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Turkey Hill Rd-Mineral Hills by pond-Lab Report SF1 SR2 spill below reportable levels
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 June 23, 2009 Valerie Tillinghast OTO Associates 293 Bridge St Suite 500 Springfield, MA 01103 Project Location: -Client Job Number: Project Number: [none] Laboratory Work Order Number: 09F0322 Enclosed are results of analyses for samples received by the laboratory on June 16, 2009. If you have any questions concerning this report, please feel free to contact me. Sincerely, Susan M. Burney Project Manager Page 1 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 ANALYTICAL SUMMARY OTO Associates 6/23/2009 293 Bridge St Suite 500 Springfield, MA 01103 ATTN: Valerie Tillinghast [none] 09F0322 The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report. PROJECT LOCATION: PURCHASE ORDER NUMBER: PROJECT NUMBER: REPORT DATE: WORK ORDER NUMBER: FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB -SR-1 09F0322-01 Soil SM 2540G SW-846 8260B SR-2 09F0322-02 Soil SM 2540G SW-846 8260B Page 2 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. No sample was provided for percent solids determination. Client requested that a nominal 90% be used for calculation purposes. SW-846 8260B Qualifications: Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. Analysis is in control. Analyte & Samples(s) Qualified: trans-1,3-Dichloropropene B001413-BSD1 Response factor was less than 0.05. Significant uncertainty is associated with this result. Analyte & Samples(s) Qualified: 1,4-Dioxane, 2-Butanone (MEK), Acetone, Tetrahydrofuran 09F0322-01[SR-1], 09F0322-02[SR-2] Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy are associated with reported result. Analyte & Samples(s) Qualified: 1,4-Dioxane, 2-Butanone (MEK), Acetone, Tetrahydrofuran B001413-BLK1, B001413-BS1, B001413-BSD1 SW-846 8260B Laboratory control sample recoveries for required MCP Data Enhancement 8260 compounds were all within limits specified by the method except for “difficult analytes” where recovery control limits somewhere between 40-160% are used and/or unless otherwise listed in this narrative. Difficult analytes: MIBK, MEK, tert-butyl alcohol, acetone, 1,4-dioxane, vinyl chloride, chloromethane, dichlorodifluoromethane, 2-hexanone, naphthalene, acrylonitrile, 1,2,3-trichloropropane, methylene chloride, n-butylbenzene, and tert-butylbenzene Duplicate laboratory fortified blank RPDs were all within control limits specified by the method except for “difficult analytes” where RPDs of 50% are used and/or unless otherwise listed in this narrative. Difficult analyte: 1,4-dioxane The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Michael A. Erickson Assistant Laboratory Director Page 3 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 6/16/2009 Project Location: -Sample Description: Work Order: 09F0322 Sample ID: 09F0322-01 Field Sample #: SR-1 Sample Matrix: Soil Sampled: 6/15/2009 12:50 Analyte Results RL Dilution Flag Analyzed Analyst Date/Time Units Date Method Prepared Volatile Organic Compounds by GC/MS Acetone ND 0.062 mg/Kg dry 1 V-02 SW-846 8260B 6/17/09 6/17/09 8:14 MFF tert-Amyl Methyl Ether (TAME) ND 0.00062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Benzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Bromobenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Bromochloromethane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Bromodichloromethane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Bromoform ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Bromomethane ND 0.0062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 2-Butanone (MEK) ND 0.025 mg/Kg dry 1 V-02 SW-846 8260B 6/17/09 6/17/09 8:14 MFF n-Butylbenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF sec-Butylbenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF tert-Butylbenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Carbon Disulfide ND 0.0037 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Carbon Tetrachloride ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Chlorobenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Chlorodibromomethane ND 0.00062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Chloroethane ND 0.012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Chloroform ND 0.0025 