federal records pertaining to the use, storage and release of OHM in the site vicinity; • A review of geological publications and maps for the site area; • Collection of three (3) soil samples; • Screening of soil samples; and • Laboratory analysis of soil samples. The investigation revealed the presence of OHM above its applicable Reportable Concentration in site soils. Therefore, a "release", as defined by the MCP, has occurred at the site. Information is presented in the following sections of this report with respect to these findings and other environmental conditions noted at the site. Phase I Environmental Site Assessment 1-1 SECTION 2 GENERAL SITE DESCRIPTION V:1 2.1 EXISTING CONDITIONS Existing conditions at the site and in the surrounding area were evaluated through a site reconnaissance visit and a review of City records. In addition, site conditions were evaluated through a review of other records and published mapping of the area surrounding the site. The conditions at the time of this investigation are described in the following sections. 2.1.1 Property Description and Site Use The subject site is located at the western end of Turkey Hill Road in the West Farms section of the Village of Florence in the City of Northampton, Hampshire County, Massachusetts. According to the Northampton Assessor's records, the site is currently owned by Jedoron Realty, Inc. of Farmington, Connecticut, and occupies approximately 165.4 acres of undeveloped land. The site consists of two (2) parcels of land identified as Lots 2 and 4 on Map 34. The northern portion of Lot 2 is shown on Map 27. Copies of the property cards and maps 27 and 34 are provided in Appendix B. The site was formerly operated as a gravel pit and quarry. 2.1.2 Surrounding Property Description The subject site is located in a zoning area designated as Rural Residential (RR). Ten (10) other parcels of land abut the subject site. This property information for the. surrounding properties is summarized in the table below. Map Lot Property Owner Land Use Size (acres) 27 2 Joseph A. Wilhelm, III, Trustee of the Mineral Hill Land Trust Vacant 30 S. Pen and J.M. Bessette Residential 56.11 kibiski Realt Partnershi Vacant 25 A. Bond Rh Residential 1.837 A. Bond Vacant 3.009 E J III and Edward A. Parsons Vacant 148 ls, Inc. Vacant 6 . McClaflin Residential 40.33 Civitarese and Gre C. Wolff Residential 5 32 ssociates, Inc. Vacant 72.13 The abutting properties a re also located within an area zoned as "Rural Residential". Of the four (4) residentially developed properties directly abutting the subject site, the earliest construction began in 1971. Phase I Environmental Site Assessment 2-1 SECTION 2 GENERAL SITE DESCRIPTION 2.2 AREA MAPPING Mapping reviewed as part of this investigation included United States Geological Survey (USGS) topographic, surficial geology and bedrock geology maps, United States Department of Housing and Urban Development Flood Insurance Rate mapping and Massachusetts Geographic Information System (MassGIS) mapping. 2.2.1 Topography and Drainage The site location is illustrated on the USGS Topographic Map for the Easthampton, Massachusetts Quadrangle (Figure 1 in Appendix A). Figure 1 shows that the site is situated approximately 480 feet above mean sea level and that the topography of the site is variable due to the quarrying operation. The topographic map shows two gravel pits within the approximate boundaries of the subject site. According to the FEMA Flood Insurance Rate Map (FIRM) No. 250167 0001 'Al (effective date April 3; 1978), the site is located in an area designated as Zone C, areas of minimal flooding. A flood zone map is provided as Figure 3 in Appendix:;: A. Additionally, there are no areas designated as flood zones within a '/?-mile radius of--the subject site. 2.2.2 Site Hydrology There is an area of mapped wetlands in the southwestern portion of the site. This wetland area appears to be the headwaters of two unnamed perennial streams. The western of these two streams is tributary to Turkey Brook. The eastern of these two streams is tributary to Parsons Brook. An unmapped stream is located on the northern parcel (see Site Plan in Appendix A). Y This stream originates in an area of standing water with hydrophytic vegetation at the ` base of an exposed bedrock wall and flows southeasterly toward the mapped stream that _i` is tributary to Parsons Brook. The source of the hydrology for this stream appears to be groundwater outbreaks from exposed bedrock fractures in the quarry wall. 2.2.3 Surficial and Bedrock Geology. According to the USGS Map Showing Textures of Unconsolidated Materials, Connecticut Valley Urban Area, Central New England (1979) there are mapped sand and gravel deposits within an area of till deposits in the vicinity of the subject site. Some layers of the sand and gravel deposits consist wholly of gravel particles; others are mixtures of gravel and sand particles; some layers contain as little as 25 percent gravel particles. Material occurs as well to poorly sorted layers of different thicknesses in which particle sizes may range from gravel'to sand both, laterally and vertically. Till Phase I Environmental Site Assessment 2-2 SECTION 2 GENERAL SITE DESCRIPTION and is typically a nonstratified, nonsorted mixture of gravel particles, sand particles, and fine particles in differing proportions. The map unit also includes large areas where no unconsolidated materials are present and bedrock is at the surface. According to the USGS Bedrock Geologic Map of Massachusetts (1983). The bedrock underlying this area of Northampton is classified as part of the Gil'e Mountain Formation. This bedrock is described as gray, slightly rusty, poorly bedded phyllite and schist containing beds of light gray, fine-grained quartzite with locally punky- brown weathering calcareous granofels or quartzose marble and vein quartz. 2.2.4 Surrounding Resource Areas According to the MassGIS map (Figure 2 in Appendix A), the site is not located within any Potentially Productive Aquifers, Zone II areas or an Interim Wellhead Protection Area of a public water supply. Also, no areas of Critical Environmental Concern, Natural Heritage and Endangered'Species Program areas, Sole Source Aquifers or Solid Waste Landfills were identified within 500 feet of the site. However, private wells.. are located within 500 feet of the property. 2.3 SITE RECONNAISSANCE On November 25, 2003, Tighe & Bond personnel conducted a site reconnaissance of the subject property. The area was viewed with respect to the general environmental condition of the property. The site was inspected for the presence of stained soil, areas, of dead or stressed vegetation, odors, areas of apparent fill, the presence and status of equipment containing polychlorinated biphenyls (PCBs), the presence of storage tanks and pits, or evidence of waste disposal or burial. The site was also inspected with respect to the presence of any wetlands or watercourses. Site Photographs are provided in Appendix C. 2.3.1 North Parcel (Lot 2) This parcel appeared to be the location of former quarrying operations. A large piece of crushing equipment was observed in proximity to the locked gate off Turkey Hill Road. This area appears to have been the center of staging and loading operations during the active period of quarry operation. Two trailers and a metal storage container with roof vents were also observed in this area. As shown on the aerial photograph provided as Figure 4 in Appendix A, the northern and western portions of this parcel consist of a mixed softwood and hardwood forest. No evidence of previous permanent structures or illegal dumping was observed at the time of this site reconnaissance. r~ I~ l SECTION 2 GENERAL SITE D'ESCRIPTION'. ' ighe&B®nd The Wzorek family sold the operation- and properties to Farmington Ready-Mix around 1983 or 1984. At that time, Farmington Ready-Mix moved the equipment from the Turkey Hill site to an operation located in Westfield, Massachusetts. I_ r~ ~r fl ~ I 't1 L I ^,t 2-5 SECTION 3 ENVIRONMENTAL REVIEW righe&B®nd J I 'J J As part of this site investigation, Tighe & Bond commissioned a database search of state and Federal records that would indicate the potential presence of environmental' hazards at, or in close proximity to, the subject site. The database search was supplemented by a file review conducted in person on November 26, 2003, at the Springfield office of the Massachusetts Department of Environmental Protection (DEP) to confirm database information and to review file data not otherwise available in the database. 3.1 DATABASE SEARCH A state and Federal database search for the site and surrounding area was conducted using, the FirstSearch Technology Corporation of Dedham, Massachusetts and is included in their Environmental FirstSearch report provided in Appendix D. The date of the most recent database update by the regulatory agency maintaining each database is listed at the beginning of the database search report. Those. sites with adequate address information are plotted on maps provided with the database report. A summary of those listings retrieved by the database search is provided in Table 3-1 below and..at the beginning of the Environmental FirstSearch report. Table 3-1 Database File Search Summary Turkey Hill Road Florence [Northampton], Massachusetts Database Searched Search Radius (mile) Sites Listed National Priority List 1 0 RCRA COR Facilities 1 0 State Identified Hazardous Waste Sites 1 2 Federal CERCLIS List .5 0 State Listed Landfills and Solid Waste Facilities .5 0 State Listed Spills - 1990 to Present .5 1 RCRA TSD Facilities .5 0 RCRA Generators - Large and Small Quantity .25 0 Emergency Response Notification System .25 1 State Registered UST/AST .25 0 The subject site was not listed. in any of the databases searched. There is one (1) state- listed spill site located within a 1/2-mile radius of the subject site. This site is a former Phase I Environmental Site Assessment 3-1 SECTION 3 ENVIRONMENTAL REVIEW i ig e&Bond automotive repair garage located at 92 Turkey Hill Road in the Village of Florence, City of Northampton, Massachusetts (RTN 1-12669). Of the 15 non-geocoded sites included in the database search, none are located within a 1-mile radius of the subject site. Those sites not researched during the DEP file review were either closed or were located crossgradient (based on inferred groundwater flow direction) to the subject site. 3.2 DEP FILE REVIEW A DEP file review was conducted on November 26, 2003, to identify any additional pertinent information for the site, to verify the relative locations of sites listed in the Environmental FirstSearch report and to assess the potential impact to the site from documented releases on any surrounding properties. The subject site was not listed in any of the databases searched. Also, no additional sites that could potentially have an environmental impact on the subject site were identified in these databases other than those listed in the Environmental FirstSearch report. A review of files for listed sites in close proximity to the subject property indicated the following: 92 Turkey Hill Road. This property is listed as a spill site (RTN 1-12669). This site is located approximately 1/2-mile southeast of the subject site. A location aid of "1,500 feet west of West Farms Road" was provided in the database search report. I A previous site investigation was prepared by Analytical Engineering, Inc. on March 18, 1997. At the time of that investigation, the site consisted of a masonry block building used for automotive repair operations and 'a small shed. ! A 275-gallon fuel oil above-ground storage tank (AST), a 40-gallon rusted drum, and a 5-gallon steel fuel container were observed at the site. Five (5) `l "grab" soil samples were collected from depths varying between 6-inches and 18-inches below grade. Of these five (5) soil samples, three (3) yielded positive detections of total petroleum hydrocarbons (TPH). Sample S-1, collected at the r j floor drain pipe outfall, had a TPH concentration of 130 mg/kg. Sample S-4, collected near the AST, had a TPH concentration of 1,100 mg/kg. Sample S-5, collected near the location of the rusted barrel, had a TPH concentration of 560 mg/kg. Each soil sample was "fingerprinted" by gas chromatography to determine the origin of the TPH contamination. Samples S-1 and S-5 were identified as motor oil and sample S-4 was identified as No. 2 fuel oil. A Release Abatement Measure (RAM) Plan, dated November 13, 1998 and prepared by Southampton Sanitary Engineering & Associates and Paul Hatch, P.E., LSP, was reviewed. This RAM Plan addressed the remediation of soil contamination in the vicinity of a former garage floor drain outlet and storage Phase I Environmental Site Assessment 3-2 SECTION 3 ENVIRONMENTAL REVIEW Teghe&B®nd shed on the property. According to the RAM Plan, TPH was detected in site soils at concentrations in exceedance of the applicable reporting concentrations. The RAM Plan included the removal and disposal of the AST, the excavation of