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Chloromethane ND 0.0062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 2-Chlorotoluene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 4-Chlorotoluene ND 0.0012 mg/Kg dry 1 SW-846 8260B 8260B 6/17/09 6/17/09 8:14 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,2-Dibromoethane (EDB) ND 0.00062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Dibromomethane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,2-Dichlorobenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,3-Dichlorobenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,4-Dichlorobenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Dichlorodifluoromethane (Freon 12) ND 0.012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,1-Dichloroethane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,2-Dichloroethane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,1-Dichloroethylene ND 0.0025 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF cis-1,2-Dichloroethylene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF trans-1,2-Dichloroethylene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,2-Dichloropropane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,3-Dichloropropane ND 0.00062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 2,2-Dichloropropane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,1-Dichloropropene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF cis-1,3-Dichloropropene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF trans-1,3-Dichloropropene ND 0.00062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Diethyl Ether ND 0.012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Diisopropyl Ether (DIPE) ND 0.00062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,4-Dioxane ND 0.062 mg/Kg dry 1 V-02 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Ethylbenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Page 4 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 6/16/2009 Project Location: -Sample Description: Work Order: 09F0322 Sample ID: 09F0322-01 Field Sample #: SR-1 Sample Matrix: Soil Sampled: 6/15/2009 12:50 Analyte Results RL Dilution Flag Analyzed Analyst Date/Time Units Date Method Prepared Volatile Organic Compounds by GC/MS Hexachlorobutadiene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 2-Hexanone (MBK) ND 0.012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Isopropylbenzene (Cumene) 0.0055 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF p-Isopropyltoluene (p-Cymene) ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0025 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Methylene Chloride ND 0.012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 4-Methyl-2-pentanone (MIBK) ND 0.012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Naphthalene ND 0.012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF n-Propylbenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Styrene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,1,1,2-Tetrachloroethane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,1,2,2-Tetrachloroethane ND 0.00062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Tetrachloroethylene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Tetrahydrofuran ND 0.0062 mg/Kg dry 1 V-02 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Toluene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,2,3-Trichlorobenzene ND 0.0062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,2,4-Trichlorobenzene ND 0.0062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,1,1-Trichloroethane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,1,2-Trichloroethane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Trichloroethylene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Trichlorofluoromethane (Freon 11) ND 0.0062 mg/Kg Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,2,3-Trichloropropane ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,2,4-Trimethylbenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF 1,3,5-Trimethylbenzene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Vinyl Chloride ND 0.0062 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF m+p Xylene ND 0.0025 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF o-Xylene ND 0.0012 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:14 MFF Surrogates % Recovery Recovery Limits Flag 