contaminated soil and additional surficial soil sampling in the area of the rusted barrel identified during the previous site investigation. A Response Action Outcome (RAO) or "closure" report, dated February 9, 1999, was also reviewed. According to this report, 45.92 tons of contaminated soil was excavated from the property and transported to Ondrick's (Chicopee, Massachusetts) for proper disposal, the masonry block garage was demolished, and three (3) groundwater monitoring wells were installed. Confirmatory soil and groundwater samples were analyzed for extractable and volatile petroleum hydrocarbons (EPH/VPH) and volatile organic compounds (VOCs),. There were no positive detections of contaminants in either soil or groundwater. As such, a Class A-1 RAO was prepared for this site. Given the extent of soil excavation, the confirmatory analytical data, and the distance of this site from the subject site, it is likely that this site will pose little, if any, threat. of environmental impact to the subject site. No other reportable incidents or listed sites reviewed during the DEP file search for the surrounding. area appear to have the potential to have impacted environmental conditions at the subject site. 3.3 FIRE DEPARTMENT RECORDS A file review was conducted on December 4, 2003, to identify the presence of historic or existing underground storage tanks (USTs) at or in proximity to the subject site. There were no records regarding the subject property in the files of the Northampton Fire Prevention Office -and the nearest UST was located at 92 Turkey Hill Road (see Section 3.2), approximately 1/2-mile southeast of the subject site. Phase I Environmental Site Assessment 3-3 r-i SECTION 4 LIMITED SOIL INVESTIGATION Tighe&B®nd- Soil sampling was conducted to provide additional information relative to the conditions of subsurface materials at the site. A total of three (3) soil samples were collected from the subject site. Details of the limited soil investigation are discussed below. 4.1 SOIL SAMPLE COLLECTION On December 16, 2003, Tighe & Bond personnel collected three (3) soil samples from the subject property. These samples are identified as S-1, S-2, and S-3. Each sample was analyzed for EPH carbon fractions, target polycyclic aromatic hydrocarbons (PAHs) and VOCs. The approximate locations of these samples are shown on the Site Plan provided in Appendix A. The sampling locations were selected based on observations made during the site reconnaissance and the December 2, 2003 telephone conversation with Mr. James F. Wzorek, Jr. L 4.2 SOIL AND GROUNDWATER CLASSIFICATION Soil and groundwater are categorized for risk assessment purposes based upon the location and uses of the site and site groundwater. Specific standards have. been -J developed for both soil and groundwater based upon these uses and the potential for human or -environmental exposure. Soil and groundwater category classification criteria are set forth in 310 CMR 40.0933 and 40.0932 of the Massachusetts Contingency Plan (MCP). Based upon site conditions and exposure scenarios, the soil at the site meets the criteria i of soil category S-1, as defined by 310 CMR 40.0933. This determination is supported by the fact that the release-impacted area is within three (3) feet of the ground surface, the site is located near residential properties and children are potentially. present on the ` site at an unknown frequency and intensity. Based on a review of the MassGIS. map (Figure. 2 in Appendix A) and on site conditions, groundwater at the site meets the criteria of groundwater categories GW-1 and GW-3. The site is not located within a current or potential drinking water source 1 / area, but portions of the property are located within 500 feet of private wells. Thus, the GW-1 standards apply to the site. All sites in Massachusetts are subject to GW-3 - standards. Thus, the applicable Characterization Standards for the site soils are S-1/GW-1 and S- 1/GW-3, and the groundwater categories are GW-1 and GW-3. However, groundwater sampling was not included in the scope of work for this site assessment and there is no direct evidence to indicate impacts to site groundwater. Phase I Environmental Site Assessment l 4-1 SECTION 4 LIMITED SOIL INVESTIGATION Tighe&Bcndf 4.3 SOIL ANALYTICAL RESULTS As shown on Table 4-1, the concentrations of Extractable Petroleum Hydrocarbons (EPH) carbon fractions detected in soil samples S-1 and S-2 do not exceed the applicable Reportable Concentrations (RCS-1) for the site or the MCP Method 1 Soil Standards ( S-1/GW-1 and S-1/GW-3). Acetone was detected at a concentration of 2.1 mg/kg in sample S-1. This concentration is below the applicable RCS-1 and Method 1, S-1 Soil Standards. 1 :r However, 2-Butanone was detected at a concentration of 0.51 mg/kg in sample S-1. This concentration exceeds the applicable RC for this compound and constitutes a reportable condition. As such, a Limited Removal Action (LRA) must be performed within 120 days of your "knowledge of this release. If the Responsible Party (as defined in the MCP) does not perform an LRA in that time frame, the "release" must be reported to DEP within 120 days of knowledge. Table 4-1 Soil Analytical Data (mg/kg) Sample ID S-1 S-2 S-3 Method 1, S-1 Soil RCS 1 Date Collected 12/16/03 12/16/03 12/16/03 GW-1 GW-2 GW-3: - EPH Carbon Ranges C9-C18Aliphatics 13.7 13.2 <4.1 1,000 1,000 1,000 1,000 C11-C22 Aromatics 175 <5.1 <4.1 200 800 8b0 200 C19-C36 Aliphatics 601 30.7 <4.1 2,500 2,500 2,500 2,500 Volatile Organic Compounds (VOCs) cetone .2.1 <0.069 <0.051 3 60 60 3 12-Butanone (MEK) 0.51 <0.028 <0.050 0.3 40 40 0.3 For reference purposes, 2-Butanone has been assigned Chemical Abstract Service (CAS) number 78-93-3. 2-Butanone is also known as Methyl Ethyl Ketone (MEK). According to the Merck Index (Eleventh Edition, 1989), 2-Butanone is most commonly used as an industrial solvent in the coating industry as well as in the manufacture of smokeless powder and resins. According to the Agency for Toxic Substances and Disease Registry (ATSDR), 2-Butanone is also present in paints and other coatings, glues and cleaning agents. J Phase I Environmental Site Assessment 4-2 r~ SECTION 5 CONCLUSION righe&BOnd (l Tighe & Bond has completed a Phase 121E Environmental Site Assessment for Quarry _ Alternatives, Inc. for property located at the western end of Turkey Hill Road in the Village of Florence, City of Northampton, Hampshire County, Massachusetts in (,I accordance with ASTM Standard E1527-00 for Phase I Environmental Assessments. ,i As part of the assessment,. Tighe & Bond performed a limited soil investigation to determine whether there is the potential for a release or threat of release of oil or hazardous materials (OHM) in accordance with Massachusetts General Law Chapter t 21E. The site is currently owned by the Jedoron Realty Corporation and consists of two (2) parcels occupying 165.4 acres of land. The site is currently vacant land, but was formerly operated as a gravel mine and quarry. A database search and subsequent review of DEP records indicated that no reportable releases have occurred at the subject site and that no releases in the vicinity of the subject site are likely to pose any threat of environmental impact to the subject site. All other reported release incidents that have occurred in the vicinity of the subject. site should have little, if any, potential for environmental impact on the subject site. The limited soil investigation, included the collection of three (3) soil samples, identified as S-l, S-2, and S-3. The results. of the laboratory analysis of the S-1 soil sample indicate that 2-Butanone was present at a concentration greater than the applicable Reportable Concentration. No other reportable concentrations were detected in the soil samples. Thus, based on the results of this investigation, it appears that a release of OHM subject to remediation and/or reporting to the DEP has occurred. i. Phase I Environmental Site Assessment 5-1 SECTION 6 LIMIT'AT'IONS righe&Bond The work described in this report was performed in a manner consistent with generally accepted professional consulting principles and practices. No other warranty, express or implied is made. These services were performed consistent with our agreement with our client. This report is solely for the use and information of our client unless otherwise noted. Any reliance on this report by a third party is at such party's sole risk. Opinions • and recommendations contained in this report apply to conditions existing when services were performed and are intended only for the client, purposes, locations, time frames and project parameters indicated. We are not responsible for the impacts of any changes in environmental standards, practices, or regulations subsequent to performance of services. We do not warranty the accuracy of information supplied by others, nor the use of segregated portions of this report. 6-1 I f I~ SECTION 7 REFERENCES Tighe&Bond Commonwealth of Massachusetts, Department of Environmental Protection, Western Regional Office. Files reviewed November 26, 2003. FirstSearch Technology Corporation. Environmental FirstSearch Report, Turkey Hill Road, Florence, Massachusetts. November 26, 2003. Massachusetts Geographic Information Systems (MassGIS) Natural Resource Map. Northampton, City of. Assessor's Office. Records reviewed November 25, 2003. Northampton, City of. Building Department. Records reviewed December 4,'2003. Northampton, City of. Fire Prevention Office. Records reviewed December 4, 2003. United States Department of Housing and Urban Development. Flood Insurance Rate Maps No. 250167 0001 A, City of Northampton, Massachusetts, Hampshire County. Effective April 3, 1978. United States Geologic Survey, Bedrock Geologic Map of Massachusetts. E-an. Zen, editor. 1983. United States Geologic Survey, Map Showing Textures of Unconsolidated Materials, Connecticut Valley Urban Area, Central New England. Janet Radway Stone, Elizabeth Haley London, and William H. Langer. 1979. Wzorek, James F. Jr. Telephone conversation. December 2, 2003. J:\N\N0523\R E P 0 RT\TEXT. DO C Phase I Environmental Site Assessment 7-1 Z. 0~~,(/~ ~Ij 1 r ~JFr' ~ i~ ) 11 U i Flu ' e o ' r ~rLJ i ` •l~on ~ ~ji ~ III ti ~ I I, , I I,, ~l Illlrti ~ I /q ~~~~7 J I~: i~ f L ray I I i 1 r I ~ I s I I l I t s ~ r t / (/~/r~ r. ~ i. ~ r I ~ ~I ~ l ~ v ~ y 1111 ....r (f'~~ ~~~1 It{~~\ Ivl t'L./ j i ~j ~ I ~ , { r •.I /I 1 1 ./I,'i / ` - I(1l.)~'\, ~ } • ~ ci . 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Ic, 1 sly 4 S( ~A I ` pp I v SITE LOCATION 1(( ' A•- '9~ ~ 11 ,.1 ~ f~~ I ~ a- 1~ ~ ~ ~i- ~ .LL -•i _i ta~tir}9 'I ~.J~I ( j i%. ~ I~ ~~;,1 ~~~1{~~/ i\~ J~ u~j~\ V / ''~'I Q' 1:',Jr r `„~i5-c. ~~nL~~-~ o J` I ` .t~\l }J JI~i' I1 t; r ° W t eSft s\t } O~ Y t~ ~'y 4„ y . f ~_✓./'.~'t~ ~ , j ~ ; ~r ESTHAM ; !y~~ ^1.1~~ '?oT - ){~~r~l (i+flJ/~` t Ill u~ ~ ! f ! ~if"" ~f~ . I 1 % /I .U ' i9 ~ ! /I r ~./~I I. ✓r~/lJ tll ~ 1~/~ / ~ ~ 7~L~~ir- C ~ ° " i' ~ ~ I lr: h fi \ ~ i ~ 1 k't !'Eli:-~ ~v , ~ `1- th, ~ ~ ~ ~ ~ ~ -mot I - -,l ~ 1 ~ •t _ ~ „ k' ! \ 1IY~., 4•~ ky~511} Ya`dlsl ` IJI)1\ t ~'~~yfii c J~~1 P CIRCLES INDICATE 500-FOOT AND 1/2-MILE RADII 'iz;\~~~ BASED ON USGS TOPOGRAPHIC MAPS FOR FIGURE 1 WESTHAMPTON & EASTHAMPTON, MA SITE LOCUS QUADRANGLES. REVISED 1987 & 1979. 3-METER & 10-FOOT CONTOUR INTERVALS. FORMER QUARRY AT TURKEY HILL N TURKEY HILL ROAD rho m~ VILLAGE OF FLORENCE NORTHAMPTON, MASSACHUSETTS MASS. W E Tighe&Bond SCALE: 1:25000 JANUARY 2004 ._Al N0523.apr'- - '.1 (I T, I 1\ )1 ~ - ~-s M. II ' 31 (n 4-g 3 -p m t z ~M o C l D 1 r .~T F 1 T. d 66 - i'\ p I % I o 1, ( { BASED ON MassGIS MAP -FEBRUARY 2002. CIRCLES INDICATE 500-FOOT AND 1/2-MILE RADII. ;y-- Nan Potenli0l Drinking Water Source Area: Medium Yield I' Public Surface Water Supply (PSWS) FIGURE 2 E;->i Non Patenlial Drinking Water Source Area: High Yield C Community Public Water Supply-Surface Water 'tiPolenliolly Productive Modium Yield Aquifer © Community Public Water Supply-Groundwater C Potentiolly Productive High Yield Aquifer ® Nml-COmmunity Non-Transienl Public Water Supply MassGIS MAPPING Q EPA Designated Sole Source Aquifer N.'Communily Transient Public Water Supply Q DEP Appmvad Wellhead Protection Araa(Zone2) NHESP 2003 Massachusetts Certified Vernal Pools DEP Interim Wellhead Protection Area (IWPA ) ® Multi- Limited A Lone s Highwey, Highway NOT Limited Across FORMER QUARRY AT TURKEY HILL 0 ®cces Public Surface Water Supply Protection Area (Zeno A) Other Numbered Highway Esc--e`:ti Lake, Pond, Stream or other Fresh Water Feature ° 11, lor Roe or Road TURKEY HILL ROAD - Minor Slra et or Rood Bay Estuary or other Sell Water Feature Tm.korTrail N VILLAGE OF FLORENCE Frash Water Nan-Foracted Welland Town Boundary itdz• Sal( Water Welland County Boundary I--I--F Train NORTHAMPTON MASSACHUSETTS NHESP 2003 Priority Flabilels for Slate-Pmtoctad O~Powedirro d Ram Species and Estimated Hab'Aels for Ram Wildlife' Pipeline W E Protected and Recreational Open Spam _ Rivers and Slraams Aqueduct R AlaesofCritical EnvironmentalConcern (ACEC) ~MafbrDreinagaBasin Tighe&Bend Solid Wesle landfill Sub Drainage Basin S - USGS Ouedrengle Boundary 'NHESP 2003 Pdmtl Hat-la Sbtc•Pml,-d Rmd Spa-1107 Nwuhnllo'S,gM.