1,2-Dichloroethane-d4 97.0 70-130 6/17/09 8:14 Toluene-d8 98.1 70-130 6/17/09 8:14 4-Bromofluorobenzene 100 70-130 6/17/09 8:14 Page 5 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 6/16/2009 Project Location: -Sample Description: Work Order: 09F0322 Sample ID: 09F0322-02 Field Sample #: SR-2 Sample Matrix: Soil Sampled: 6/15/2009 13:05 Analyte Results RL Dilution Flag Analyzed Analyst Date/Time Units Date Method Prepared Volatile Organic Compounds by GC/MS Acetone ND 0.063 mg/Kg dry 1 V-02 SW-846 8260B 6/17/09 6/17/09 8:38 MFF tert-Amyl Methyl Ether (TAME) ND 0.00063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Benzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Bromobenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Bromochloromethane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Bromodichloromethane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Bromoform ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Bromomethane ND 0.0063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 2-Butanone (MEK) ND 0.025 mg/Kg dry 1 V-02 SW-846 8260B 6/17/09 6/17/09 8:38 MFF n-Butylbenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF sec-Butylbenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF tert-Butylbenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.00063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Carbon Disulfide ND 0.0038 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Carbon Tetrachloride ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Chlorobenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Chlorodibromomethane ND 0.00063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Chloroethane ND 0.013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Chloroform ND 0.0025 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Chloromethane ND 0.0063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 2-Chlorotoluene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 4-Chlorotoluene ND 0.0013 mg/Kg dry 1 SW-846 8260B 8260B 6/17/09 6/17/09 8:38 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,2-Dibromoethane (EDB) ND 0.00063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Dibromomethane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,2-Dichlorobenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,3-Dichlorobenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,4-Dichlorobenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Dichlorodifluoromethane (Freon 12) ND 0.013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,1-Dichloroethane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,2-Dichloroethane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,1-Dichloroethylene ND 0.0025 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF cis-1,2-Dichloroethylene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF trans-1,2-Dichloroethylene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,2-Dichloropropane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,3-Dichloropropane ND 0.00063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 2,2-Dichloropropane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,1-Dichloropropene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF cis-1,3-Dichloropropene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF trans-1,3-Dichloropropene ND 0.00063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Diethyl Ether ND 0.013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Diisopropyl Ether (DIPE) ND 0.00063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,4-Dioxane ND 0.063 mg/Kg dry 1 V-02 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Ethylbenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Page 6 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Date Received: 6/16/2009 Project Location: -Sample Description: Work Order: 09F0322 Sample ID: 09F0322-02 Field Sample #: SR-2 Sample Matrix: Soil Sampled: 6/15/2009 13:05 Analyte Results RL Dilution Flag Analyzed Analyst Date/Time Units Date Method Prepared Volatile Organic Compounds by GC/MS Hexachlorobutadiene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 2-Hexanone (MBK) ND 0.013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Isopropylbenzene (Cumene) ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF p-Isopropyltoluene (p-Cymene) ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0025 