-I Heanorni dasigaatad under Ah,-h-M Endmga,ad 5,,., Act SCALE: ,I IIHESP 2003 EnmSOd llnbbu la Rao Wdd,t.FcrU,. wish lha MAYiNmb Prclacaon Ad Ragutatms f310 CMR 101 1:25000' JANUARYr~~/ 2014 N0523.apr I f (-j l_~l I_J J1 ~I J I~J I SITE LOCATION l CIRCLES INDICATE 500-FOOT AND 1/2-MILE RADII. MAP LEGEND: FIGURE 3 FEMA Flood Zones A MHD Rds by Class Ig scale Limited Access Highway FLOOD ZONE MAP AE Multi-Lane Highway, NOT Limited Access AH Other Numbered Hwy FORMER QUARRY AT TURKEY HILL ® AO V N Major Road - Connector it Minor street Road TURKEY HILL ROAD VE l Track or Trail r y ^ VILLAGE OF FLORENCE AN[ _ x tk NORTHAMPTON, MASSACHUSETTS W E o X500 Tghe&Bond D UNDES SCALE: 1:25000 JANUARY 2004 N0523.apr 1 ~J ++r ` l JJ1 i I 1 N0523.apr C) C) a C) C) co LLI i c- F- U ah d J > U ° o E 0 _ z a o Z o p o l I o w a a " Lil J as _j - U Q U > Z ? ti 0 . 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I lJ } f (f I f I~ I f`7 I i ~ Photo 3 - Constructed stormwater management feature on Lot 4. Photo 4 - Constructed stormwater detention basin on Lot 4. Locked access gate to Lot 2 visible in background. 'r i Photo 5 - View of roadway through Lot 4 from the north. Stone-filled gabions visible on either side:,,.: of roadway. Photo 6 - Access roadway/staging area to former quarry operations. Trailer visible on left side of picture. Ir ~ t I j ~ J I I~ ~ f Il ~J I~ it ~j f~. Photo 7 - View, from south, of abandoned rock crusher on Lot 2. Photo 8 - View, from north, of abandoned rock crusher on Lot 2. r-i I~~l _j r~ i j I -1 Photo 9 - Close-up of abandoned rock crusher on Lot 2. Photo 10 - "Headwater" wetland (to unmapped intermittent stream) on Lot 2. FarstSearch Technology Corporation Environmental FirstSearcW Report IJ . ~J r; TARGET PROPERTY: TURKEY HILL ROAD FLORENCE MA 01062 Job Number: 230523172 PREPARED FOR: Tighe & Bond 130 Southampton. Road Westfield, MA 01085 11-26-03 I` I Tel: (781) 320-3720 Fax: (781) 320-3715 Environmental FirstSearch is a registered trademark of FirstSearch Technology Corporation. All rights reserved. ~I r-~ IJ ~J l_J I j n l~ 1 ~J I~ r~ ~l Environmental Firsdearch Site Detail Report TARGET SITE: TURKEY HILL ROAD JOB: 230513172 FLORENCE MA 01062 QUARRY PHASE 121E SOLID WASTE LANDFILL SITE SEARCH ID: 16 DIST/DIR: NON GC MAP ID: NAME: EASTHAMPTON LANDFILL REV: 7/2/03 ADDRESS: LOUDVILLE RD IDl. SL0087.003 EASTHAMPTON MA ID2: STATUS: CLOSED CONTACT: PHONE: OWNER INFORMATION OWNER: TOWN OF EASTHAMPTON TYPE OF OWNER: MUNICIPAL OWNER ADDRESS: 43 MAIN ST EASTI•IAMPTON, MA 01027 OWNER CONTACT: JOSEPH PIPCYZNSKI, DPW DIR OWNER PHONE: (413)527-0793 OPERATOR INFORMATION OPERATOR: TOWN OF EASTHAMPTON OPERATOR ADDRESS: 43 MAIN ST EASTHAMPTON, MA 01027 OPERATOR CONTACT: JOSEPH PIPCYZNSKI, DPW DIR OPERATOR PHONE: (413)527-0793 SITE INFORMATION YEAR OPENED: 0 YEAR OPERATIONS CEASED: ' 1969 OPERATIONAL PLAN/PERMIT?. PLAN/PERMIT APPROVAL DATE: TYPE OF LANDFILL: MUNICI TONS PER DAY OF SOLID WASTE SITE MAY HANDLE OR DISPOSE: 0 SITE SIZE ASSIGNED BY LOCAL BOARD OF HEALTH: 6 ACRES SITE SIZE APPROVED BY DEP: 6 ACRES LEACHATE COLL.: LINER?: Not Lined CAPPING TYPE: Capped CAPPING TYPE: Capped Site Details Page - •2 it l TARGET SITE: Environmental FirstSearch Site Detail Report TURKEY HILL ROAD FLORENCE MA 01062 JOB: 230523172 QUARRY PHASE I 21E STATE SPILLS SITE SEARCH ID: 6 DIST/DIR: NON GC MAP ID: NAME: EMPRESS OIL ROLLOVER REV: ADDRESS: KINGS HIGHWAY IDI: W93-0323 WESTHAMPTON MA 01027 ID2: 0000 STATUS: CONTACT: WRIGHT, A PHONE: CASE CLOSED? YES SPILL DATE: 19930624 SPILL TIME: 12:OOPM DATE REPORTED: 19930624 REPORT TIME: 01:30PM SPILL NOTIFIER: JANINE DOMINA/EXPRESS OIL CO NOTIFIER PRONE: SPILL DESCRIPTION: INCIDENT: M.V. ACCIDENT MATERIAL SPILLED: 42 FUEL OIL AMT RPTD SPILLED: UNKNOWN GALLONS ACTUAL AMT SPILLED: 251-500 GALLONS SOURCE OF SPILL: TANKER TRUCK PET/B.AZ: PETROLEUM VIR/WASTE: VIRGIN PCB LEVEL: NONE ENVIRONMENTAL IMPACT: SOIL LUST?: NO SOIL CONTAMINATED?: CONTRACTOR: NOT USED PREPARE REPORT: DAYS/CLOSE: 0 Site Details Page - 3 _l TARGET SITE: Environmental Firsdearch Site Detail Report TURKEY HILL ROAD JOB: 230523172 FLORENCE MA 01062 QUARRY PHASE I 21E STATE SPILLS SITE SEARCH ID: 7 DIST/DIR: NON GC MAP ID: NAME: FRM ZONOLITE PLANT REV: 10/10/03 ADDRESS: WEMELCO WAY IDI: 1-0013515 EASTHAMPTON MA 01027 ID2: STATUS: TIER 2 CONTACT: PHONE: SITE IMF, ORYIATION STATUS: TIER 2 -A site/release receiving a total NRS scoreless than 350, unless the site meets any of the Tier 1 Inclusionary Criteria (CMR 40.0520(2)(a)). Permits are not required at Tier 2 sites/releases and response actions may be performed under the supervision of an LSP without prior DEP approval. All pre-1993 transition sites that have accepted waivers are categoricallyTier 2 sites. CATEGORY: TWO HR 21E STATUS: TIER 2 DATE: 6/30/2000 23E DATE: 7/2/2001 PHASE: PHASE II HAZMAT TYPE: HAZARDOUS MATERIAL RAO CLASS: LOCATION TYPE: INDUSTRIAL,, SOURCE: HISTORICAL; SITE DESCRIPTION: CHEMICALS ASBESTOS SITE ACTIONS ACT DATE: 6/30/2000 ACT USE LIMITATION: LSP: ACT STATUS: REPORT ACT TYPE: REPORTABLE RELEASE UNDER MGL 2 RAO TYPE: ACT DATE: 7/2/2001 ACT USE LIMITATION: LSP: ACT STATUS: TIERII ACT TYPE: TIER 2 CLASSIFICATION RAO TYPE: ACT DATE: 7/2/2001 ACT USE LIMITATION: LSP: ACT STATUS: CSRCVD ACT TYPE: COMPLETION STATEMENT RECEIVED RAO TYPE: I Site Details Page - 4 i1 l TARGET SITE: I~. a_. I~ f' I] l~ iT t-l ; !l_J • IL Environmental Firsdearch Site Detail Report TURKEY HILL ROAD JOB: 230523172 FLORENCE MA 01062 QUARRY PHASE 12 1E STATE SITE SEARCHED: 3 DIST/DIR: NON GC MAP ID: NAME: FRM ZONOLITE PLANT REV: 10/10/03 ADDRESS: WEMELCO WAY IDI: 1-0013515 EASTHAMPTON MA 01027 ID2: STATUS: TIER 2 CONTACT: PHONE: SITE INTOILiTATION STATUS: TIER 2 -A site/release receiving a total NRS scoreless than 350, unless the site meets any of the Tier 1 Inclusionary Criteria (CMR 40.0520(2)(a)). Permits are not required at Tier 2 sites/releases and response actions may be performed under the supervision of an LSP without prior DEP approval. All pre-1993 transition sites that have accepted waivers are categorical lyTier 2 sites. CATEGORY: TWO HR 21E STATUS: TIER2 DATE: 6/30/2000 21 E DATE: 7/2/2001 PHASE: PHASE II HAZMAT TYPE: HAZARDOUS MATERIAL RAO CLASS: LOCATION TYPE: INDUSTRIAL, SOURCE: HISTORICAL; SITE DESCRIPTION: CHEMICALS ASBESTOS SITE ACTIONS ACT DATE: 6/30/2000 ACT USE LIMITATION: LSP: ACT STATUS: REPORT ACT TYPE: REPORTABLE RELEASE UNDER MGL 2 RAO TYPE: ACT DATE: 7/2/2001 ACT USE LIMITATION: LSP: ACT STATUS: TIERII ACT TYPE: TIER 2 CLASSIFICATION RAO TYPE: ACT DATE: 7/2/2001 ACT USE LIMITATION: LSP: ACT STATUS:" CSRCVD ACT TYPE: COMPLETION STATEMENT RECEIVED RAO TYPE: Site Details Page - 5 1 TARGET SITE: Environmental FirstSearch Site Detail Report TURKEY HILL ROAD JOB: 230523172 FLORENCE MA 01062 QUARRY PHASE 12 1E STATE SITE SEARCH ID: 4 DIST/DIR: NON GC MAP ID: NAME: OXBOW STATE BOAT RAMP REV: 10/23/02 ADDRESS: ROUTE 5 ID1: I-0013709 EASTHAMPTON MAO 1027 ID2: STATUS: DEF TIER 1B CONTACT: PHONE: SITE INrOILI'IATION STATUS: DEF TIER IB -(Default Tier 1B): A site/release where the responsible party fails to provide a required submittal to DEP by a specified deadline. CATEGORY: TWO HR 21E STATUS: DEF TIER 1B DATE: 12/4/2000 21E DATE: 12/11/2001 PHASE: HAZMAT TYPE: RAO CLASS: LOCATION TYPE: STATE, SOURCE: DRUMS; SITE DESCRIPTION: CHEMICALS UNKNOWN CHEMICAL OF UNKNOWN TYPE 26 GAL UNKNOWN CHEMICAL OF UNKNOWN TYPE 26 GAL SITE ACTIONS ACT DATE: 12/04/2000 ACT USE LIMITATION: LSP: ACT STATUS: REPORTABLE RELEASE UNDER MGL 21E ACT TYPE: RELEASE DISPOSITION RAO TYPE: ACT DATE: 12/04/2000 ACT USE LIMITATION: LSP: ACT STATUS: ORAL APPROVAL OF PLAN ACT TYPE: IMMEDIATE RESPONSE ACTION RAO TYPE: ACT DATE: 12/04/2000 ACT USE LIMITATION: LSP: ACT STATUS: WORK STARTED ACT TYPE: IMMEDIATE RESPONSE ACTION - DEP LEAD RAO TYPE: I Site Details Page - 10 r~ I l_J L_1 I. u r~ IJ I I I~ I~Iii I~ J Environmental FirstSearch Site Detail Report TARGET SITE: TURKEY HILL ROAD JOB: 230523172 FLORENCE MA 01062 QUARRY PHASE 12 1E STATE SPILLS SITE SEARCH ID: 11 DISUDIR: NON GC MAP ID: NAME: POLE 918 58 REV: 10/10/03 ADDRESS: MAIN RD IDI: 1-0014684 WESTHAMPTON MA 01027 ID2: STATUS: RAO CONTACT: PHONE: SITE INFORA MTION STATUS: RAO - (Response Action Outcome): a site/release where an RAO statement was submitted. An RAO Statement asserts that response actions were sufficient to achieve a level of no significant risk or at least ensure that all substantial hazards were eliminated. CATEGORY: TWO HR 21E STATUS: RAO DATE: 12/17/2002 21E DATE: 2/19/2003 PHASE: HAZMAT TYPE: OIL RAO CLASS: •A2 - A PERMANENT SOLUTION LOCATION TYPE: ROADWAY, SOURCE: TRANSFORM; SITE DESCRIPTION: CHEMICALS UNKNOWN CHEMICAL OF TYPE - OIL 14 GAL SITE ACTIONS ACT DATE: 12/17/2002 ACT USE LIMITATION: LSP: ACT STATUS: REPORT ACT TYPE: REPORTABLE RELEASE UNDER MGL 2 RAO TYPE: ACT DATE: 2/19/2003 ACT USE LIMITATION: NONE LSP: 4589 ACT STATUS: RAORCD ACT TYPE: RAO STATEMENT RECEIVED RAO TYPE: A2 - A PERMANENT SOLUTION HAS ACT DATE: 2/19/2003 ACT USE LIMITATION: LSP: ACT STATUS: REPORT ACT TYPE: REPORTABLE RELEASE UNDER MGL 2 RAO TYPE: - Continued on next page - i Site Details Page - 11 I r` _I ii r~ ' I n 1J IF-' L. ~ I J I~ L-~ J Environmental FirstSearch Site Detail Report TARGET SITE: TURKEY HILL ROAD JOB: 230523172 FLORENCE MA 01062 QUARRY PHASE 121E STATE SPILLS SITE SEARCH ID: 11 DIST/DIR: NON GC MAP ID: NAME: POLE #18 58 REV: 10/10/03 ADDRESS: MAIN RD IDI: 1-0014684 WESTHAMPTON MA 01027 ID2: STATUS: RAO CONTACT: PRONE: ACT DATE: 12/17/2002 ACT USE LIMITATION: LSP: ACT STATUS: APORAL ACT TYPE: ORAL APPROVAL OF PLAN RAO TYPE: Site Details Page - 12 TARGET SITE i ~J IL ~J r~ ~J I f7 ,L. ~f 4-~ _J Li Environmental Firsdearch Site Detail Report TURKEY HILL ROAD JOB: 230523172 FLORENCE MA. 01062 QUARRY PHASE I 21E STATE SPILLS SITE SEARCH ID: 5 DIST/DIR: NON GC MAP ID: NAME: POLE 4-03 REV: 10/10/03 ADDRESS: PINE STREET EXT IDI: 1-0014568 NORTHAMPTON MA ID2: STATUS: RAO- CONTACT: PHONE: SITE INF01?PL4TI0N STATUS: RAO -(Response Action Outcome): a site/release where an RAO statement was submitted. An RAO Statement asserts that response actions were sufficient to achieve a level of no significant risk or at least ensure that all substantial hazards were eliminated. CATEGORY: TWO HR 21E STATUS: RAO DATE: 9/11/2002 21E DATE: 11/13/2002 PHASE: HAZMAT TYPE: RAO CLASS: A2 - A PERMANENT SOLUTION LOCATION TYPE: ROADWAY, SOURCE: TRANSFORM; SITE DESCRIPTION: CHEMICALS UNKNOWN CHEMICAL OF UNKNOWN TYPE 40 GAL SITE ACTIONS ACT DATE: - 9/11/2002 ACT USE LIMITATION: LSP: ACT STATUS: REPORT ACT TYPE: REPORTABLE RELEASE UNDER MGL 2 RAO TYPE: ACT DATE: 9/11/2002 ACT USE LIMITATION: LSP: EVAN JOHNSON ACT STATUS: APORAL ACT TYPE: ORAL APPROVAL OF PLAN RAO TYPE: ACT DATE: 9/4/2003 ACT USE LIMITATION: NONE LSP: EVAN JOHNSON ACT STATUS: TSAUD ACT TYPE: TECHNICAL SCREEN AUDIT RAO TYPE: A2 - A PERMANENT SOLUTION HAS - Continued on ne-rt page - ~'tJ Site Details Page - 13 I^~ Environmental FirstSearch Site Detail Report J TARGET SITE: TURKEY HILL ROAD JOB: 230523172 FLORENCE MA 01062 QUARRY PHASE 12 1E STATE SPILLS SITE SEARCH ID: 5 DIST/DIR: NON GC MAP ID: NAME: POLE 4-03 REV: 10/10/03 ADDRESS: PINE STREET EXT IDI: 1-0014568 NORTHAIMPTON MA ID2: STATUS: RAO CONTACT: PHONE: ACT DATE: 9/23/2002 ACT USE LIMITATION: LSP: ACT STATUS: REPORT ACT TYPE: REPORTABLE RELEASE UNDER MGL 2 RAO TYPE: 1 'J ---Site DMc i7s Page - I Environmental FirstSearch Site Detail Report r: TARGET SITE: TURKEY BILL ROAD JOB:. 230523172 FLORENCE MA 01062 QUARRY PHASE I 21E STATE SPILLS SITE SEARCH ID: 12 DIST/DIR: NON GC MAP ID: NAME: RAVINE OFF REV: ADDRESS: KNIPFER AVENUE IDI: W92-0140 EASTHAMPTON MA 01027 ID2: 0000 STATUS: CONTACT: CARPENTER, C PHONE: CASE CLOSED? YES SPILL DATE: 19920330 SPILL TIME: DATE REPORTED: 19920330 REPORT TIME: SPILL NOTIFIER: AL MORRISETTE-EH AMPTON FIRE NOTIFIER PHONE: SPILL DESCRIPTION: INCIDENT: OTHER RELEASE > SUSPECTED HAZ MATERIAL SPILLED: OTHER MATERIAL > ANIT RPTD SPILLED: 1-10 DRUMS ACTUAL AMT SPILLED: 1-10 DRUMS SOURCE OF SPILL: DRUM PET/-AZ: NEITHER VIR/WASTE: WASTE PCB LEVEL: NONE ENVIRONMENTAL IMPACT: LUST?: NO SOIL CONTAMINATED?: CONTRACTOR: NOT USED PREPARE REPORT: -DAYS/CLOSE: 1 Site Details Page - 15 Environmental FirstSearch Site Detail Report TARGET SITE: TURKEY HILL ROAD JOB:_ 230523172 FLORENCE MA 01062 QUARRY PHASE 12 1E STATE SPILLS SITE SEARCH ID: 13 DIST/DIR: NON GC MAP ID: NAME: SEWAGE LIFT STATION/LOWER MILL REV: ADDRESS: LIBERTY STREET ID1: W92-0192 EASTHAMPTON MA 01027 ID2: 0000 HAMPSHIRE STATUS: CONTACT: SLOWICK, D PHONE: CASE CLOSED? YES SPILL DATE: 19920425 SPILL TIME: 07:OOAM DATE REPORTED: 19920425 REPORT TIME: 08:30AM SPILL NOTIFIER: DAVE GAGNON- EHAMP SEWER DIVISION NOTIFIER PHONE: SPILL DESCRIPTION: INCIDENT: OTHER RELEASE > FLOODED OUT MATERIAL SPILLED: DIESEL FUEL AMT RPTD SPILLED: 101-250 GALLONS ACTUAL AIMT SPILLED: 101-250 GALLONS SOURCE OF SPILL: ABOVE-GRND TANK PET/HAZ: PETROLEUM VIR/WASTE: VIRGIN PCB LEVEL: NONE ENVIRONMENTAL IMPACT: LUST?: NO SOIL CONTAMINATED?: CONTRACTOR: NOT USED PREPARE REPORT: DAYS/CLOSE: 128 Site Details Page - 16 Environmental FirstSearch Site Detail Report TARGET SITE: TURKEY HELL ROAD FLORENCE MA 01062 JOB: 230523172 QUARRY PHASE 121E STATE SPILLS SITE SEARCH ID: 14 DIST/DIR: NON GC MAP ID: NAME: STORM DRAINAGE REV: ADDRESS: FROMT OF CHAPMAN AVENUE IDI: W91-0219 EASTHAMPTON MA 01027 ID2: 0000 HAMPSHIRE STATUS: CONTACT: FISH, B PHONE: CASE CLOSED? YES SPILL DATE: 19910425 SPILL TIME: DATE REPORTED: 19910426 REPORT TIME: 10:40AIvi SPILL NOTIFIER: AL MORRISETTE- EHAMP FIRE DEPT. NOTIFIER PHONE: SPILL DESCRIPTION: INCIDENT: DUMPING MATERIAL SPILLED: 92 FUEL OIL AMT RPTD SPILLED: UNKNOWN GALLONS ACTUAL AMT SPILLED: LESS THAN 1 GALLONS, SOURCE OF SPILL: OTHER SOURCE > UN KNOWN PET/HAZ: PETROLEUM VIR/WASTE: VIRGIN PCB LEVEL: NONE ENVIRONMENTAL IMPACT: LUST?: NO SOIL CONTAMINATED?: CONTRACTOR: NOT USED PREPARE REPORT: DAYS/CLOSE: 3 Site Details Page - 17 Environmental Firsdearch Site Detail Report TARGET SITE: TURKEY HILL ROAD JOB: 230523172 FLORENCE MA 01062 QUARRY PHASE I 21E STATE SPILLS SITE SEARCH ID: 15 DIST/DZR: NON GC MAP ID: NAME: TTU ACCIDENT REV: 10/10/03 ADDRESS: PARK ST IDI: 1-0011609 EASTHAMPTON MA 01027 ID2: STATUS: RAO CONTACT: PHONE: SITE INFORMATION STATUS: RAO - (Response Action Outcome): a site/release where an RAO statement was submitted. An RAO Statement asserts that response actions were sufficient to achieve a level of no significant risk or at least ensure that all substantial hazards were eliminated. CATEGORY: TWO HR 21E STATUS: RAO DATE: 11/26/1996 21E DATE: 5/23/1997 PHASE: HAZII4AT TYPE: OIL RAO CLASS: Al - A PERMANENT SOLUTION LOCATION TYPE: ROADWAY, SOURCE: VEHICLE; SITE DESCRIPTION: .CHEMICALS DIESEL FUEL 40 GAL UNKNOWN CHEMICAL OF UNKNOWN TYPE SITE ACTIONS ACT DATE: 11/2611996 ACT USE LIMITATION: LSP: ACT STATUS: REPORT ACT TYPE: REPORTABLE RELEASE UNDER MGL 2 RAO TYPE: ACT DATE: 5/27/1997 ACT USE LIMITATION: NONE LSP: PAUL HATCH ACT STATUS: FEEREC ACT TYPE: FEE RECEIVED-FMCRAUSE ONLY RAO TYPE: Al - A PERMANENT SOLUTION HAS ACT DATE: 1/15/1997 ACT USE LIMITATION: LSP: ACT STATUS: REPORT ACT TYPE: REPORTABLE RELEASE UNDER MGL 2 RAO TYPE: - Continued on next page - l_J Site Details Page - 18 Environmental FirstSearch Site Detail Report `I i TARGET SITE: TURKEY H]LL ROAD FLORENCE MA 01062 JOB: 230523172 QUARRY PHASE I 21E STATE SPILLS SITE SEARCH ID: 15 DIST/DIR: NON GC MAP ID: NAME: TTU ACCIDENT REV: 10/10/03 ADDRESS: PARK ST IDI: 1-0011609 EASTHAMPTON MA 01027 ID2: STATUS: RAO CONTACT: PHONE: ACT DATE: 3/28/1997 ACT USE LIMITATION: LSP: PAUL HATCH ACT STATUS: STRCVD ACT TYPE: STATUS REPORT RECEIVED RAO TYPE: a Site Details Page - 19 ~L Environmental FirstSearch Site Detail Report TARGET SITE: TURKEY HILL ROAD JOB: 230523172 FLORENCE MA 01062 QUARRY PHASE 121E I~I i F1 I I_ r-, J i r~ I L_i 'LL IL I i. i f ~j i EMERGENCY RESPONSE NOTIFICATION SITE SEARCH ID: 2 DIST/DIR: NON GC MAP ID: NAME: WHITING ENERGY FUEL REV: 11/14/900 ADDRESS: SIX STRTS:STRAW/VERONA/GARFIELD/HIGH/CHE ID1: 190641 FLORENCE MA ID2: STATUS: CONTACT: PHONE: SPILL INFORMATION DATE OF SPILL: 11/14/90 TIME OF SPILL: 1133 PRODUCT RELEASED (1): HOME HEATING OIL QUANTITY (1): 101 UNITS (1): GAL PRODUCT RELEASED (2): QUANTITY (2): UNITS (2): PRODUCT RELEASED (3): QUANTITY (3): UNITS (3): MEDIUM/MEDIA AFFECTED AIR: NO GROUNDWATER: NO LAND: YES FIXED FACILITY: NO WATER: NO OTHER: NO WATERBODY AFFECTED BY RELEASE: NONE CAUSE OF RELEASE DUMPING: NO EQUIPMENT FAILURE: NO NATURAL PHENOMENON: NO OPERATOR ERROR: NO OTHER CAUSE: NO TRANSP. ACCIDENT: NO UNKNOWN: NO ACTIONS TAKEN: FIRE DEPT BUILT A DAM OF ABSORBS AROUND DRAIN-USED SLICKWICK & CORNHUS KS TO AB RELEASE DETECTION: TRUCK CARRYING 5200 GAL HOME HEATING OIL CASTING BROKE OFF THE DELIVERY PUMP MISC. NOTES: FIRE F IGHTERS TRIED TO CLEAN OIL OUT OF STORM DRAIN WITH ABSORBANT TOW ELS DISCHARGER INFORMATION DISCHARGER ID: 190641 -DUN & BRADSTREET TYPE OF DISCHARGER: NAME OF DISCHARGER: WHITING ENERGY FUEL ADDRESS: Site Details Pate - 20 Environmental FirstSearch Street Name Report for Streets within .25111file(s) of Target Property TARGET SITE: TURKEY HILL ROAD JOB: 230523172 FLORENCE MA 01062 QUARRY PHASE I 21E Street Name Dist/Dir Street Name Dist/Dir Turkey Hill Rd 0.00-- 'Li w Environmental FirstSearch ~Iw & e 1 Mile Radius ASTM Map: NPL, RCRACOR, STATE Sites TURKEY HILL ROAD, FLORENCE MA 01062 Envixvnruental, FIRSTS. i .fir I•y. lee II I t5 ti ~~1 Z lTJ a 0 0 3 fD II Source: 1999 U.S. Census TIGER Files Target Site (Latitude: 42.310845 Longitude: -72.730626) Identified Site, Multiple Sites, Receptor L d ) or Hazar ous Waste NPL, Solid Waste Landfill (SW Railroads - Black Rings Represent I/4 Mile Radii; Red Ring Represents 500 ft. Radius _J Cf d' Environmental FirstSearch .5 Mile Radius ASTM Map: CERCLIS, RCRATSD, LUST, SWL TURKEY HILL ROAD, FLORENCE MA 01062 n Eu~r~~ FIRSTS i. I Fowre: 1999 U.S. Census TIGER Files Tar6get Site (Latitude: 42.310845 Longitude: -72.730626 I ) J Identified Site, Multiple Sites, Receptor NPL, Solid Waste Landfill (SWL) or Hazardous Waste I Railroads - Black Rings Represent 1/4 Mile Radii; Red Ring Represents 500 li. Radius CS ~I Environmental FirstSearch .25 Mile Radius ASTM Map: RCRAGEN, ERNS, UST TURKEY HILL ROAD, FLORENCE MA 01062 Envirunmemwwdl, FIRSTS Turke. Source: 1999 U.S. Census TIGER Files , Target Site (Latitude: 42.310845 Longitude: -72.730626) Identified Site, Multiple Sites, Receptor NPI, Solid Waste Landfill (SWL) or Hazardous Waste Railroads - Black Rings Represent 1/4 Mile Radii; Red Ring Represents 500 It. Radius w Environmental FirstSearch nv 5 Mile Radius FIRSTS< = Non-ASTM Map: Spills 90 u TURKEY HILL ROAD, FLORENCE MA 01062 n -Source: 1999 U.S. Census TIGER Files J Target Site (Latitude: 42.310845 Longitude: -72.730626) Identified Site, Multiple Sites, Receptor im NPL, Solid Waste Landfill (SWL) or Hazardous Waste National Historic Sites and Landmark Sites Railroads - Black Rings Represent 1/4 Mile Radii; Red Ring Represents 500 fl. Radius i l r'. I I f j f I-J f-~ I i -I r-1 Y 1 J n ) f, 1 1i I i f -J I I I Y t .1 ) ~ I 1 Sall AnalyOcal Data ' Ferm.r0uamy.tTurk.y Hol Turks HIII Read, Northam ron,Mu.achua.da Samploo 11 5.2 .3 Mothed I. S•1 Sea R.POnwbl. Dote C.A.00d 17116107 12/12-7 12116107 Cmc.npadons GW-1 GW2 GW-3 RCS-1 UCL EPH Carbon Ran .a 9r eA6pheocs 13.7• 17,2 4.1 1.000 1,000 1.000 1,000 20,000 Cu•C•a Nemotla 175 45.1 <q,1 200 Sao 900 200 70,000 GrCa AlphOAC$ 601 70.7 0.1 2.500 2.500 2500 2.500 20,000 To .tad PAH Ana s Aconopl Tona 40,10 40,51 40.17 20 1.000 1.000 20 10,000 AcemphN,n, 4040 40,51 40,41 100 100 100 t3 'a.G3 Andw...no 4.40 40.51 :OA1 1400 1,000 1,000 1,000 10,000 El no <OAO 40.51 4,11 0.7. 0.7 0.7 D.7 100 Bomo(aIR'rano 4.40 -0.51 40.91 0.7 0.7 0.7 0,7 100 BomO(b)AUOI.nNene :DAO 40.51 40.91 0.7 0.7 0.7 0.7 100 Bemo[gh3)parylen0 40.40 4051 4.41 1.000 1.000 1.000 1,000 10.000 Bonm(k)AUareNhena 40A 40.51 'OA1 7 7 7 7 40D Chrysane 40.90 40.51 40.41 1 1 7 7 400 DiOemo[ah)onthr...no 'OAD :0.5 40.41 0.7 . 0,7 0.7 0.7 100 FNormWen. :OAO 40.51 40.41 1,OOD 1,000 1,000 1.000 10,000 FWOrono -<OAO 40.51 4Al 400 1,000 1,000 400 10,000 Ndano[123cdtpy.n. 40.10 40,51 4.41 0.7 0.7 .0.7 03 100 2-MoUtMephlbelena 40.40 4451 <OAi 4 500 SOD 4 10,000 NophmOlone GOAD 40,51 :OA1 4 100 100 4 .10,000 PhemnOeem :0.40 451 <0,41 700 1,000 100 100 10,000 <Q40 40.51 40.91 700 Too 700 700 10.000 v.l.al. Gr anle cwm Duna. Dc. A,-[.-- 2.1 <0.069 40.051 7 60 6D 3 10,000 lon•ArN maUV ether m.OO3 <0.003 .0.03 - - - - - Bemone <o.003 -0,003 4.013 10 40 40 10 2,000 Biomobom.n. :0'003 0.0 :03 <0.G03 - - - too - 8romowelamoMw. 0.00] 40.007 -0.007 - - - - - Bromoditblormotheno '0403 :o,007 -0.003 CA 20 20 0.1 900 Brorn-f n 4.003 :0.003 <OA13 0.1 20 100 0.1 7,000 Bromomomano .0.005 4.007 'a.3S 10 7 s0 3 7.000 2.8u lra,(MEK) 0.61 :0.029 10.050 04 40 40 0] 10,000 o.8Wb.mem :OA 03 4p1001 10.007 - - - - - sm•BurNbom.no <p,003 4.003 .0.003 - - - - - Ied-BUrAba...a 40.001 :0 D3 -0.003 - - - - CeNandsu110o 40.055 40.069 -0.051 - - - 100 - ColbwnlebocNadda :0.00] <oDD7 :0.007 1 4 7 1 400 CWeb-., / 0.007 40.001 40.007 9 90 40 a 10.000 CNuaathene '0.005 -OA07 40.005 - - - 100 - CNu41arm '01007 40.003 .0.003 0.1 10 20D 0.1 5,000 CNUO..Mo. 44005 40,007 :0,005 - - - 100 - 2-CNoratolo- <O,oo1 :0.003 -p.003 - - - - - 4CNonoidmno 40,007 <p,003 'O. DO - - - - - 1.2-Dibmmu3.wempropem 40.007 40,00] 40,003 - - - 10 - Dibmmowarom.lhano '0403 :0.007 40.00] 0.09 10 10 0.00 700 Oibramameth.ne :0.007 4.007 10,007 - - - 500 - 1,2 Dlbtomoethene 40.003 4.007 <OA3 - - - - - 1,7•Dichimob.men. 40.003 40.003 40401 100 100 100 10D 5,000 ,.3-' N-be- -0.001 :0,03 :0.007 100 1GO 100 100 5,000 1,401chl. ob.- 0.003 40.003 40.007 2 40 40 2 2.000 11 DicNOraelnen. .0.003 :0.003 40.003 3 100 100 3 5.000 1,2 Diwoloathon. 40.007 <0.003 40.001 0.05 0,2 10 0.D5 600 I, MN.-Mone 4.03 :0.001 40.007 0.7 0.1 2 D.1 90 tisDk olo.man. '0.00] 0.00] 40AO3 - - - - - U-1.2-Diwemeth ona <O,OD7 4 500 500 4 10000 o-Didhi Mon. 4.013 4.007 4.007 - - - - - DidkrodAUolomahme 4.007 <o.O03 4.013 - - - - - I.2-DIcNOraprop.nO .0.003 40.003 40.003 0,1 02 a 0.1 400 1,30IcNerop,.p.n. 4.007 40.003 -0.007 0.01 0.1 7 Soo - 2.7-Dichloropropen. :0.003 10.003 .0103 - - - - - Diworeliropena 0,001 40.003 <0.003 - - - - - 1,3.Oiwaroplopone 4.007 0.D1 0.1 3 0.01 200 ds11DlWOlop4pono :0.007 -0.003 4.001 - - - V.ns1,3-Dlwaopopem -0.003 40.003 -0.003 - - - DI.W whor cDCD] cp.003 :0.003 - - - - - DlioWnoW odor 4.003 -0.003 4.003 - - - 1.4-Choma 4027 40.34 4016 Edlyb.Mo. 40.003 4.003 4.001 60 500 NO 90 10,000 EWona led•bulyi other 4.003 :0.003 4.003 - - - - - HemcNoiabumdi.ne 4,003 .0.OD3 40.003 3 3 5 3 400 2-Hir.nan. e0.072 , 10,029 4.020 - - - too - Bepn.prm.men. 40403 :403 4.003 - - - - - plsoproprkalu.no 40.003 :0.003 :0.003 - - - - - M.NoneW rid, 10.005 40.001 40,005 CA 100 100 0,1 7,000 4Matlp47-p.Nenone(h9BK) 4.022 4429 4.020 1 70 70 05 10,000 MobAt.bbr#...l 40.005 4,007 4.005 0,3 100 100 0.7 5,000 Nor, ran. 4.027 4.034 40.026 4 100 100 4 10,000 nProprtbOmene 40.001 4413 10.01] - - - - - St7lane 4 0.00] 4CAM 40.003 2 20 2D 2 1,000 1,1,1,2•TOtraworoothone 10,003 40403 40.00] 0.9 0.5 9 OA 200 1.1.2,7•TeboeNmomhao. 04003 10.00] 40.00] 0.02 0.2 OS 0.02 20 T.-WoneNeno :0.003 4000] c0A93 0.5 20 20 1 1,000 T.alydrol n. 40.005 4.007 40.005 - - - - - Twm. 4.003 40.00] <p,003 90 500 500 90 10,000 U2 3-Tdw.rON- 40.007 4.001 :0.013 - - - - - 1,2,4Tdwarab.mena 4.003 40.003 40.007 100 409 400 too 10,000 1,1,1•Tdwolaelhom 4Ao] 4407 40,007 30 too 100 30 5.000 1,1.2-TdcNamaman. 40.007 40.00] 40.00] 0] 7 7 D] 190 TriMloroam... 4,003 :0.003 40403 0.9 20 70 OA SAGS Tnwmolmn-ou han. 4.001 <D.003 4.003 - - - - - 1,7,3-Td[Narogop.n. 4.007 1.113 4.001 - - - 100 - :'3.5-na 40.003 4413 4103 - - - 10 - 1.2.4Tdm.0Alb.men. 4.03 4.03 40.003 - - - I.ODG - virtylwadd. 4AO5 4.007 40.005 03 0.3 DD 07 20 o-XNano 03 4.003 :0.003 soo Soo sea 500 10.000 136 X ands 4.007 :0,007 0407 SOD 500 50o 500 10400 l I _..1 Melissa Parsons Tighe and Bond, Inc. r 53 Southampton Road } Westfield, MA 01085 l ~I L-. 12/29/2003 Report Number: 212086 I I:. Dear Melissa Parsons, STL STL Westfield 53 Southampton Road Westfield, MA 01085 Tel: 413 572 4000 Fax: 413 572 3707 www.stl-inc.com The analysis of your sample(s) submitted on 12/17/2003 is now complete and the appropriate analytical report is enclosed. ? The samples were prepared and analyzed according to established:! methodologies and protocols. All holding times were met for the methods performed on these samples, unless otherwise noted in the report's case narrative. li If you have any questions regarding this report, please contact r_ your project manager. If you have questions, concerns or comments ii regarding our service, please do not hesitate to contact me directly. l Thank you for selecting STL-Westfield, and we look forward to working `t with you on future projects. i Steven C. Hartmann 'j. Laboratory Director `-J STL Westfield r~ Technical Review: O r- I ~.1 I Total number of pages in this report: Severn Trent Laboratories, Inc. i 1 r I i 1 r' i I i ~ 'f i I f~ I. _ Signature Name: Anne M. Fuller Title: Project Manager- j i_ E-Mail: afuller@s.tl-inc.com I: ® ST T R D NY DOH 10843 j L CTDPH PH 0494 494 NH DES 25390 53901-A VT DEC_ WSD. NELAP NY10843 (2 Dat Westfield Executive Park 53 Southampton. Road Westfield, MA 01085 PHONE: 413-572=4000 FAX..: 413-572-3707 STL Westfield 53 Southampton Rd. Westfield, MA 0108$ Tel: (413) 572-4000 Fax* (413) 5723707 STL Billerica 149 Rangeway Rd. N. Billerica, MA 01862 Tel: (978) 667-1400 Fax: (978) 667-7871 MADEP MCP Analytical Method Report Certification Form Laboratory Name: Severn Trent Laboratory (STL) Westfield Project 212086 Project Location: Quarry Alt. - phase I MADEP RTN': This form-provides certifications for the following data set:[list Laboratory Sample ID Number(s)] 212086-1-4 Sample Matrices: Groundwater Soil/Sediment Drinking Water bther: M~CIP4 t '1, S , 8'46 8260B(x) 8151A ( ) 8330( ) 6010E O 7470A/lA ( ) Other( M~f od Used 8270C( 8081A ( ) VPH O 6020 ( ) 9014M ( ) s spe~ifed in MADEP 8082( ) 8021 B ( ) EPH (x) 7000S ( ) 7196A ( ) `~.ompendillrn of d" 1 List Release Tracking Number (RTN), if known