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Methylene Chloride ND 0.013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 4-Methyl-2-pentanone (MIBK) ND 0.013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Naphthalene ND 0.013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/6/17/09 8:38 MFF n-Propylbenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Styrene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,1,1,2-Tetrachloroethane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,1,2,2-Tetrachloroethane ND 0.00063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Tetrachloroethylene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Tetrahydrofuran ND 0.0063 mg/Kg dry 1 V-02 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Toluene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,2,3-Trichlorobenzene ND 0.0063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,2,4-Trichlorobenzene ND 0.0063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,1,1-Trichloroethane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,1,2-Trichloroethane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Trichloroethylene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Trichlorofluoromethane (Freon 11) ND 0.0063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,2,3-Trichloropropane ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,2,4-Trimethylbenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF 1,3,5-Trimethylbenzene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Vinyl Chloride ND 0.0063 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF m+p Xylene ND 0.0025 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF o-Xylene ND 0.0013 mg/Kg dry 1 SW-846 8260B 6/17/09 6/17/09 8:38 MFF Surrogates % Recovery Recovery Limits Flag 1,2-Dichloroethane-d4 96.9 70-130 6/17/09 8:38 Toluene-d8 96.7 70-130 6/17/09 8:38 4-Bromofluorobenzene 98.5 70-130 6/17/09 8:38 Page 7 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Sample Extracton Data Prep Method: SW-846 5035-SW-846 8260B Lab Number [Field ID] Batch Initial [g] Final [mL] Date 09F0322-01 [SR-1] B001413 9.03 10 06/17/09 09F0322-02 [SR-2] B001413 8.79 10 06/17/09 Page 8 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Analyte Limit Notes Volatile Organic Compounds by GC/MS -Quality Control QUALITY CONTROL Batch B001413 -SW-846 5035 Blank (B001413-BLK1) Prepared & Analyzed: 06/17/09 Acetone ND 0.10 mg/Kg wet V-16 tert-Amyl Methyl Ether (TAME) ND 0.0010 mg/Kg wet Benzene ND 0.0020 mg/Kg wet Bromobenzene ND 0.0020 mg/Kg wet Bromochloromethane ND 0.0020 mg/Kg wet Bromodichloromethane ND 0.0020 mg/Kg wet Bromoform ND 0.0020 mg/Kg wet Bromomethane ND 0.010 mg/Kg wet 2-Butanone (MEK) ND 0.040 mg/Kg wet V-16 n-Butylbenzene ND 0.0020 mg/Kg wet sec-Butylbenzene ND 0.0020 mg/Kg wet tert-Butylbenzene ND 0.0020 mg/Kg wet tert-Butyl Ethyl Ether (TBEE) ND 0.0010 mg/Kg wet Carbon Disulfide ND 0.0060 mg/Kg wet Carbon Tetrachloride ND 0.0020 mg/Kg wet Chlorobenzene ND 0.0020 mg/Kg wet Chlorodibromomethane ND 0.0010 mg/Kg wet Chloroethane ND 0.020 mg/Kg wet Chloroform ND 0.0040 mg/Kg wet Chloromethane ND 0.010 mg/Kg wet 2-Chlorotoluene ND 0.0020 mg/Kg wet 4-Chlorotoluene ND 0.0020 mg/Kg wet 1,2-Dibromo-3-chloropropane (DBCP) ND 0.010 mg/Kg wet 1,2-Dibromoethane (EDB) ND 0.0010 mg/Kg wet Dibromomethane ND 0.0020 mg/Kg wet 1,2-Dichlorobenzene ND 0.0020 mg/Kg wet 1,3-Dichlorobenzene ND 0.0020 mg/Kg wet 1,4-Dichlorobenzene ND 0.0020 mg/Kg wet Dichlorodifluoromethane (Freon 12) ND 0.020 mg/Kg wet 1,1-Dichloroethane ND 0.0020 mg/Kg wet 1,2-Dichloroethane ND 0.0020 mg/Kg wet 1,1-Dichloroethylene ND 0.0040 mg/Kg wet cis-1,2-Dichloroethylene ND 0.0020 mg/Kg wet trans-1,2-Dichloroethylene ND 0.0020 mg/Kg wet 1,2-Dichloropropane ND 0.0020 mg/Kg wet 1,3-Dichloropropane ND 0.0010 mg/Kg wet 2,2-Dichloropropane ND 0.0020 mg/Kg wet 1,1-Dichloropropene ND 0.0020 mg/Kg wet cis-1,3-Dichloropropene ND 0.0020 mg/Kg wet trans-1,3-Dichloropropene ND 0.0010 mg/Kg wet Diethyl Ether ND 0.020 mg/Kg wet Diisopropyl Ether (DIPE) ND 0.0010 mg/Kg wet 1,4-Dioxane ND 0.10 mg/Kg wet V-16 Ethylbenzene ND 0.0020 mg/Kg wet Hexachlorobutadiene ND 0.0020 mg/Kg wet 2-Hexanone (MBK) ND 0.020 mg/Kg wet Isopropylbenzene (Cumene) ND 0.0020 mg/Kg wet p-Isopropyltoluene (p-Cymene) ND 0.0020 mg/Kg wet Methyl tert-Butyl Ether (MTBE) ND 0.0040 mg/Kg wet Methylene Chloride ND 0.020 mg/Kg wet 4-Methyl-2-pentanone (MIBK) ND 0.020 mg/Kg wet Naphthalene ND 0.020 mg/Kg wet Page 9 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Analyte Limit Notes Volatile Organic Compounds by GC/MS -Quality Control QUALITY CONTROL Batch B001413 -SW-846 5035 Blank (B001413-BLK1) Prepared & Analyzed: 06/17/09 n-Propylbenzene ND 0.0020 mg/Kg wet Styrene ND 0.0020 mg/Kg wet 1,1,1,2-Tetrachloroethane ND 0.0020 mg/Kg wet 1,1,2,2-Tetrachloroethane ND 0.0010 mg/Kg wet Tetrachloroethylene ND 0.0020 mg/Kg wet Tetrahydrofuran ND 0.010 mg/Kg wet V-16 Toluene ND 0.0020 mg/Kg wet 1,2,3-Trichlorobenzene ND 0.010 mg/Kg wet 1,2,4-Trichlorobenzene ND 0.010 mg/Kg wet 1,1,1-Trichloroethane ND 0.0020 mg/Kg wet 1,1,2-Trichloroethane ND 0.0020 mg/Kg wet Trichloroethylene ND 0.0020 mg/Kg wet Trichlorofluoromethane (Freon 11) ND 0.010 mg/Kg wet 1,2,3-Trichloropropane ND 0.0020 mg/Kg wet 1,2,4-Trimethylbenzene ND 0.0020 mg/Kg wet 1,3,5-Trimethylbenzene ND 0.0020 mg/Kg wet Vinyl Chloride ND 0.010 mg/Kg wet m+p Xylene ND 0.0040 mg/Kg wet o-Xylene ND 0.0020 mg/Kg wet Surrogate: 1,2-Dichloroethane-d4 0.0441 mg/Kg wet 0.0500 88.2 70-130 Surrogate: Toluene-d8 0.0482 mg/Kg wet 0.0500 96.4 70-130 Surrogate: 4-Bromofluorobenzene 0.0485 mg/Kg wet 0.0500 97.1 70-130 LCS (B001413-BS1) Prepared & Analyzed: 06/17/09 Acetone 0.245 0.10 mg/Kg wet 0.200 122 70-160 V-16 † tert-Amyl Methyl Ether (TAME) 0.0226 0.0010 mg/Kg wet 0.0200 113 70-130 Benzene 0.0187 0.0020 mg/Kg wet 0.0200 93.7 70-130 Bromobenzene 0.0188 0.0020 mg/Kg wet 0.0200 94.0 70-130 Bromochloromethane 0.0181 0.0020 mg/Kg wet 0.0200 90.6 70-130 Bromodichloromethane 0.0181 0.0020 mg/Kg wet 0.0200 90.6 70-130 Bromoform 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 Bromomethane 0.0139 0.010 mg/Kg wet 0.0200 69.4 40-130 † 2-Butanone (MEK) 0.223 0.040 mg/Kg wet 0.200 112 70-160 V-16 † n-Butylbenzene 0.0194 0.0020 mg/Kg wet 0.0200 97.1 70-130 sec-Butylbenzene 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 tert-Butylbenzene 0.0200 0.0020 mg/Kg wet 0.0200 100 70-160 † tert-Butyl Ethyl Ethyl Ether (TBEE) 0.0219 0.0010 mg/Kg wet 0.0200 110 70-130 Carbon Disulfide 0.0195 0.0060 mg/Kg wet 0.0200 97.6 70-130 Carbon Tetrachloride 0.0204 0.0020 mg/Kg wet 0.0200 102 70-130 Chlorobenzene 0.0183 0.0020 mg/Kg wet 0.0200 91.7 70-130 Chlorodibromomethane 0.0197 0.0010 mg/Kg wet 0.0200 98.7 70-130 Chloroethane 0.0154 0.0040 mg/Kg wet 0.0200 77.2 70-130 Chloroform 0.0187 0.0040 mg/Kg wet 0.0200 93.5 70-130 Chloromethane 0.0145 0.010 mg/Kg wet 0.0200 72.5 70-130 2-Chlorotoluene 0.0196 0.0020 mg/Kg wet 0.0200 97.8 70-130 4-Chlorotoluene 0.0197 0.0020 mg/Kg wet 0.0200 98.6 70-130 1,2-Dibromo-3-chloropropane (DBCP) 0.0175 0.010 mg/Kg wet 0.0200 87.4 70-130 1,2-Dibromoethane (EDB) 0.0196 0.0010 mg/Kg wet 0.0200 97.8 70-130 Dibromomethane 0.0187 0.0020 mg/Kg wet 0.0200 93.6 70-130 1,2-Dichlorobenzene 0.0181 0.0020 mg/Kg wet 0.0200 90.5 70-130 1,3-Dichlorobenzene 0.0177 0.0020 mg/Kg wet 0.0200 88.6 70-130 1,4-Dichlorobenzene 0.0172 0.0020 mg/Kg wet 0.0200 86.0 70-130 Page 10 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Analyte Limit Notes Volatile Organic Compounds by GC/MS -Quality Control QUALITY CONTROL Batch B001413 -SW-846 5035 LCS (B001413-BS1) Prepared & Analyzed: 06/17/09 Dichlorodifluoromethane (Freon 12) 0.0146 0.0040 mg/Kg wet 0.0200 72.8 40-160 † 1,1-Dichloroethane 0.0185 0.0020 mg/Kg wet 0.0200 92.3 70-130 1,2-Dichloroethane 0.0185 0.0020 mg/Kg wet 0.0200 92.7 70-130 1,1-Dichloroethylene 0.0184 0.0040 mg/Kg wet 0.0200 92.2 70-130 cis-1,2-Dichloroethylene 0.0185 0.0020 mg/Kg wet 0.0200 92.5 70-130 trans-1,2-Dichloroethylene 0.0185 0.0020 mg/Kg wet 0.0200 92.6 70-130 1,2-Dichloropropan e 0.0189 0.0020 mg/Kg wet 0.0200 94.3 70-130 1,3-Dichloropropane 0.0187 0.0010 mg/Kg wet 0.0200 93.6 70-130 2,2-Dichloropropane 0.0197 0.0020 mg/Kg wet 0.0200 98.6 70-130 1,1-Dichloropropene 0.0194 0.0020 mg/Kg wet 0.0200 97.0 70-130 cis-1,3-Dichloropropene 0.0194 0.0020 mg/Kg wet 0.0200 97.1 70-130 trans-1,3-Dichloropropene 0.0254 0.0010 mg/Kg wet 0.0200 127 70-130 Diethyl Ether 0.0188 0.0040 mg/Kg wet 0.0200 93.9 70-130 Diisopropyl Ether (DIPE) 0.0209 0.0010 mg/Kg wet 0.0200 105 70-130 1,4-Dioxane 0.187 0.10 mg/Kg wet 0.200 93.3 40-160 V-16 † Ethylbenzene 0.0195 0.0020 mg/Kg wet 0.0200 97.4 70-130 Hexachlorobutadiene 0.0194 0.0020 mg/Kg wet 0.0200 97.2 70-160 2-Hexanone (MBK) 0.242 0.020 mg/Kg wet 0.200 