Ate h t. ~Jeth~ds 2 M - SW-846 Method 9014 or MADEP Physiologically Available Cyanide (PAC) Method (check k aJl t lat a 3S - SW-846 Methods 7000 Series List individual method and analyte. An affirmative response to questions A, B, C and D is required for "Presumptive Certainty" status A Were all samples received by the laboratory in a condition consistent.with KTTsD No' that described on the Chain-of-Custody documentation for the data set? Were all QA/QC procedures required for the specified analytical method(s) B included in this report followed, including the requirement to note and No' discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? Does the analytical data included in this report meet all the requirements C for "Presumptive Certainty", as described in Section 2.0 of the MADEP N/A No' document CAM VII A, " Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data"? VPH and EPH methods only: Was the VPH or EPH method run without D significant modifications, as specified in Section 11.37 N/A No' A response to questions E and F below is required for "Presumptive Certainty" status E Were all QC performance standards and recommendations for the Yes No' specified methods achieved? F Were results for all analyte-list compounds/elements for the specified es N/A No' method(s) reported? ' All Negative responses must be addressed in an attached Environmental Laboratory case narrative. I, the undersigned, attest under the pains and- penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical reportis, to the best of my knowledge and belief, accurate and complete. Signature: A~ IIIAI- Position: Laboratory Director Printed Name: Steven C. Hartmann Date: l02 a9 0 3 MADEP MA014 RIDOH57 NY DOH 10843 ® S T .L L CTDPH 0494 NH DES 253901-A VT DECWSD NELAP NY10843 STL Westfield STL Billerica 53 Southampton Rd, 149 Rangeway Rd Westrield, MA 01085 C N.Billerica, MA 01862 CACy a Tel:(413)572.4000 Tel:(978)667:1400 lay-o- Fax:(413)572-3707 Fax:(978)667-7871 MCP CASE NARRATIVE Client: Tighe & Bond, Inc. Report Number: 212086 - , This case narrative is in the form of an exception report, where only the anomalies related to this report, method specific performance and/or QA/QC issues are discussed. If there are no issues to report, this narrative will include a r statement that documents that there are no relevant data issues as stipulated in the-MCP reporting requirements. All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below. The project samples were received on 12/17/03; the samples arrived in good condition, properly preserved and on ice. SW846 8260B For MCP method SW846 8260B, the LCS that was analyzed with this analytical batch was prepared from the same source standards that were used to create the calibration curve. An Initial Calibration Verification (ICV) standard was originally analyzed to validate the calibration curve and met method criteria. Use of sodium bisulfate in the low-level solid preservation method for samples with high organic matter or humic material content has been known to result in the presence of acetone and methyl ethyl ketone (MEK) at potentially significant concentrations in samples. (Reference: Method SW846 5035). . t A LCS/LCSD was performed on this job for precision and accuracy. measurements, instead of an MS/MSD. The LCS/LCSD recovered within MCP control criteria. There were no additional QA/QC deviations or issues reported for this method. MADEP EPH A LCS/LCSD was performed on this job for precision and accuracy measurements, instead of an MS/MSD. The LCS/LCSD recovered within MCP control criteria. I! The performance of C9 recovery in the LCS and LCSD is low and outside of method control limits for this analysis. In STL Westfield's experience, the C9 control limits should be considered advisory for this method. The RSD for Chrysene.recovered' high (29.5) and outside method control limits (<25) for the continuing calibration verification. This compound was riot detected in any sample associated with this job. There were no additional QA/QC deviations or issues reported for this method. I VPH/EPH CERTIFICATION Job Number: 212086 l The samples in this data set were analyzed by the MADEP VPH and/or EPH Methods (Revision 0 January 1998). The following information is provided relative to sample receipt, QA/QC procedures and method modifications. Sample Receipt and Analysis: -,I Sample containers were received in -satisfactory condition: • Samples were received at 4±2°C or on ice. i Aqueous samples were.preserved properly. '.I _l • VPH soil samples were properly preserved with methanol (1:1 ± 25%; covered soil). EPH water and soil samples are prepared for analysis by liquid-liquid and sonication and/or soxhlet _ extraction, respectively. Reporting Conventions: The Unadjusted C11-1322 aromatic range excludes concentrations of any surrogate(s) and/or internal standards eluting in that range. j C11-C22 aromatic hydrocarbons exclude the concentration of target PAH analytes. • Unadjusted VPH ranges exclude the concentrations of any surrogate(s) and/or internal standards eluting in that range. I~ • C5-C8 aliphatic hydrocarbons exclude the concentrations of target analytes eluting in that range. 1 C9-C12 aliphatic hydrocarbons exclude the concentration of target analytes eluting in that range and the concentration of C9-C10 aromatic hydrocarbons. i_. QA/QC Procedures: • All QA/QC procedures required by the EPHNPH Methods were followed. All Method t _J performance/acceptance standards were achieved, unless noted in the case narrative, with the _ following exception. In the EPH analysis the recovery performance for the lowest molecular weight j aliphatic marker, (C9), is considered advisory. • The method specified surrogate standard recovery ranges are 40%-140% (EPH) and 70%-130% (VPH). Method Modifications: "I • Sample and standard chromatograms are corrected for column bleed and a single component r t contaminant from the SPE cartridge. Certification: The signature on the report cover page serves as the attestation for the method specified certification: I attest under the pains of perjury that, based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my I knowledge and'belief, accurate and complete. 1 > Q:\QAQC\wrtp\EPHVPH Cert\Cert Temp.doc Page 1 of 1 12/29103, 9:07 AM ii i l STL Westfield STL Billerica ` MADEP MA014 53 Southampton Rd. 149 Rangeway Rd. ST L Westfield, MA 01085 N. Billerica, MP 01862 IDOH67 NY DOH 10843 R k oR Tel: (413) 572-4000 Tel: (978) 667.1400 1 1 L CTDPH 0494 NH DES 2539 Fax7(413) 572.3707. Fax: (976) 667.7871 VT DECWSD SD ® , NELAP NY10843 A 1 J i STL WESTFIELD DATA REPORTING QUALIFIERS AND TERMINOLOGY A number of data qualifiers are widely used within the environmental testing industry and may be utilized in our data reports. The majority of the qualifiers have evolved from the EPA Contract Laboratory Program (CLP). Report Comments: ALL pages of this-report are integral parts of the analytical data. Therefore, this report should be reproduced only in its entirety. Soil, sediment and sludge sample results are reported on a "dry weight" basis. Reporting limits are adjusted for sample size used, dilutions and moisture content,' if applicable. The test results for the noted analytical method(s) meet the requirements of NELAC. Lab Cert.ID# 10843. STL-Westfield Certifications:.MADEP MA014, CT DPH 0494, NH DES, 253901-A, NY DOH 10843, RI DOH 57, VT DECWSD~:- According to 40CFR Part 136.3, pH, Total Residual Chlorine and Dissolved Oxygen analyses are to be performed immediately after aqueous sample collection. When these parameters are not indicated as field analyses, they were not analyzed immediately, but as soon as possible on laboratory receipt. Analytical result(s) reported as 'IND", indicates that the analyte was analyzed for but "not detected." Analytical result(s) reported as IITNTCII indicates that the microbiological test was "too numerous to count." Glossary of Qualifiers: I l Inorganic Qualifiers (Q-column): U Indicates that the analyte was analyzed for but not detected. E Indicates an estimated value due to the presence of interference. When applied to GFAA analysis', indicates the one-point method of addition recovered between 40-85 percent. B Indicates an estimated result value. The result was measured between the reporting limit and the method detection limit (MDL). Organic Qualifiers (Q-column): U Indicates that the compound was analyzed for but not detected. J Indicates an estimated result value. This qualifier is used when mass spectral data indicated the presence of a compound that. meets the identification criteria and the result is less than the specified quantitation limit, but greater than the method detection limit (MDL). B Indicates that the compound was found. in both the sample and its associated laboratory blank. Indicates possible/probable blank contamination and warns the data user to exercise caution when applying the results to this compound. D Indicates all compounds identified in an analysis at a secondary dilution factor. E Indicates that the compound in an analysis has exceeded the instrument Linear calibration range. Glossary of Terms: Surrogates (Surrogate Standards): An organic compound, which is similar to the target analyte(s) in chemical composition and behavior in the analytical process, but are not normally found in environmental samples. For semi-volatiLes and pesticides/Arochlors, surrogate compounds are added to every blank, sample, matrix spike, matrix spiked duplicate, matrix spike blank (LCS), and standard. These compounds are used to evaluate analytical efficiency by measuring recovery. Poor surrogate recovery may indicate a problem with the sample composition. STL Westfield STL Billerica ® MADEP MA014 53 Southampton Rd. 149 Rangeway Rd. STL RIDOH57 NY DOH 10843 Westfield, MA 0108¢ N. Billerica, MA 01862 CTDPH 0494 NH DES 253901-A 'NTel: (413) 57213000 Tel: (978) 667.1400 VT DECWSD. NELAP NY10843 Faxr (413) 5723707 Fax: (978) 667-7871 Internal Standard: An organic compound, which is similar to the target analytes) in chemical composition and behavior in the analytical process. For GC/MS semi -volatiles and volatiles, internal standards are added to every blank, sample, matrix spike, matrix spike duplicate, matrix spike blank (LCS), and standard. Internal standard responses outside of established limits will adversely affect the quantitation and final concentration of target compounds. Matrix Spike'(MS): An aliquot of a sample (water or soil) fortified (spiked) with known quantities of specific compounds (target analytes) and subjected to the entire analytical procedure in order to indicate the appropriateness of the method for matrix interference by measuring recovery. The spiking occurs prior to sample preparation and analysis. Poor spike recovery may indicate a problem with the sample composition. ~ -1 1 Laboratory Control Sample (LCS): An aliquot of analyte-free reagent water or sand fortifed (spiked) with known quantities of specific compounds (target analytes) and subjected to the entire analytical procedure in order to indicate the appropriateness of the method efficiency. Blank: An artificial sample of analyte-free water or solvent, designed to monitor the introduction of contaminates into the analytical process. Method Dectection•Limit (MDL): The minimum concentration of an analyte or compound that can be measured and reported with 99% confidence that the result concentration is greater than zero. Petroleum Hydrocarbon Comments: The following comments are specific to Diesel Range Organics (DRO), by GC/FID: Results for DRO are based on chromatographabLe portions of the petroleum product. The Carbon Range refers to the approximate chromatographic region covered by the specified petroleum product in straight-chain carbon units between C9-C36. Quantitation is based on the average response factors for a series of hydrocarbons standards. The sample result from the DRO fraction is independent of the target compound assignment. Samples yielding chromatographic patterns that do not agree with any.of the method targets are reported as "unmatched". page STL Westfield STL Billerica STL MADEP MA014 RIDOH57 NY DOH 19843 53 Southampton Rd. Westfield, MA 01 1085 Tel: (413) 572-4000 149 R, y Rd. N. Billerica, MA 01 01862 Tel: (978) 667.1400 CTDPH 0494 ® NH DES 253901-A VT DECWSD NELAP NY10843 <dl kG 4<.!: Faxi (413) 572.3707 Fax: (978) 667-7871 :...::............................................:..................:.............:...:......:.::.......S . A.. M.:.F.. L...E....::: t ::N:.:{ .:0...: .ix Job Number.: 212086 Project Number.........: 20001962 Customer...: Tighe and Bond, Inc. Customer Project ID....: N523 Attn.......: Melissa Parsons Project Description....: N523 . 1 ar.•. Y : •r:z>s>s»»»::>::::»::>:«::.::>srs......CUStfl er ::>i ;::.::;;:Sam '>Q:<te>; a • `:>''sE>€'.€:T i:irie':>>:'•»#`> < ::>:`:`Qa T. . t.m...::...:.... :Sam e...I.R ? :::•::::::::::::::::.S ; .......................................am .1.e.13........................ ......................................................1 ..............................P................................... •::tx::>::::> M.... r..:....... :;<::..S m .l......... :..::.........I?.............. m ..............A............... ec....... ..et....... . 212086-1 S-1 S0i4 12/16/2003 14:20 12/17/2003 11:55_ 212086-2 S-2 Soil 12/16/2003 14:53 12/17/2003 11:55 212086-3 S-3 SoiL 12/16/2003 15:40 12/17/2003 11:55 212086-4 Trip Blank Methanol 12/16/2003 12:00 12/17/2003 11:55 page 5 STL Westfield STL Billerica MADEP MA014 53 Southampton Rd. 149 Rangeway.Rd. STL RIDOH57 NY DOH 10843 M ACOp"o, .t , Westfield, MA 01086 Tel: (413) 5724000 N. Billerica, MA 01862 Tel: (978) 667-1400 CTDPH 0494 NH DES 253901-A n~= Fax: (413) 572.3707 978 667 7871 F VT DECWSD NELAP NY10843 ;j , ) . ax: ( L A B 0 R A T 0 R Y_ T E S T R E S U L T S Job Number: 212086 Date: 12/29/2003 .and::'•:B.on . In. P 0 ECT#>E'Nfi232€>:<:>:?>'>?;:>`<:<::#: , . G.U.S70MEli.....T. ~.9 r...:.........:...:.................:..::.....:.:..::.::::::.:..:.....::..:..........::.:.:...::...................:......................:..:::::7..: N.: Me.l:l:ssa.: P Customer Sample ID: S-1 Laboratory Sample ID: 212086-1 Date Sampled......: 12/16/2003 Date Received.......: 12/17/2003 Time Sampled....... 14:20 Time Received........ 11:55 Sample Matrix.....: Soil :;:::~z::<::::»:: »::::»>"s<::::;:::::>;::>:: ;::>;;::::.PARAMETERf..T.ES7.;D(SCRIPTIOtr............................:.. . .:SU:::.`:>: ::SAMP.LE..R.. . L.T..... E .4 P > .G :I .RE...QIrT.LN ...LIM..T. ;<:S'::;::><:: .....UNIT......... DATE .TECH: . SW846 5030 Met Sample Preparation Complete Text 12/23/03 caox % Solids 160.3 % Solids 79.9 0.1 % 12/18/03 grb MADEP EPH MCP SemivolatiLe Organics Acenaphthene* ND U 0.40 mg/Kg 12/23/03 fwd Acenaphthylene* ND U 0.40 mg/Kg 12/23/03 fwd Anthracene* ND U 0.40 mg/Kg 12/23/03 fwd Benzo(a)anthracene* ND U 0.40 mg/Kg 12/23/03 fwd Benzo(a)pyrene* ND U 0.40 mg/Kg,,' 12/23/03 fwd Benzo(b)fluoranthene* ND U 0.40 mg/Kg' 12/23/03 fwd Benzo(ghi)perylene* ND U 0.40 mg/Kg, 12/23/03 fwd Benzo(k)fluoranthene* ND U 0.40 mg/Kg 12/23/03 fwd Chrysene* ND U 0.40 mg/Kg 12/23/03 fwd Dibenzo(a,h)anthracene* ND U 0.40 mg/Kg 12/23/03 fwd FLuoranthene* ND U 0.40 mg/Kg 12/23/03 fwd FLuorene*. ND U 0.40 mg/Kg 12/23/03 fwd Indeno(1,2,3-cd)pyrene* ND U 0.40 mg/Kg 12/23/03 fwd 2-Methylnaphthalene* ND U 0.40 mg/Kg 12/23/03 fwd Naphthalene* ND U 0.40 mg/Kg 12/23/03 fwd Phenanthrene* ND U 0.40 mg/Kg 12/23/03 fwd Pyrene* ND U 0.40 mg/Kg 12/23/03 fwd C9-C18 Aliphatics* 13.7 4.0 mg/Kg 12/23/03 fwd C11-C22 Aromatics* 175, 4.0 mg/Kg 12/23/03 fwd C19-C36 Aliphatics* 601 4.0 mg/Kg 12/23/03 fwd Unadjusted C11-C22 Aromatics* 175 4.0 mg/Kg 12/23/03 fwd EPH Concentration (Total)* 789 4.0 mg/Kg 12/23/03 fwd SW8468260B MCP VoLatile Organics Dichlorodifluoromethane (Freon 12)* ND U 3 ug/Kg 12/23/03 gib Chloromethane* ND U 5 ug/Kg 12/23/03 gjb Vinyl chloride*- NO U 5 ug/Kg 12/23/03 gjb Bromomethane* ND U 5 ug/Kg 12/23/03 gib Chloroethane* ND U 5 ug/Kg 12/23/03 gib Trichlorofluoromethane (Freon 11)* ND U 3 ug/Kg 12/23/03 gib 1,1-Dichloroethene* NO U 3 ug/Kg 12/23/03 gib cis-Dichloroethene* NO U 3 ug/Kg 12/23/03 gib trans-Dichloroethene* ND U 3 ug/Kg 12/23/03 gib 1,2-Dibromo-3-chLoropropane* ND U 3 ug/Kg 12/23/03 gib Carbon disulfide* ND U 55 ug/Kg 12/23/03 gib Acetone* 2100 55 ug%Kg 12/23/03 gjb Methylene chloride* ND U 5 ug/Kg 12/23/03 gjb Methyl-tert-butyl-ether (MTBE)* ND U 5 ug/Kg 12/23/03 gjb 1,1-Dichloroethane* ND U 3 ug/Kg 12/23/03 gib 2,2-Dichloropropane* ND U 3 ug/Kg 12/23/03 gjb 2-Butanone (MEW 510 22 ug/Kg 12/23/03 gjb Bromochloromethane* ND U 3 ug/Kg 12/23/03 gjb Tetrahydrofuran (THF)* ND U 5 ug/Kg 12/23/03 gib * In Description = Dry Wgt. ~ TT ® RIDO7 NY DOH 10843 ADEP S 1 JJ C T PH 049414 NH DES 253901-A ® VT DECWSD NELAP NY10843 Page 4 STL Westfield 53 Southampton Rd. ° ACCp4°,N cam ° Westfield, MA 0108$ 413 l 572 4000 T . i ) e : ( - Fax: (413) 572-3707 STL Billerica 149 Rangeway Rd. N. Billerica, MA 01862 Tel: (978) 667-1400 Fax: (978) 667-7871 r-I I L _ L A B O R A T O R Y T E S T R E S U L T S - Date: 12/29/2003 Job Number: 212086 Asa ar : I . c ::»>:<;::;:::;::>::>:;::<e:»>:>:::<>::;:. OJl T:: N23>:::>;::::<>:>::>'•> Me. A. n5.:.:':>:::;>`>>:>:>::>:::.::<:::::::><::::: CU.ST.OMER....T~ he..and..Bond G ••:::::::...::.:.:::....P.~ 9 Customer Sample ID: S-1 Laboratory Sample ID: 212086-1 Date Sampled......: 12/16/2003 Date Received.......: 12/17/2003 Time Sampled....... 14:20 Time Received........ 11:55 Sample Matrix.....: Soil NIE.T..HQ4::::.: ......:.......P.ARAM..tER..T> 5.7...RE..CR.IP.7Z.O.N.................:.::::.....:: :.::.MP..:......:......:.:....::. . aE..ORT:IEN.G:;L;:I:M:I7; X X `...U. IT... 7 : OA .E... ' i CH. ..:T:E.. . Chloroform* ND U 3 ug/Kg 12/23/03 gjb 1,1,1-Trichloroethane* ND U 3 ug/Kg 12/23/03 gjb 1,1-Dichloropropene* NO U 3 ug/Kg 12/23/03 gjb Carbon tetrachloride* NO U 3 ug/Kg 12/23/03 gjb Benzene* ND U 3 ug/Kg 12/23/03 gib 1,2-Dichloroethane* ND U 3 ug/Kg 12/23/03 gib Trichloroethene (TCE)* NO U 3 ug/Kg 12/23/03 gjb 1,2-Dichloropropane* NO U 3 ug/Kg 12/23/03 gjb Dibromomethane* ND U 3 ug/Kg 12/23/03 gjb Bromodichloromethane* ND U 3 ug/Kg 12/23/03 gib cis-1,3-Dichloropropene* ND U 3 ug/Kg::. 12/23103 gjb 4-MethyL-2-pentanone (MIBK)* ND U 22 ug/Kg 12/23/03 gjb Toluene* NO U 3 ug/Kg 12/23/03 gib trans-1,3-Dichloropropene* ND U 3 ug/Kg 12/23/03 gib 1,1,2-Trichloroethane* ND U 3 ug/Kg 12/23/03 gib Tetr.achloroethene*. NO U 3 ug/Kg 12/23/03 gib 1,3-Dichloropropane* NO U 3 ug/Kg 12/23/03 gib 2-Hexanone (MNBK)* NO U 22 ug/Kg 12/23/03 gib Dibromochloromethane* NO. U 3 ug/Kg 12/23/03 gib 1,2-Dibromoethane (EDB)* NO U 3 ug/Kg. 12/23/03 gib Chlorobenzene*. NO U 3 ug/Kg 12/'23/03 gib 1,1,1,2-Tetrachloroethane* ND U 3 ug/Kg 12/23/03 gjb Ethylbenzene* NO U 3 ug/Kg 12/23/03 gib m&p-Xylenes* ND U 3 ug/Kg 12/23/03 gjb o-XyLene* ND U. 3 ug/Kg 12/23/03 gjb Styrene* NO U 3 ug/Kg 12/23/03 gjb Bromoform* NO U 3 ug/Kg 12/23/03 gib Isopropylbenzene* ND U 3 ug/Kg 12/23/03 gib Bromobenzene* ND U 3 ug/Kg 12/23/03 gjb 1,1,2,2-Tetrachloroethane* NO U 3 ug/Kg 12/23/03 gjb 1,2,3-Trichloropropane* NO U 3 ug/Kg 12/23/03 gjb n-Propylbenzene* NO U 3 ug/Kg 12/23/03 gib 2-Chlorotoluene* ND U 3 ug/Kg 12/23/03 gjb 1,3,5-Trimethylbenzene* ND U 3 ug/Kg 12/23/03 gib 4-Chlorotoluene* NO U 3 ug/Kg 12/23/03 gib tent-Butylbenzene* ND U 3 ug/Kg 12/23/03 gjb 1,2,4-Trimethylbenzene* ND U 3 ug/Kg 12/23/03 gib sec-Butylbenzene* NO U 3 ug/Kg 12/23/03 gib 1,3-Dichlorobenzene* NO U 3 ug/Kg 12/23/03 gjb p-IsopropyLtoluene* ND U 3 ug/Kg 12/23/03 gjb 1,4-Dichlorobenzene* ND U 3 ug/Kg 12/23/03 gjb n-Butylbenzene* ND U 3 ug/Kg 12/23/03 gib 1,2-Dichlorobenzene* ND U 3 ug/Kg 12/23/03 gjb 1,2,4-Trichlorobenzene* ND U 3 ug/Kg 12/23/03 gib Hexachlorobutadiene* NO U 3 ug/Kg 12/23/03 gjb Naphthalene* ND U 27 ug/Kg 12/23/03 gib 1,2,3-Trichlorobenzene* ND U 3 ug/Kg 12/23/03 gjb Diethyl ether (Ether)* ND U 3 ug/Kg 12/23/03 gib DiisopropyL ether (DIPE)* NO U 3 ug/Kg 12/23/03 gjb * In Description = Dry Wgt. STL MADEP I4 CTDPH 0494 VTDECWSD Page 5 `~O ,n accc o~ NY DOH 10843 NH DES 263901-A c NELAP NY10843 Q. STL Westfield 53 Southampton Rd. Westfield, MA 01085 Tel: (413) 5724000 Fax! (413) 572-3707 STL Billerica 149 Rangeway Rd. N Billerica, MA 01862 Tel- (978) 667-1400 Fax: (978)667.7871 L A B 0 R A T 0 R Y_ T E S T R E S U L T S Job Number: 212086 Date: 12/29/2003 C E ;.;:•7~. he.::and:::B.ohd: ::>:•Inc;.»:::>:>::::;::>:.> .....::.:::.::::.................Ixl?OdECT....NZ sa :P. Customer Sample ID: S-1• Laboratory Sample ID: 212086-1. Date Sampled......: 12/16/2003 Date Received.......: 12/17/2003 Time Sampled....... 14:20 Time Received........ 11:55 Sample Matrix.....: Soil : MET.KpR T. ET ::>:z::` ii':'>:Y•`i i:i:#, c: PARAM7 7ERf.•..T.ES.T:.;:R.E:SCR.I PT Z pN . ShMF..: >RE SULT:>:; ::4.. :I 1:: REP.ORT..NG...L.LM. T. <:< '.U ' ..NITS..... D E A7 TE C .....H. 1,4-Dioxane* ND U 270 ug/Kg 12/23/03 gib Ethylene tert-butyl ether (ETBE)* ND U 3 ug/Kg 12/23/03 gib tert-Amyl methyl ether (TAME)* ND U 3 ug/Kg 12/23/03 gib * In Description = Dry Wgt. CTY MADEP MA014 RIDOH57 J 1 L CTDPH 0494 i VT DECWSD NY DOH 10843 ° ~CCpgO+ NH DES 253901-A NELAP NY10843 STL Westfield 53 Southampton Rd. Westfield, MA 01085 Tel: (413)672.4000 Fax! (413) 572-3707 STL Billerica 149 Rangeway Rd. N. Billerica, MA 01862 Tel: (978) 667-1400 Fax: (978)667-7871 Page 6 L A B 0 R A T 0 R Y_ T E S T R E S U L T S Job Number: 212086 Date: 12/29/2003 • ,..,;>:»>:<:>:::<»:«<:: ::>:<.;>s::>::>:>:rr:a::::<::r>:>:>::«;:»:> >T :'»:'.~la:a'a<P"arson CLJ _..T.i. he:.and:.B.o.nd. •::.I.nc.. .....................:...:...:..::::.:.:.::.....P.RO ]I C.T....N5.23...........:..::::.:......:::::::::::::::::::::::::::::::::. pT..:N:::1..:.:.:....::..:...::.:.......:............:.................. Customer Sample ID: S-2 Laboratory Sample ID: 212086-2 Date Sampled......: 12/16/2003 Date Received.......: 12/17/2003 Time Sampled....... 14:53 Time Received........ 11:55 Sample Matrix.....: Soil i:: ; . :;a:•:: T.SST :•s:;:;;.;:.;:.;>:•..;;;::::;;;:::;;:. .......i'.EZ:E.:i%.''..... ..S' L': i : RO : I G DA E%-,--. C> .....H. SW846 5030 Met Sample Preparation Complete Text 12/23/03 caox % Solids 160.3 % Solids 63.5 0.1 % 12/18/03 grb MADEP EPH MCP Semivolatile Organics Acenaphthene* ND U 0.51 mg/Kg 12/24/03 fwd Acenaphthylene* ND U 0.51 mg/Kg 12/24/03 fwd Anthracene* ND U 0.51 mg/Kg 12/24/03 fwd Benzo(a)anthracene* ND U 0.51 mg/Kg , 12/24/03 fwd Senzo(a)pyrene* ND U' 0.51 mg/Kg.- 12/24/03 fwd Benzo(b)fluoranthene* ND U 0.51 mg/Kg 12/24/03 fwd Benzo(ghi)perylene* ND U 0.51 mg/Kg 12/24/03 fwd Benzo(k)fLuoranthene* ND U 0.51 mg/Kg 12/24/03 fwd Chrysene* ND U 0.51 mg/Kg 12/24/03 fwd Dibenzo(a,h)anthracene* ND U 0.51 mg/Kg 12/24/03 fwd' Fluoranthene* ND U 0.51 mg/Kg 12/24/03 fwd Fluorene* ND U 0.51 mg/Kg 12/24/03 fwd Indeno(1,2,3-cd)pyrene* ND U 0.51 mg/Kg 12/24/03 fwd 2-Methylnaphthalene* ND U 0.51 mg/Kg 12/24/03 fwd Naphthalene* ND U 0.51 mg/Kg 12/24/03 fwd Phenanthrene* ND U 0.51 mg/Kg 12124103 fwd Pyrene* ND U 0.51 mg/Kg 12/24/03 fwd C9-C18 Aliphatics* 13.2 5.1 mg/Kg 12/24/03 fwd C11-C22 Aromatics* ND U 5.1 mg/Kg 12/24/03 fwd C19-C36 Aliphatics* 30.7 5.1 mg/Kg 12/24/03 fwd Unadjusted C11-C22 Aromatics* ND U 5.1 mg/Kg 12/24/03 fwd EPH Concentration (Total)* 43.9 5.1 mg/Kg 12/24/03 fwd SW84682608 MCP Volatile Organics Dichlorodifluoromethane (Freon 12)* ND U 3 ug/Kg 12/23/03 gjb Chloromethane* ND U 7 ug/Kg 12/23/03 gjb Vinyl chloride* ND U 7 ug/Kg 12/23/03 gjb Bromomethane* ND U 7' ug/Kg 12/23/03 gjb Chloroethane* ND U 7 ug/Kg 12/23/03 gjb Trichlorofluoromethane (Freon 11)* ND U 3 ug/Kg 12/23/03 gjb .1,1-Dichloroethene* ND U 3 ug/Kg 12/23/03 gjb cis-Dichloroethene* ND U 3 ug/Kg 12/23/03 gjb trans-Dichloroethene* ND U 3 ug/Kg 12/23/03 gjb 1,2-Dibromo-3-chloropropane* ND U .3 ug/Kg 12/23/03 gjb carbon disulfide* ND U 69 ug/Kg 12/23/03 gjb Acetone* ND U 69 ug/Kg 12/23/03 gjb Methylene chloride* ND U .7 ug/Kg 12/23/03 gib Methyl-tert-butyl-ether (MTBE)* ND U 7 ug/Kg 12/23/03 gib 1,1-Dichloroethane* ND U 3 ug/Kg 12/23/03 gjb 2,2-Dichloropropane* ND U 3 ug/Kg 12/23/03 gjb 2-Butanone NEW NO U . 28 ug/Kg 12/23/03 gjb Bromochloromethane* ND U 3 ug/Kg 12/23/03 gjb Tetrahydrofuran (THF)* ND U 7 ug/Kg 12/23/03 gjb * In Description = Dry Wgt. f ® MADEP MA014 RI 5 1 it ® f DPH 0494 J VT DECWSD Page 7 NY DOH 10843 NH DES 253901-A NELAPNY10843 art STL Westfield 53 Southampton Rd. Westfield, MA 01085 Tel: (413) 572-4000 Fax' (413)672.3707 SYL Billerica 149 Rangeway Rd. N Billerica MA 01862 Tel: (978) 667-1400 Fax: (978) 667-7871 (1 i~ I! . J L A B 0 R A T Job Number: 212086 Date: 12/29/2003 ':GU9TOMER< >T•:; glYe`a;'nd.:..:.. r:n:.;:;;;:•;:•;::•:::;:• Customer Sample ID: S-2 Laboratory SampLe ID: 212086-2 Date Sampled......: 12/16/2003 Date Received 12/17/2003 Time Sampled......: 14:53 Time Received 11:55 Sample Matrix.....: Soil »......:E>>P R..TE. 7 DE. . TE S S I M. A : Chloroform* 1,1,1-Trichloroethane* 1,1-Dichloropropene* Carbon tetrachloride* _ - - 12/23/03 - Benzene* ND U 3 ug/Kg 12/23/03 gib 1,2-Dichloroethane* ND U 3 ug/Kg 12/23/03 gib Trichloroethene (TCE)* ND U 3 ug/Kg 12/23/03 gjb 1,2-Dichloropropane* ND U 3 ug/Kg 12/23/03 gjb Dibromomethane* ND U 3 ug/Kg 12/23/03 gib Bromodichloromethane* ND U 3 ug/Kg 12/23/03 gjb cis-1,3-Dichloropropene* ND U 3 ug/Kg: 12/23/03 gib 4-Methyl-2-pentanone (MIBK)* ND U 28 ug/Kg 12/23/03 gjb Toluene* ND U 3 ug/Kg 12/23/03 gib trans-1,3-Dichloropropene* ND U 3 ug/Kg 12/23/03 gjb 1,1,2-Trichloroethane* ND U 3 ug/Kg 12/23/03 gib Tetrachloroethene* ND U 3 ug/Kg 12/23/03 gib 1,3-Dichloropropane* ND U 3 ug/Kg 12%23/03 gjb 2-Hexanone (MNBK)* ND U 28 ug/Kg 12/23/03 gib Dibromochloromethane* ND U 3 ug/Kg 12/23/03 gjb 1,2-Dibromoethane (EDB)* ND U 3 ug/Kg 12/23/03 gib Chlorobenzene* ND U 3 ug/Kg 12/23/03 gjb 1,1,1,2-Tetrachloroethane* ND U 3 ug/Kg 12/23/03 gjb Ethylbenzene* ND U 3 ug/Kg 12/23/03 gjb m&p-Xylenes* ND U 3 ug/Kg 12/23/03 gjb o-Xylene* ND U 3 ug/Kg 12/23/03 gib Styrene* ND U 3 ug/Kg 12/23/03 gjb Bromoform* ND U 3 ug/Kg 12/23/03 gib Isopropylbenzene* ND U 3 ug/Kg 12/23/03 gib Bromobenzene* ND U 3 ug/Kg 12/23/03 gjb 1,1,2,2-Tetrachloroethane* ND U .3 ug/Kg 12/23/03 gjb 1,2,3-Trichloropropane* ND U 3 ug/Kg 12/23/03 gib n-Propylbenzene* ND U 3 ug/Kg 12/23/03 gjb 2-Chlorotoluene* ND U 3 ug/Kg 12/23/03 gjb 1,3,5-Trimethylbenzene* ND U 3 ug/Kg 12/23/03 gib 4-Chlorotoluene* ND U 3 ug/Kg 12/23/03 gib tert-Butylbenzene* ND U 3 ug/Kg 12/23/03 gib 1,2,4-Trimethylbenzene* ND U 3 ug/Kg 12/23/03 gib sec-Butylbenzene* ND U 3 ug/Kg 12/23/03 gib 1,3-Dichlorobenzene* ND U 3 ug/Kg 12/23/03 gjb p-Isopropyltoluene* ND U 3 ug/Kg 12/23/03 gjb 1,4-Dichlorobenzene* ND U 3 ug/Kg 12/23/03 gjb n-Butylbenzene* ND U 3 ug/Kg 12/23/03 gjb 1,2-Dichlorobenzene* ND U 3 ug/Kg 12/23/03 gib 1,2,4-Trichlorobenzene* ND U 3 ug/Kg 12/23/03 gjb Hexachlorobutadiene* ND U 3 ug/Kg 12/23/03 gib Naphthalene* ND U 34 ug/Kg. 12/23/03 gjb 1,2,3-Trichlorobenzene* ND U 3 ug/Kg 12/23/03 gjb Diethyl ether (Ether)* ND U 3 ug/Kg 12/23/03 gjb Diisopropyl ether (DIPE)* ND U 3 ug/Kg 12/23/03 gjb * In Description =Dry Wgt. i MADEP MA014 r m~ STL RIDOH57 NY DOH 10843 ® CTDPH 0494 NH DES 253901-A VT DECWSD NELAP NY10843 Page 8 STL Westfield STL Billerica E " ""0q° e I, 1L Vl, 53 Southampton Rd. Westfield, MA 01085 Tel: (413) 5724000 Fax! (413)572.3707 149 Rangeway.Rd. N. Billerica, MA 01862 Tel: (978) 667-1400 Fax: (978)667.7871 LABO R A T O R Y _ •T E S T R E S U L T S Job Number: 212086 Date: 12/29/2003 end:>B.ohd...1.nc.. ................................................PR.QdEC.T... N: =i E c:' >:»'A7T M lissa ..N P?