121 70-160 † Isopropylbenzene (Cumene) 0.0220 0.0020 mg/Kg wet 0.0200 110 70-130 p-Isopropyltoluene (p-Cymene) 0.0208 0.0020 mg/Kg wet 0.0200 104 70-130 Methyl tert-Butyl Ether (MTBE) 0.0211 0.0040 mg/Kg wet 0.0200 105 70-130 Methylene Chloride 0.0190 0.0040 mg/Kg wet 0.0200 95.1 40-160 † 4-Methyl-2-pentanone (MIBK) 0.228 0.020 mg/Kg wet 0.200 114 70-160 † Naphthalene 0.0193 0.010 mg/Kg wet 0.0200 96.4 40-130 † n-Propylbenzene 0.0207 0.0020 mg/Kg wet 0.0200 104 70-130 Styrene 0.0197 0.0020 mg/Kg wet 0.0200 98.3 70-130 1,1,1,2-Tetrachloroethane 0.0195 0.0020 mg/Kg wet 0.0200 97.7 70-130 1,1,2,2-Tetrachloro ethane 0.0184 0.0010 mg/Kg wet 0.0200 91.9 70-130 Tetrachloroethylene 0.0198 0.0020 mg/Kg wet 0.0200 99.0 70-130 Tetrahydrofuran 0.0205 0.010 mg/Kg wet 0.0200 102 70-130 V-16 Toluene 0.0189 0.0020 mg/Kg wet 0.0200 94.5 70-130 1,2,3-Trichlorobenzene 0.0182 0.010 mg/Kg wet 0.0200 90.9 70-130 1,2,4-Trichlorobenzene 0.0190 0.010 mg/Kg wet 0.0200 95.0 70-130 1,1,1-Trichloroethane 0.0195 0.0020 mg/Kg wet 0.0200 97.7 70-130 1,1,2-Trichloroethane 0.0183 0.0020 mg/Kg wet 0.0200 91.3 70-130 Trichloroethylene 0.0191 0.0020 mg/Kg wet 0.0200 95.7 70-130 Trichlorofluoromethane (Freon 11) 0.0172 0.010 mg/Kg wet 0.0200 86.0 70-130 1,2,3-Trichloropropane 0.0205 0.0020 mg/Kg wet 0.0200 102 70-130 1,2,4-Trimethylbenzene 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 1,3,5-Trimethylbenzene 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 Vinyl Chloride 0.0160 0.010 mg/Kg wet 0.0200 80.0 40-130 † m+p Xylene 0.0398 0.0040 mg/Kg wet 0.0400 99.4 70-130 o-Xylene 0.0196 0.0020 mg/Kg wet 0.0200 98.2 70-130 Surrogate: 1,2-Dichloroethane-d4 0.0471 mg/Kg wet 0.0500 94.2 70-130 Surrogate: Toluene-d8 0.0499 mg/Kg wet 0.0500 99.8 70-130 Surrogate: 4-Bromofluorobenze ne 0.0499 mg/Kg wet 0.0500 99.8 70-130 Page 11 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Analyte Limit Notes Volatile Organic Compounds by GC/MS -Quality Control QUALITY CONTROL Batch B001413 -SW-846 5035 LCS Dup (B001413-BSD1) Prepared & Analyzed: 06/17/09 Acetone 0.250 0.10 mg/Kg wet 0.200 125 70-160 2.18 25 V-16 † tert-Amyl Methyl Ether (TAME) 0.0230 0.0010 mg/Kg wet 0.0200 115 70-130 1.76 25 Benzene 0.0196 0.0020 mg/Kg wet 0.0200 97.8 70-130 4.28 25 Bromobenzene 0.0199 0.0020 mg/Kg wet 0.0200 99.3 70-130 5.48 25 Bromochloromethane 0.0189 0.0020 mg/Kg wet 0.0200 94.4 70-130 4.11 25 Bromodichloromethane 0.0192 0.0020 mg/Kg wet 0.0200 95.8 70-130 5.58 25 Bromoform 0.0207 0.0020 mg/Kg wet 0.0200 104 70-130 2.44 25 Bromomethane 0.0163 0.010 mg/Kg wet 0.0200 81.3 40-130 15.8 25 † 2-Butanone (MEK) 0.213 0.040 mg/Kg wet 0.200 106 70-160 4.80 25 V-16 † n-Butylbenzene 0.0207 0.0020 mg/Kg wet 0.0200 104 70-130 6.57 25 sec-Butylbenzene 0.0220 0.0020 mg/Kg wet 0.0200 110 70-130 6.68 25 tert-Butylbenzene 0.0212 0.0020 mg/Kg wet 0.0200 106 70-160 5.44 25 † tert-Butyl Ethyl Ether (TBEE) 0.0223 0.0010 mg/Kg wet 0.0200 111 70-130 1.72 25 Carbon Disulfide 0.0212 0.0060 mg/Kg wet 0.0200 106 70-130 8.25 25 Carbon Tetrachloride 0.0217 0.0020 mg/Kg wet 0.0200 108 70-130 5.99 25 Chlorobenzene 0.0192 0.0020 mg/Kg wet 0.0200 96.1 70-130 4.69 25 Chlorodibromomethane 0.0204 0.0010 mg/Kg wet 0.0200 102 70-130 3.19 25 Chloroethane 0.0172 0.0040 mg/Kg wet 0.0200 86.1 70-130 10.9 25 Chloroform 0.0197 0.0040 mg/Kg wet 0.0200 98.4 70-130 5.11 25 Chloromethane 0.0159 0.010 mg/Kg wet 0.0200 79.6 70-130 9.34 25 2-Chlorotoluene 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 5.37 25 4-Chlorotoluene 0.0209 0.0020 mg/Kg wet 0.0200 104 70-130 5.62 25 1,2-Dibromo-3-chloropropane (DBCP) 0.0173 0.010 mg/Kg wet 0.0200 86.3 70-130 1.27 25 1,2-Dibromoethane (EDB) 0.0200 0.0010 mg/Kg wet 0.0200 100 70-130 2.32 25 Dibromomethane 0.0194 0.0020 mg/Kg wet 0.0200 96.8 70-130 3.36 25 1,2-Dichlorobenzene 0.0193 0.0020 mg/Kg wet 0.0200 96.3 70-130 6.21 25 1,3-Dichlorobenzene 0.0189 0.0020 mg/Kg wet 0.0200 94.7 70-130 6.66 25 1,4-Dichlorobenzene 0.0181 0.0020 mg/Kg wet 0.0200 90.4 70-130 4.99 25 Dichlorodifluoromethane (Freon 12) 0.0153 0.0040 mg/Kg wet 0.0200 76.3 40-160 4.69 25 † 1,1-Dichloroethane 0.0194 0.0020 mg/Kg wet 0.0200 96.9 70-130 4.86 25 1,2-Dichloroethane 0.0195 0.0020 mg/Kg wet 0.0200 97.4 70-130 4.94 25 1,1-Dichloroethylene 0.0200 0.0040 mg/Kg wet 0.0200 99.8 70-130 7.92 25 cis-1,2-Dichloroethylene 0.0193 0.0020 mg/Kg wet 0.0200 96.4 70-130 4.13 25 trans-1,2-Dichloroethylene 0.0194 0.0020 mg/Kg wet 0.0200 96.8 70-130 4.44 25 1,2-Dichloropropane 0.0195 0.0020 mg/Kg wet 0.0200 97.6 70-130 3.44 25 1,3-Dichloropropane 0.0195 0.0010 mg/Kg wet 0.0200 97.3 70-130 3.88 25 2,2-Dichloropropane 0.0209 0.0020 mg/Kg wet 0.0200 105 70-130 5.91 25 1,1-Dichloropropene 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 4.14 25 cis-1,3-Dichloropropene 0.0204 0.0020 mg/Kg wet 0.0200 102 70-130 4.73 25 trans-1,3-Dichloropropene 0.0261 0.0010 mg/Kg wet 0.0200 131 * 70-130 2.87 25 L-07 Diethyl Ether 0.0203 0.020 mg/Kg wet 0.0200 101 70-130 7.68 25 Diisopropyl Ether (DIPE) 0.0214 0.0010 mg/Kg wet 0.0200 107 70-130 2.17 25 1,4-Dioxane 0.198 0.10 mg/Kg wet 0.200 99.0 40-160 5.98 50 V-16 † ‡ Ethylbenzene 0.0213 0.0020 mg/Kg wet 0.0200 106 70-130 8.74 25 Hexachlorobutadiene 0.0206 0.0020 mg/Kg wet 0.0200 103 70-160 5.79 25 2-Hexanone (MBK) 0.233 0.020 mg/Kg wet 0.200 117 70-160 3.55 25 † Isopropylbenzene (Cumene) 0.0236 0.0020 mg/Kg wet 0.0200 118 70-130 6.75 25 p-Isopropyltoluene (p-Cymene) 0.0222 0.0020 mg/Kg wet 0.0200 111 70-130 6.70 25 Methyl tert-Butyl Ether (MTBE) 0.0214 0.0040 mg/Kg wet 0.0200 107 70-130 1.41 25 Methylene Chloride 0.0195 0.0040 mg/Kg wet 0.0200 97.7 40-160 2.70 25 † 4-Methyl-2-pentanone (MIBK) 0.222 0.020 mg/Kg wet 0.200 111 70-160 2.35 25 † Naphthalene 0.0190 0.010 mg/Kg wet 0.0200 94.9 40-130 1.57 25 † Page 12 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Analyte Limit Notes Volatile Organic Compounds by GC/MS -Quality Control QUALITY CONTROL Batch B001413 -SW-846 5035 LCS Dup (B001413-BSD1) Prepared & Analyzed: 06/17/09 n-Propylbenzene 0.0219 0.0020 mg/Kg wet 0.0200 110 70-130 5.82 25 Styrene 0.0208 0.0020 mg/Kg wet 0.0200 104 70-130 5.54 25 1,1,1,2-Tetrachloroethane 0.0204 0.0020 mg/Kg wet 0.0200 102 70-130 4.31 25 1,1,2,2-Tetrachloroethane 0.0184 0.0010 mg/Kg wet 0.0200 92.1 70-130 0.217 25 Tetrachloroethylene 0.0215 0.0020 mg/Kg wet 0.0200 107 70-130 8.05 25 Tetrahydrofuran 0.0191 0.010 mg/Kg wet 0.0200 95.4 70-130 7.08 25 V-16 Toluene 0.0200 0.0020 mg/Kg wet 0.0200 99.9 70-130 5.56 25 1,2,3-Trichlorobenzene 0.0185 0.010 mg/Kg wet 0.0200 92.7 70-130 1.96 25 1,2,4-Trichlorobenzene 0.0194 0.010 mg/Kg wet 0.0200 96.9 70-130 1.98 25 1,1,1-Trichloroethane 0.0207 0.0020 mg/Kg wet 0.0200 104 70-130 5.96 25 1,1,2-Trichloroethane 0.0188 0.0020 mg/Kg wet 0.0200 93.8 70-130 2.70 25 Trichloroethylene 0.0205 0.0020 mg/Kg wet 0.0200 102 70-130 6.67 25 Trichlorofluoromethane (Freon 11) 0.0185 0.010 mg/Kg wet 0.0200 92.7 70-130 7.50 25 1,2,3-Trichloropropane 0.0204 0.0020 mg/Kg wet 0.0200 102 70-130 0.392 25 1,2,4-Trimethylbenzene 0.0215 0.0020 mg/Kg wet 0.0200 107 70-130 6.25 25 1,3,5-Trimethylbenzene 0.0214 0.0020 mg/Kg wet 0.0200 107 70-130 5.86 25 Vinyl Chloride 0.0171 0.010 mg/Kg wet 0.0200 85.6 40-130 6.76 25 † m+p Xylene 0.0420 0.0040 mg/Kg wet 0.0400 105 70-130 5.38 25 o-Xylene 0.0211 0.0020 mg/Kg wet 0.0200 105 70-130 6.98 25 Surrogate: 1,2-Dichloroethane-d4 0.0450 mg/Kg wet 0.0500 90.1 70-130 Surrogate: Toluene-d8 0.0497 mg/Kg wet 0.0500 99.3 70-130 Surrogate: 4-Bromofluorobenzene 0.0499 mg/Kg wet 0.0500 99.8 70-130 Page 13 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. † Wide recovery limits estabished for difficult compound. ‡ Wide RPD limits estabished for difficult compound. # Data exceeded client recommended or regulatory level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. Analysis is in control. L-07 V-02 Response factor was less than 0.05. Significant uncertainty is associated with this result. Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy are associated with reported result. V-16 Page 14 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Analyte Certifications CERTIFICATIONS Certified Analyses included in this Report SW-846 8260B in Soil Acetone CT,NH,NY Benzene CT,NH,NY Bromobenzene NH,NY Bromochloromethane NH,NY Bromodichloromethane CT,NH,NY Bromoform CT,NH,NY Bromomethane CT,NH,NY 2-Butanone (MEK) CT,NH,NY n-Butylbenzene CT,NH,NY sec-Butylbenzene CT,NH,NY tert-Butylbenzene CT,NH,NY Carbon Disulfide CT,NH,NY Carbon Tetrachloride CT,NH,NY Chlorobenzene CT,NH,NY Chlorodibromomethane CT,NH,NY Chloroethane CT,NH,NY Chloroform CT,NH,NY Chloromethane CT,NH,NY 2-Chlorotoluene CT,NH,NY 4-Chlorotoluene CT,NH,NY Dibromomethane NH,NY 1,2-Dichlorobenzene CT,NH,NY 1,3-Dichlorobenzene CT,NH,NY 1,4-Dichlorobenzen e CT,NH,NY Dichlorodifluoromethane (Freon 12) NY 