`i?5E'`'`"i%`i>~>'iEn`''.'•#3i£iii?iiii`?': o s ;...a rs..n . Customer Sample ID: S-2 Laboratory Sample ID: 212086-2 Date Sampled......: 12/16/2003 Date Received.......: 12/17/2003 Time Sampled....... 14:53 Time Received........ 11:55 Sample Matrix.....: Soil . :.::::S•::.. •.HOD TB.. T...M1 T :.:::::.:....:..:::...::::::PAR ..SRMF..L.E. .P .S..L.7...: 4 1,4-Dioxane* ND U 340 ug/Kg 12/23/03 gib Ethylene tert-butyL ether (ETBE)* ND U 3 ug/Kg 12/23/03 gib tert-AmyL methyl ether (TAME)* ND U 3 ug/Kg 12/23/03 gib * In Description = Dry Wgt. L_ MADEP MA014 r , STL RDOH5 ® CTDPH 0494 VT DECWSD Page 9 NY DOH 10843 NH DES 253901-A NELAP NY10843 STL Westfield 53 Southampton Rd. Westfield, MA 01065 Tel: (413) 572-4000 Fax' (413) 572.3707 STL Billerica 149 RangewayRd. N. Billerica, MA 01862 Tel: (978)667.1400 Fax: (978) 667-7871 I~ I~ L A B O R A T O R Y - T E S S T R E S U L T S Job Number: 212086 Date: 12129/2003 d :.:.I• PkOJE.GT...N5.23:...::::::::........................................A7:TN°:Mel:js::ns.:.:•:...:::.:•:•::.:•.:..::::.: CUSTOMS&::>;:T:a:9he..and..B.on ,nc.. Customer Sample ID: S-3 Laboratory Sample ID: 212086-3 Date Sampled......: 12/16/2003 Date Received.......: 12/17/2003 Time Sampled....... 15:40 Time Received........ 11:55 Sample Matrix.....: Soil : E.5 ....E .HOD ::::::::.:::::::::::E:.:i':?::'•E'•i«.<f:i:i?i::>::?:>: . PARAM.ETER/.tEST..pEsGK.I.P.7I0............,...:....:...::.::::: h1P.L..:..::................. SW846 5030 Met Sample Preparation Complete Text 12/23/03 caox % Solids 160.3 % Solids 77.7 0.1 % 12/18/03 grb MADEP EPH MCP SemivolatiLe Organics Acenaphthene* ND U 0.41 mg/Kg 12/24/03 fwd Acenaphthylene* ND U 0.41• mg/Kg 12/24/03 fwd Anthracene* ND U 0.41 mg/Kg 12/24/03 fwd Benzo(a)anthracene* ND U 0.41 mg/Kg 12/24/03 fwd Benzo(a)pyrene* ND U 0.41 mg/Kg 12/24/03 fwd Benzo(b)fluoranthene* ND U 0.41 mg/Kg 12/24/03 fwd Benzo(ghi)perylene* ND U 0.41 mg/Kg 12/24/03 fwd Benzo(k)fluoranthene* ND U 0.41 mg/Kg 12/24103 fwd Chrysene* ND U 0.41 mg/Kg 12/24/03 fwd Dibenzo(a,h)anthracene* ND U 0.41 mg/Kg 12/24/03 fwd Fluoranthene* ND U 0.41 mg/Kg 12/24/03 fwd FLuorene* ND U 0.41 mg/Kg 12/24/03 fwd Indeno(1,2,3-cd)pyrene* ND U 0.41 mg/Kg 12/24/03 fwd 2-Methylnaphthalene* ND U 0.41 mg/Kg 12/24/03 fwd Naphthalene* ND U 0.41 mg/Kg 12/24/03 fwd Phenanthrene* ND U 0.41 mg/Kg 12/24/03 fwd Pyrene* ND U 0.41 mg/Kg 12/24/03 fwd C9-C18 ALiphatics* ND U 4.1 mg/Kg 12/24/03 fwd C11-C22 Aromatics* ND U 4.1 mg/Kg 12/24/03 fwd C19-C36 ALiphatics* ND U 4.1 mg/Kg 12/24/03 fwd unadjusted C11-C22 Aromatics* ND U 4.1 mg/Kg 12/24/03 fwd EPH Concentration (Total)* NO U 4.1 mg/Kg 12/24/03 fwd SW8468260B MCP Volatile Organics Dichlorodifluoromethane (Freon 12)* ND U 3 ug/Kg 12/23/03 gib Chloromethane* ND U 5 ug/Kg 12/23/03 gib Vinyl chloride* ND U 5 ug/Kg 12/23/03 gib Bromomethane* ND U 5' ug/Kg 12/23/03 gib Chloroethene* NO U 5 ug/Kg 12/23/03 gib TrichLorofLuoromethane (Freon 11)* ND U 3 ug/Kg 12/23/03 gib 1, 1-Didhloroethene* ND U 3 ug/Kg 12/23/03 gib cis-Dichloroethene* ND U 3 ug/Kg 12/23/03 gib trans-Dichloroethene* NO U 3 ug/Kg 12/23/03 gib 1-,2-Dibromo-3-chloropropane* ND U 3 ug/Kg 12/23/03 gib Carbon disulfide* ND U 51 ug/Kg 12/23/03 gib Acetone* ND U 51 ug/Kg 12/23/03 gib Methylene chloride* ND U 5 ug/Kg 12/23/03 gib Methyl-tert-butyL-ether (MTBE)* ND U 5 ug/Kg 12/23/03 gib 1,1-Dichloroethane* ND U 3 ug/Kg 12/23/03 gib 2,2-Dichloropropane* ND U 3 ug/Kg 12/23/03 gib 2-Butanone (MEW ND U 20 ug/Kg 12/23/03 gib Bromochloromethane* ND U 3 ug/Kg 12/23/03 gjb Tetrahydrofuran (THF)* ND U 5 ug/Kg 12/23/03 gib * In Description = Dry Wgt. MADEP RDOH5MA014 US CTDPH 0494 S T L VT DECWSD Page 10 NY DOH 10843 NH DES 253901-A NELAP NY10843 STL Westfield 63 Southampton Rd. Westfield, MA 01085 Tel: (413) 572-4000 Fax:(413)572.3707 STL Billerica 149 Rangeway.Rd. N. Billerica, MA 01862 Tel: (978) 667-1400 Fax: (978) 667-7871 L A B 0 R A T 0 R Y_ T E S T R E S U L T S. Job Number: 212086 Date: 12/29/2003 T.. e>'i rih 3o d ,.I•ncs:::;::<:r;>::>:: PROJEG<':> 523::::`'.:: >>'z~»>>` >:<?`>>`•<>`> M C.USTOMER.......) gh n...:::..:.:.:..::.::..::::::::::::::::.:::::::.:..:::...:....:......:T..... N......::.::...........................................................................:):..:...:.:::...:,.:.:....::::,..::::..:.:..:.::::.:.:....::: Customer Sample ID: S-3 Laboratory Sample ID: 212086-3 Date Sampled......: 12/16/2003 Date Received.......: 12/17/2003 Time Sampled....... 15:40 Time Received........ 11:55 Sample Matrix.....: Soil. . 71 ST:.;.M~.T.NO . E:. :E <N: > : .............................PARAM..TER/.7 S..T...RE..GIt.I...II O MP..:....:.:.:?::.:: q. P..:RT.I.NG...I.:M.:.:. chloroform* ND U 3 ug/Kg 12/23/03 gib 1,1,1-Trichloroethane* ND U 3 ug/Kg 12/23/03 gib 1,1-Dichloropropene* ND U 3 ug/Kg 12/23/03 gib carbon tetrachloride* ND 0 3 ug/Kg 12/23/03 gib Benzene* ND U 3 ug/Kg 12/23/03 gib 1,2-Dichloroethane* ND U 3 ug/Kg 12/23/03 gib Trichloroethene (TCE)* ND U 3 ug/Kg 12/23/03 gib 1,2-DichLoropropane* ND U 3 ug/Kg 12/23/03 gib Dibromomethane* ND U 3 ug/Kg 12/23/03 gib Bromodichloromethane* ND U 3 ug/Kg 12/23/03 gib cis-1,3-Dichloropropene* ND U 3 ug/Kg 12/23/03 gib 4-Methyl-2-pentanone (MIBK)* ND U 20 ug/Kg 12/23/03 gjb Toluene* ND U 3 ug/Kg 12/23/03 gib trans-1,3-DichLoropropene* ND U 3 ug/Kg 12/23103 gjb 1,1,2-Trichloroethane* ND U 3 ug/Kg 12/23/03 gib Tetrachloroethene* ND U 3 ug/Kg 12/23/03 gjb 1,3-DichLoropropane* ND U 3 ug/Kg 12/23/03 gib 2-Hexanone (MNBK)* ND U 20 ug/Kg 12/23/03 gib Dibromochloromethane* ND U 3 ug/Kg 12/23/03 gib 1,2-Dibromoethane (EDB)* ND U. 3 ug/Kg 12/23/03 gib Chlorobenzene* ND U 3 ug/Kg 12/23103 gib 1,1,1,2-Tetrachloroethane* ND U 3 ug/Kg 12/23/03 gib Ethylbenzene* ND U 3 ug/Kg 12/23/03 gib m&p-Xylenes* ND U 3 ug/Kg 12/23/03 gib o-XyLene* ND U 3 ug/Kg 12/23/03 gib Styrene* ND U 3 ug/Kg 12/23/03 gib Bromoform* ND U 3 ug/Kg 12/23/03 gib Isopropylbenzene* ND U 3 ug/Kg 12/23/03 gjb Bromobenzene* ND U 3 ug/Kg 12/23/03 gjb 1,1,2,2-Tetrachloroethane* ND U 3 ug/Kg 12/23/03 gib 1,2,3-Trichloropropane* ND U 3 ug/Kg 12/23/03 gib n-Propylbenzene* ND U 3 ug/Kg 12/23/03 gib 2-Chlorotoluene* ND U 3 ug/Kg 12/23/03 gib 1,3,5-Trimethylbenzene* ND U 3 ug/Kg 12/23/03 gib 4-Chlorotoluene* ND U 3 ug/Kg 12/23/03 gib tert-Butylbenzene* ND U 3 ug/Kg 12/23/03 gjb 1,2,4-Trimethylbenzene* ND U 3 ug/Kg 12/23/03 gib sec-Butylbenzene* ND U 3 Ug/Kg 12/23/03 gib 1,3-Dichlorobenzene* ND U 3 ug/Kg 12/23/03 gib p-Isopropyltoluene* ND U 3 ug/Kg 12/23/03 gib 1,4-Dichlorobenzene* ND U 3 ug/Kg 12/23/03 gib n-Butylbenzene* ND U 3 ug/Kg 12/23/03 gib 1,2-Dichlorobenzene* ND U 3 ug/Kg 12/23/03 gjb 1,2,4-TrichLorobenzene* ND U 3 ug/Kg 12/23/03 gib Hexachlorobutadiene* ND U 3 ug/Kg 12/23/03 gjb Naphthalene* ND U 26 ug/Kg 12/23/03 gib 1,2,3-Trichlorobenzene* ND U 3 ug/Kg 12/23/03 gib Diethyl ether (Ether)* ND U 3 ug/Kg 12/23/03 gib DiisopropyL ether (DIPE)* ND U 3 ug/Kg 12/23/03 gib J * In Description = Dry Wgt. r , STL MADEP RIDOH57 NY DOH 10843 14 I T PH 494 NH DES 253901-A C VT DECWSD NELAP NY10843 Page 11 STL Westfield 53 Southampton Rd. Westfield, MA 01085 Tel: (413) 572 4000 - F : 572 3707 413 ax ( ) - STL Billerica 149 Rangeway.Rd. N. Billerica, MA 01862 Tel: (978) 667-1400 Fax: (978) 667-7871 l) r.. ~ • L A B ORATORY _ TES T R E S U L T S Job Number: 212086 Date: 12/29/2003 r , . . <:•s;:;;:>:::>;>:•~::>::>::> ..Bond..:::I:nc.,::::::::•::::.:.........:...:...................pRO.d~..T.:.:............................... ...CUS7; MCk.....T'~ he..ahd........., :;:;:>::>s•>;.. AT.T.N.::Me..issa:.P..ars.ons Customer Sample ID. S-3 Laboratory Sample ID: 212086-3 12/16/2003 Date Sampled... Date Received... 12/17/2003 J Time Sampled.. 15:40 Time Received.. 11:55 Sample Matrix.....: Soil . .S THQR : ; ; E. ER:TEST..D.ESCa.I.A.7T'ON.:.:...........:.. ::........................:.:PARAM..:T...:./......:.:.:::.:............................,..:..:•::.: > :::SA P,a E.>:.RES 7..... :.:::.M.................:::.:::::::... 4 . ERO :.ING :..t.I:MI:.T.: R.. fT ::::U.N,LTS..::..::: ..::DATE.:.;< TE1 H> 4-Dioxane* 1 ND U 260 ug/Kg 12/23/03 gib ~ , Ethylene tert-butyl ether (ETBE)* tert-Amyl methyl ether (TAME)* ND NO U U 3 3 ug/Kg ug/Kg 12/23/03 12/23/03 gib gib l J: . n ~ L J rl * In Description = Dry Wgt. Page 12 - STL Westfield STL Billerica ® MADEP MA014 RIDOH57 NY DOH 10843 S h .cecy,{ e "5 53 Southampton Rd. 149 Ranica, MA 01862 Westfield, MA 01085 N. Billerica, MA 01862 Tel: (413) 5724000 Tel: (978) 667.1400 CTDPH 0494 NH DES 253901 A e ~ n ~ 7871 572 3707 F 978 667 413 ` VT DECWSD DECSD NELAP NY10843 = ax: ( ) . ) . Fax . ( n _i ii L A B 0 R A T 0 R Y_ T E S T R E S U L T S Job Number: 212086 Date: 12/29%2003 • • • s>r ATTN.:.Me :issa'•>:rs ns `.T•.:i:..tte.~and>Bo.nd::;.:I:nc........~ ..R~..JE..T :a ..GUST. MER.. 9 Customer Sample ID: Trip Blank Laboratory Sample ID: 212086-4 Date Sampled......: 12/16/2003 Date Received.......: 12/17/2003 Time Sampled....... 12:00 Time Received........ 11:55 Sample Matrix.....: Methanol _:TEST:•:NET HdD PANRh1..TERf.TEST..t?E. .R IP.T.I 0..............:...:::..:::.,.:.. :..F UL-«:':;. MP..:..:.................. 4 . RE80K7I:NG>:;L:I:M SW846 5030 Met Sample Preparation Complete Text 12/23/03 caox SW8468260B MCP Volatile Organics Dichlorodifluoromethane (Freon 12) NO U 2 ug/Kg 12/23/03 gib Chloromethane NO U 5 ug/Kg 12/23/03 gib Vinyl chloride NO U 5 ug/Kg 12/23/03 gib Bromomethane NO U 5 ug/Kg 12/23/03 gjb Chloroethane NO U 5 ug/Kg 12/23/03 gjb Trichlorofluoromethene (Freon 11) NO U 2 ug/Kg 12/23/03 gib 1,1-DichLoroethene NO U 2 ug/Kg 12/23/03 gjb cis-Dichloroethene NO U 2 ug/Kg 12/23/03 gib. trans-Dichloroethene NO U 2 ug/Kg 12/23/03 gjb 1,2-Dibromo-3ichloropropane NO U 2 ug/Kg 12/23/03 gjb Carbon disuL.fide NO U 50 ug/Kg 12/23/03 gjb Acetone NO U 50 ug/Kg 12/23/03 gib Methylene chloride NO U 5 ug/Kg 12/23/03 gib Methyl-tert-butyl-ether (MTBE) NO U 5 ug/Kg 12/23/03 gib 1,1-Dichloroethane NO U 2 ug/Kg. 12/23/03 gib 2,2-Dichloropropane NO U 2 ug/Kg 12/23/03 gjb 2-Butanone (MEK) NO U 20 ug/Kg 12/23/03 gib Bromochloromethane NO U 2 ug/Kg 12/23/03 gjb Tetrahydrofuran (THF) NO U 5 ug/Kg 12/23/03 gib Chloroform NO U 2 ug/Kg 12/23/03 gib 1,1,1-Trichloroethane NO U 2 ug/Kg 12/23/03 gib 1,1-Dichlof~opropene ND U 2 ug/Kg 12/23/03 gib Carbon tetrachloride NO U 2 ug/Kg 12/23/03 gib Benzene NO U 2 ug/Kg 12/23/03 gib 1,2-Dichloroethane NO U 2 ug/Kg 12/23/03 gib Trichloroethene (TCE) NO U 2 ug/Kg 12/23/03 gib 1,2-Dichloropropane NO U 2 ug/Kg 12/23/03 gjb Dibromomethane NO U 2 ug/Kg 12/23/03 gjb Bromodichloromethane NO U 2 ug/Kg 12/23/03 gib cis-1,3-Dichloropropene NO U 2. ug/Kg 12/23/03 gjb 4-Methyl-2-pentanone (MIBK) NO U 20 ug/Kg 12/23/03 Sib Toluene NO U 2 ug/Kg 12/23/03 gib irans-1,3-Dichloropropene NO U 2 ug/Kg 12/23/03 gib 1,1,2-Trichloroethane NO U 2 ug/Kg 12/23/03 gib Tetrachloroethene NO U 2 ug/Kg 12/23/03 gib 1,3-Dichloropropane NO U 2 ug/Kg 12/23/03 gib 2-Hexanone (MNBK) NO U 20 ug/Kg 12/23/03 gjb Dibromochloromethane NO U 2 ug/Kg 12/23/03 gib 1,2-Dibromoethane (EDB) ND U 2 ug/Kg 12/23/03 gib Chlorobenzene NO U 2 ug/Kg 12/23/03 gib 1,1,1,2-Tetrachloroethane NO U 2 ug/Kg 12/23/03 gib Ethylbenzene NO U 2 ug/Kg 12/23/03 gjb m&p-Xylenes NO U 2 ug/Kg 12/23/03 gjb o-Xylene NO U 2 ug/Kg 12/23/03 gjb Styrene NO U 2 ug/Kg 12/23/03 gib * In Description= Dry Wgt. MADEP MA014 ® R DOH5 ST L VT CTDPH 0494 DECWSD Page 13 NY DOH 10843 NH DES 253901-A NELAP NY10843 CC y 'ids; - - STL Westfield 53 Southampton Rd. Westfield, MA 01085 Tel: (413)572.4000 Fax.'(413)572.3707 STL Billerica 149 Rangeway Rd. N. Billerica, MA 01862 Tel: (978) 667-1400 Fax: (978) 667-7871 n L A B O R A T O R Y _ T E ST R E S U L.T S Job Number: 212086 Date: 12/29/2003 »::>:»::::>•:<:>::>':«:::>:<?'