1,1-Dichloroethane CT,NH,NY 1,2-Dichloroethane CT,NH,NY 1,1-Dichloroethylene CT,NH,NY cis-1,2-Dichloroethylene CT,NH,NY trans-1,2-Dichloroethylene CT,NH,NY 1,2-Dichloropropane CT,NH,NY 1,3-Dichloropropane NH,NY 2,2-2,2-Dichloropropane NH,NY 1,1-Dichloropropene NH,NY cis-1,3-Dichloropropene CT,NH,NY trans-1,3-Dichloropropene CT,NH,NY Ethylbenzene CT,NH,NY Hexachlorobutadiene NH,NY 2-Hexanone (MBK) CT,NH,NY Isopropylbenzene (Cumene) CT,NH,NY Methylene Chloride CT,NH,NY 4-Methyl-2-pentanone (MIBK) CT,NH,NY Naphthalene NH,NY Styrene CT,NH,NY 1,1,1,2-Tetrachloroethane CT,NH,NY 1,1,2,2-Tetrachloroethane CT,NH,NY Tetrachloroethylene CT,NH,NY Page 15 of 19 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Analyte Certifications CERTIFICATIONS Certified Analyses included in this Report SW-846 8260B in Soil Toluene CT,NH,NY 1,2,4-Trichlorobenzene NH,NY 1,1,1-Trichloroethane CT,NH,NY 1,1,2-Trichloroethane CT,NH,NY Trichloroethylene CT,NH,NY Trichlorofluoromethane (Freon 11) CT,NH,NY 1,2,3-Trichloropropan e NH,NY 1,2,4-Trimethylbenzene CT,NH,NY 1,3,5-Trimethylbenzene CT,NH,NY Vinyl Chloride CT,NH,NY m+p Xylene CT,NH,NY o-Xylene CT,NH,NY The CON-TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA American Industrial Hygiene Association 100033 01/1/2010 MA Massachusetts DEP M-MA100 06/30/2009 CT Connecticut Department of Publilc Health PH-0567 09/30/2009 NY New York State Department of Health 10899 NELAP 04/1/2010 NH New Hampshire Environmental Lab 2516 NELAP 02/5/2010 RI Rhode Island Department of Health LAO00112 12/30/2009 NC North Carolina Div. of Water Quality 652 12/31/2009 NJ New Jersey DEP MA007 NELAP 06/30/2009 FL Florida Department of Health E871027 NELAP 06/30/2009 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2010 WA State of Washington Department of Ecology C2065 03/23/2010 Page 16 of 19 Page 17 of 19 Page 18 of 19 MADEP MCP Analytical Method Report Certification Form Laboratory Name: Con-Test Analytical Laboratory Project #: Project Location: This Form provides certifications for the following data set: [list Laboratory Sample ID Number(s)] 09F0322 09F0322-01 thru 09F0322-028260B (X) 8151A ( ) 8330 ( ) 6010B ( ) 7470A/1A ( ) 8270C ( ) 8081A ( ) VPH ( ) 6020 ( ) 9014M² ( ) 8082 ( ) 8021B ( ) EPH ( ) 7000 S³ ( ) 7196A ( ) MCP SW-846 Methods Used As specified in MADEP Compendium of Analytical Methods. (check all that apply) 1 List Release Tracking Number (RTN), if known 2 M --SW-846 Method 9014 or MADEP Physiologically Available Cyanide (PAC) Method 3 S --SW-846 Methods 7000 Series List individual method and analyte -Sample Matrices: MADEP RTN1¹: Soil An affirmative response to questions A, B, C and D is required for “Presumptive Certainty” status A Were all samples received by the laboratory in a condition consistent with that ü Yes No¹ described on the Chain-of-Custody documentation for the data set? B Were all QA/QC procedures required for the specified analytical method(s) ü Yes No¹ included in this report followed, including the requirement to note and discuss in a narrative QC data that did not meet appropriate performance standards or guidelines? C Does the data included in this report meet all the analytical requirements for ü Yes No¹ “Presumptive Certainty”, as described in Section 2.0 (a), (b), (c) and (d) of the MADEP document CAM VII A, “Quality Assurance and Quality Control Guidelines for the Acquisition and Reporting of Analytical Data? D VPH and EPH Methods only: Was the VPH or EPH Method conducted without Yes No¹ significant modifications (see Section 11.3 of respective Methods) E Were all analytical QC performance standards and recommendations for the specified methods achieved? Yes ü No¹ A response to questions E and F below is required for “Presumptive Certainty” status Were results for all analyte-list compounds/elements for the specified method(s) reported? F ü Yes No¹ I, the undersigned, attest under the pains and penalties of perjury that, based upon my personal inquiry of those responsible for obtaining the information, the material contained in this analytical report is, to the best of my knowledge and belief, accurate and complete. ¹All Negative responses must be addressed in an attached Environmental Laboratory case narrative. Signature: Printed Name: Position: Date: Assistant Laboratory Director Michael A. Erickson 06/22/09 CAM VII A, rev. 3.2 April 2004 Page 19 of 19