•ROJEGT:`" 523»>•::::>>»<z::>;:<:::<::»:>:>>«:: P r... ns . CUB70MER.....T. t9he.: an..::..:.:.....:..! N.:....:::::.::.................................................................................................................:......:...::....:..,.. Customer Sample ID: Trip Blank Laboratory Sample ID: 212086-4 Date Sampled......: 12/16/2003 Date Received.......: 12/17/2003 Time Sampled....... 12:00 Time Received........ 11:55 ,Sample Matrix :,MethanoL •:<;:<.::'E:>::: :.ME.HOD 5 i:•'G? is z: i:f` 7i t:i2 i; • "Si::;i?i:::3 <>::3 it;%' =:;:f:E: E: i > :..:::::::::::::::::::::::::.RARRME.T.ERf.,7ES.T..:.4.E.S.GR.I:P.•T..Z..0.1..:::.::::.::......:.......... _ ..SAMP..L.E..R.. _ L7...... Q .KEP Bromoform ND U 2 ug/Kg 12/23/03 gjb Isopropylbenzene ND U 2 ug/Kg 12/23/03 gjb Bromobenzene ND U 2 ug/Kg 12/23/03 gjb 1,1,2,2-Tetrachloroethane ND U 2 ug/Kg 12/23/03 gjb 1,2,3-Trichloropropane ND U 2 ug/Kg 12/23/03 gib n-Propylbenzene ND U 2 ug/Kg 12/23/03 gib 2-Chlorotoluene ND U 2 ug/Kg 12/23/03 gib 1,3,5-Trimethylbenzene ND U 2 ug/Kg 12/23/03 gjb 4-Chlorotoluene ND U 2 ug/Kg 12/23/03 gjb tert-Butylbenzene ND U 2 ug/Kg 12/23/03 gib 1,2,4-Trimethylbenzene ND U 2 ug/Kg 12/23/03 gib . sec-Butylbenzene ND U 2 ug/Kg 12/23/03 gjb 1,3-Dichlorobenzene ND U 2 ug/Kg 12/23/03 gjb p-Isopropyltoluene ND U 2 ug/Kg 12/23/03 gib 1,4-Dichlorobenzene ND U 2 ug/Kg 12/23/03 gjb n-Butylbenzene ND U 2 ug/Kg 12/23/03 gib 1,2-Dichlorobenzene ND U 2 ug/Kg 12/23/03 gib 1,2,4-Trichlorobenzene ND U 2 ug/Kg 12/23/03 gjb HexachLorobutadiene ND U 2 ug/Kg 12/23/03 gjb Naphthalene ND U .25 ug/Kg 12/23/03 gib 1,2,3-Trichlorobenzene ND U 2 ug/Kg 12/23/03 gjb Diethyl ether (Ether) ND U 2 ug/Kg 12/23/03 gjb Diisopropyl ether (DIPE) ND U 2 ug/Kg 12/23/03 gib 1,4-Dioxane ND U 250 ug/Kg 12/23/03 gib Ethylene tert-butyL ether (ETBE) ND U 2 ug/Kg 12/23/03 gib tert-Amyl methyl ether (TAME) ND U 2 ug/Kg 12/23/03 gjb * In Description = Dry Wgt. ® STL MADEP 1 H5 7 NY DOH 10843 DO ® NH DES -A C DPH 0494 253901 VT DECWSD NEL4P NY 10843 Page 14 STL Westfield 53 Southampton Rd, o " "OAO,y Westfield, MA 01085 413 5724000 T l e ) : ( ' (413)572.3707 Fax STL Billerica 149 Rangeway.Rd. N. Billerica, MA 01862 Tel: (978)667.1400 Fax: (978) 667-7871 n Job Number: 212086 r~ L A B 0 R A T 0 R.Y C H R O N I C L E Lab ID: 212086-1 Client ID: S-1 METHOD DESCRIPTION % Solids 160.3 % Solids Determination SW846 5030 Met 5030 Methanol Extr. Purge & Trap SW846 3550B Extraction Ultrasonic (EPH) QC Semi-Volatile Report; Level 2 QC Volatile Report, Level 2 .QC Wet Chemistry Report, Level 2 MADEP EPH MCP Semivolatile Organics SW8468260B MCP Volatile Organics Lab ID: 212086-2 Client ID: S-2 METHOD DESCRIPTION % Solids 160.3 % Solids Determination SW846 5030 Met 5030 Methanol Extr. Purge & Trap SW846 35508 Extraction Ultrasonic (EPH) MADEP EPH MCP S.emivolatile Organics SW8468260B MCP Volatile Organics Date: 12/29/2003 Date Recvd: 12/17/2003 Sample Date. 12/16/2003 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 22022 12/18/2003 0000 1 22209 12/23/2003 1517 1 22160 12/22/2003 0000 1 22228 12/26/2003 0000 1 22217 12/24/2003 0000 1 22023 12/18/2003 0000 1 22225 22160 12/23/2003 2333 1 22216 12/23/2003 2137 Date Recvd: 12/17/2003 Sample Date: 12/16/2003 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 22022 12/18/2003 0000 1 22209 12/23/2003 1518 1 22160 12/22/2003 0000 1 22225 22160 12/24/2003 0011 1 22216 12/23/2003 2211 Lab ID: 212086-3 Client ID: S-3 METHOD DESCRIPTION % Solids 160.3 % Solids Determination SW846 5030 Met 5030 Methanol Extr. Purge & Trap SW846 35506 Extraction Ultrasonic (EPH) MADEP EPH MCP Semivolatile Organics SW8468260B MCP Volatile Organics Lab ID: 212086-4 Client ID: Trip Blank METHOD DESCRIPTION SW846 5030 Met 5030 Methanol Extr. Purge & Trap SW8468260B MCP Volatile Organics r l• Date Recvd: 12/17/2003 Sample Date: 12/16/2003 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 22022 12/18/2003 0000 1 22209 12/23/2003 1518 1 22160 12/22/2003 0000 1 22225 22160 12/24/2003 0048 1 22216 12/23/2003 2244 Date Re cvd: 12/17/2003 Sample Date: 12/16/2003 RUN# BATCH# PREP BT #(S) DATE/TIME ANALYZED 1 22209 12/23/2003 1518 1 22216 12/23/2003 2317 DILUTION 1 DILUTION 1 DILUTION 1 DILUTION 1 patle 15 STL Westfield STL Billerica STL MADEP MA014 RIDOH57 NY DOH 10843 t^~*!,`°+ era 53 Southampton 85 Westfleld, MA 01085 Tel: (413) 572-4000 149 Ra , MRd. N. Billerica, MA 01862 667 1 ® CTDPH 0494 NH DES 253901-A VT DECWSD NELAP NY10843 v of M Fax: (413) 572.3707 Tel: (978) - 400 Fax: (978) 667-7871 S U R R O G A T E R E"C O V E R I E S R E P O R'T Job Number.: 212086 ' Report Date.: 12/29/2003 CllS7o. 12......... he...aTl........ rld ....Ln..., . DJE T:. u 2 T K ea`°r's...:. ' •.S s>::>::z:>>::::>:::::<::>::>:::.n.><:.: M5.........5 :...........................P.R__ .C.........5 ...:......................................................:.....:...A..T....:..M.......5..a..P.r.. ah r, Method........: Volatile Organics Method Code...: 8260M Prep Batch....: Batch(s)...... : 22216 Test Matrix...: Water Equipment Code: VHPMS1 - Lab ID DT Sample ID 212086- 1 S-1 } 212086- 2 S-2 212086- 3 S-3 212086- 4 Trip Blank Test Test Description 12DCED 1,2-Dichloroethane-d4 (surr) BRFLBE 4-Bromofluorobenzene (surr) DBRFLM Dibromofluoromethane (surr) TOLD8 Toluene-d8 (surr) r r ^l i4 J f l .I ~ MADEP r A014 (1"1TT R V 1 L OOH57 1 ~ CTDPH 0494 VT DECWSD. Date 12DCED BRFLBE DBRFLM TOLD8 12/23/2003 99.8 103.0 94.8 101.0 12/23/2003 101.2 105.8 95.5 101.0 12/23/2003 110.3 107.8 97.1 101.2 12/23/2003 120.0 112.0 98.0 102.5 Limits 70.0 - 130. 70.0 - 130. 70.0 - 130. 70.0 - 130. STL Westfield STL Billerica 53 Southampton Rd. 149 Rangeway Rd. NY DOH 10843 Westfield, MA 01065 l 413 5724000 T N. Billerica, MA 01862 NH DES 253901-A a a ~ e : ( ) Fax'(413) 572-3707 Tel: (978) 667-1400 978 ; NELAP NY10843 ~ ) 667-7871 Fax: ( Method........: semivolatile Organics Method Code...: EPHM Prep Batch....: 22160 r Batch(s)...... : 22225 Test M atrix...: Water Equipment Code: Lab ID DT Sample ID Date 2BRONS 2FLUBP CLOODN OTERPH 1 212086- 1 S-1 12/23/2003 40.0 73.2 46.0 _ 42.5 212086- 2 S-2 12/24/2003 47.4 76.0 111.6 114.8 212086- 3 S-3 12/24/2003 59.0 102.2 52.4 65.5. I•., Test Test Description Limits 2BRONS 2-Bromonaphthalene (surr) 40.0 - 140. 2FLUBP 2-Fluorobiphenyl (surr) 40.0 - 140. CLOODN Chloro-octadecane (surr) 40.0 - 140. I% OTERPH. o-Terphenyl (surr) 40.0 - 140. r-, I i I III 'I i. J ~ I t ) I ~ I ~ 1 r^I I . Page STL Westfield STL Billerica MADEP MA014 ® RIDOH57 CTDPH 0494 STL Y DOH 10843 NH DES 253901-A n .«oAO 53 Southampton Rd. Westfield, MA 01085 Tel: (413) 572.4000 149 Rangeway Rd. N. Billerica, MA 01862 Tel: (978) 667-1400 VT DECWSD NELAP NY1 0843 n go ~ ~ Fax!(413) 572-3707 Fax: (978) 667-7871 / ~ t~ „ I I I N r~ cm ~LL a i~ i O IL..~ U _a r . I. M `O Cl) N 0] N r O ~ N CL co ) a N Q) Y Q a U) Y 0) .C Co 07 N a Z Ii 0 .O O O O O O O O O O O O O O O O O O O O O O. O O O O O Y • M M M M M M M M M M M Co M M M M M M M M M M M M M M .a ~ r T r r r T T T r r r T T r 6 r r r m T r r m r m r 0 0 0 0 0 0 0 0 00 0 0 0 0 0'6 0 0 6 0 0 0 0 0 6 0 0 a 0 0 0 p 0 6 6 ti o ti ti p 6 6 ti r` ti ti ti o CJ ~ M N rt• O d' M T N N r r r N O N O M O r r r M N r O N , 0 C N d' N N (D Q N N 1- CO CD O O 0 CO O 1~ CD 'ch / B~ cl T r T r T r T T T T r L . cl) 0 M 'cf N M CO N O Cn 0 0 I` r,. Co CO O O O w I- m M 0 r 0 r 0 0 (n C) m O 0 0 0 0 m 0 0 m 0 O 0 0) N 0 0 0 0 0 T U O 0 - 00 (A M O L!7 O N O r to O O O m 0 0 m. 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N N N N CV fV N CV N CV C,4 N N N N CV CV CV N N CV CV N CV j co f~ [0 J U > > P D > > D M D Z) ~ i" N c46 N 1 j I_ E ~ R in m m m m O LO M LO u7 Lq Ln U~ V~ Lq Lo Lq Lq Lq u~ uq N N N N CV N CV N N CV N N N N N N N N N N N N N W U U F- a) c ro c m a) L c (9 4) C ro d N E O a~ r Q) Q) c m 2 o p U L L CL O CD 0 U N E O :E a) E 2 0 O :E m L V O E V O C CD 1 -0_ O O M Z T F 5 T m r U 1- a) a) c a~ c c w a) U II U L a) o s m m 0- U o o .C 0 E - o c v O O O E O 0- 2 L O N m c L p L U 0 .O O 'O a) C C C a) N c N F^ c a) 0) U _ U ~ O U N x 2 .n f X m Ch w O N r O „C ch w a) = O L T L .r a X T w N U W r 3 'd u H 0 G N O N OJ to m o 3 ¢ is rn N C cn m F m 0 0 00 ° 'O O. Q C tY1 W ~ N uni ul r_. 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O to 0 0 0 to 0 0 0 to to 0 0 to to to to to 0 0 0 U~ (o to o CV N N N N N N N N N N N N N N CV CV N N N N N N ; N ❑ CO J ti p to to U7 LO O U7 to to c!) to to U') LO U7 U) to u7 to to to to tf) U7 p N CV N CV CV N CV N CV N N N N N N N CV CV CV N N N N N > U U U) ~ N C ll Q C (D C: C ro O ro ro ' N N CU N. d OL C w w N r- CL O C C (U U N O - C C C (U a Q j C C A w N N N C -0 T N C= N C a> d U) L U CU CU C a O Y M co = O C 7 O O j C N N 0 .0 Co .0 N M I O O O 0 O CU N C _ O E E p C E C O O N O G C O O Q 2 L C N Z a 0 T O • p 9 -0 O L O 1 L .2p o L ro .U a) C O . O C1 p l~ F- p T H Q U O N U U U .O O H s a E O` L to M L d' 7 y Os E N 0 X a M C _hi p O` d. U C N U m N m M O` r. ~t m N ,CV ty N co N LL A D7 C N T y r CO r T C T r T i T Z r J ✓I 7 cu H 14 W .Qu U F+ O G N a~-+ v ~ o Z `D co o ~ T O ~ n 3 ¢ ~ is CD m C ~ ~ v J p~ lU X N r m H [i ~ m. p O o n 'D n Q 9' o? 't m ~ ~ sn N y V 3 ) J (n w a x N G F w s~ p '13 3bJ 7Y M Q co O O c~ z 0 W F J Z z z v o ~ Q w = W O F 9 p O Z Q~ H O Cn CO N N N N U U cu cu m m C y O 'rn C9 CU X Q W ce) O C) 0 N (7) N U r J = U 0.. J ui 0-0 I N W fl co E CaC ^ ' Q v, co c ~(d F- C2 :3 Cl) U) W W J O r Z Y O m U E a tJ C C O m 0 a~ 04 m N H L z ~ .n LD - U y C 0 T 0 r 0 T 0 T 0 T 0 T 0 T 0 0 r r 0 d' T Q. 'J 0 0 0 0 0 0 0 0 ' 0 c1" d' It It It It cY d d:. i1 D . .CL r Q) O O O) t.() (o M r M O Le5 0. pUj 0 O m t` m Cb ti O ti t` ti O co Q) CO r m m 00 N m J. 0 N LL C m ' t~ CO N 00 m 0 N CO O O J U U ) . CV ct 't N 0 N to r L O CO 't ~ to I` L6 r CO o CJ .Cn ~ Cl) T (a N f~ r tl- r I` c co co co ~ co C) rn U ~ J C) ch O ~ O r O Cp d 0 CO O CO m co t1) M U C5 C'~ N LL LLI U 0 0 0 0 0 O O O C) 0 J (o. (o CD CD (o CD CD m Co CD J co co co co co co co co m co E E • d' Cn Ch ( M C M M M co (0 O O . O O . 0 .0 C O O O m J r- m M M' M M 0 co co c) co c) N O O O O O O O O O O LL CV C: C Cll (D CD a) CD CL U a) a Q) m C LL1 J (A r 0) N N cc V L C N s s Q 1E U U U U U Z Q Q CL U c (D • U (D N CD CD W O + L~ O m ~ Q tr~ m •C 1---~ rn at x U)i Y m E w U) . N N E LO LO N ~ ~ KI M o m 3 N w *0. e 0 U ~.~Yro Ogb~ J V CC) PSG m o = N °N O O a z xZ Z d' Q Q ~ r o x o 0 o A v O 0 ~i ~ O H ~ c+ V J ccs O U F+ N O II ~ II C) n I; i1 F7 I' ~I t~ n N ' J l_J p h- Z ~J Q 1_- ~ J Q a 1 F7 D L9 I 0 m i (0 00 m Q ~ _ r 01 N F- 7 Z 4-i l O N C', ❑ ~ N T ~ O N ~ Q U d• T VJ . ❑ 'D ~I E r I VJ' 0 ~ Y C CO m ~ ~ o o aw. o Q N E O U r U a) N d ~ . . o ~ C U R{ Q d ' Ln vi Q UN U N .Z o L2 ^ O 19 C, ,Q f0 N 2 (D COD lT l9 C m ax U) M Fes- lL Ir O O r. oo0M Q N N to LO N w ~ M M J co x 3 LL or~~ Q co CY) co IR O V } N IL oo z z z z v °Q rn W ti o 3 W = 2 O C- W ~aC) a E-~ cn Page 1 rpjsckL Job Sample Receipt Checklist Report V2 Job Number.: 212086 Location.: 57345 Check L ist Number.: 1 Description.: Customer Job ID.....: Job C heck List Date.: Date of the Report..: 12/17/2003 Project Number.: 20001962 Project Description.: N523 Project Manager.....: amf Customer.......: Tighe and Bond, Inc. Contact.: Melissa Parsons Questions ? (Y/N) Comments Chain-of-Custody Present? Y ....If "yes", completed properly? Y Custody seal on.shipping container? N ...If "yes", custody seal intact? Custody seals on sample containers? N ...If "yescustody seal intact? Samples iced? Y Temperature of cooler acceptable? (4 deg C 2). Y ...Temperature at receipt 2.9C. Samples received intact (good condition)?......... Y Volatile samples acceptable? (no headspace)....... Y Is a Trip Blank required? Y Was a Trip Blank provided? Y Correct containers,used? Y Adequate sample volume provided? Y Samples preserved correctly? Y Samples received within holding-time? Y Agreement between CDC and sample labels?.......... Y Comments............ If samples were shipped was there an air bill Sample Custodian Signature/Date MJB 12/17/03 J-t- L~ J~ N T f; U ' ~ co I n V W N m 0)C ~ N O m m v m a I~~z l ca Lry o°°` IL I r 1 ~ ~ ~ IL vT ~n r, oc2m2 3' y r O F aQ o'i `co O i I VJ F1 r. N G1 L O _ 0 L N r U L. O 76 a7 Ct:.:'. J ' : - Jay}O N m •J' i• o d O C m L 001 / aseaJOf!O . N J m .U ° ~}IOIxo L 6f 21: _ 1 J in E m . a ,2 t leo!6o!oua}oeg ~ ai ai . E Cr a m m3o' ' N E x y o s ti}s!Wago!eJauaO E i= H coo N g a 3-E 9 MC 'OOZ / 0609 sle}aW ar - o m m " m m'C a, . ' E c CD. E y a E Hdn / Hd r Q x o ° o 1 ' D g d 0 0 m sap!o!}sad / eOd ai N ' to m -0 m ii D QLZ8 EOnIWaS co M eon!uJaS I I N s 620.8 sal!}e!o W c i7Z9 / i7Z9 s9111e10A \ U y 0.0 auo - O of N f a c N 0 EOZSZEN a o. Z6< Hd o} HOeN r R o 2 Z> Hd o} IOH a°i I I Z> Hd 01-tOSZH co ' I t a ` Z> Hd o} EONH I t ' OaW/bOSHe a J (E))sse10 Jo (d)ogseld ~r cu U m U i ° tm sJau!e}uo0.# in CO woo O U U C V t N Y R y qeJ~ a v w v .O ` O ~ a) ~ p o a) E O F= a ~ uJ w o 0 Y , m -5 CL o . J a: lY w Z O I I I s!e ' p~ y} n o es eg s,Jaldw ` T r-. . adA_L i e ~ o!dweS 0 c m ~ ~`r x m = L l U <L j = N•v O m~?0 cn 0 Q 0 m c j d H a CD Q ! Lo v N = T . • Q L a) N cu p N ~ J7 ~ ~II CD oo N U n 3 `m = , N N 1G . ~ in C: m m m m ~ cu a) Tw la O c N O "In in O L. L y y 7 7 ?~~~v_ p, m I ! I n Q G p C O w U E >C°n m a~ d ---Q-.-:_- - O N _r r 0 ym Cl) Q 0 2 O (D O U) O U aMS II N Y C CL T O U 'I_ O CL u 3 0 a) w a a; 1 a N rn m