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39-060 Atwood Drive wireless tower siteEnvironm.entalSafetyHealthGeotechnical T O'Reilly, Talbot & Okun 4VTMTMVrab 293 Bridge Street [ A S S O C I A T E S] - Suite 500 ~ II Springfield, MA 01103 Tel 413 788 6222 Fax 413 788 8830 Email office@oto-env.com D D U November 3, 1999 File No. J84-05-17 Mr. Peter McErlain Office of Planning and Development City Hall 210 Main Street Northampton, MA 01060 Re: Limited Removal Action Atwood Drive Northampton, MA Dear Mr. McErlain: This letter documents completion of a Limited Removal Action (LRA) as defined in the Massachusetts Contingency Plan (310 CMR 40.0318) to remove lead contaminated soil from the above referenced property in Northampton, Massachusetts. Our report is subject to the limitations 'attached in Appendix A. Background A site locus and site plan are provided as Figures 1 and 2 respectively. An environmental site assessment performed by O'Reilly, Talbot & Okun Associates, Inc. (OTO) for a perspective leasee indicated that fill material was likely present on the Atwood Drive property. A series of test pits was performed on the property, which included analytical testing of the fill material. The fill material was tested for Extractable Petroleum Hydrocarbons (EPH), polychlorinated byphenols (PCBs) and RCRA 8 metals. Location Test Pit .1 (TP-1) contained approximately 2.5 feet of granular fill with concentrations of lead at 347 mg/kg, above the applicable Reportable Concentration (RCS-1) for total lead of 300 mg/kg. No EPH or PCB compounds were detected above Reportable Concentrations. A copy of the test pit log for TP-1 is provided in Appendix B. Analytical data are summarized in Table 1 and analytical data sheets are provided in Appendix C. We understand that the City of Northampton was notified of concentrations of lead in site soil above reportable concentrations by facsimile letter dated February 3, 1999 Additional Fill Characterization The extent of, lead impacted soil around TP-1 was further characterized through a boring program performed December 18, 1998 and January 29, 1999. Ten additional soil samples were collected on these dates and analyzed for total lead. The results are summarized in Table 1. The locations of samples (NOHO-2,3,5,7,8,9,101,103,105, and 108) and results of total lead analyses are shown on Figure 2. Each of these samples was collected from the fill material within 2.0 to 2.5 feet of the ground surface, with the exception of NOHO-9, which was collected from the natural soil material underlying the fill. Soil sample NOHO-5 had the highest total lead concentration at 783 mg/kg. The T O'Reilly, Talbot & Olcun [ A S _S 0 C- I_A T _.E. S ] i - _ OHO-5 sample was tested for leachable lead by the Toxicity Characteristic Leaching Procedure N (TCLP) and found to contain a leachable lead concentration of 6.07 mg/1, which exceeded the 5.0 mg/l standard defining a characteristically hazardous waste. Based on the analytical data, an area of lead contaminated soil of approximately 20 cubic yards was identified as shown on Figure 2. n Groundwater Characterization In addition to fill characterization, a groundwater monitoring well (NOHO-1) was installed adjacent to test pit TP-1 (approximately 15 feet south in the inferred downgradient groundwater flow direction) to evaluate potential groundwater impacts. The well was installed on December 18, 1999 in a boring drilled to a depth of 24 feet. The monitoring well installation and subsurface conditions encountered are shown on the boring log attached in Appendix B. Soil samples were collected by split spoon using standard penetration tests continuously to depths of 15 feet and screened for VOCs with the PID: No VOCs were detected. Soil conditions consisted of granular fill to a depth of 2 feet, followed by fine to medium sand, with trace amounts of silt. Thin (1 to 2 inch thick) layers of clay were observed below 10 feet. Groundwater was encountered at a depth of approximately 18 feet. a On December 28, 1998 a groundwater sample was collected from the monitoring well. The groundwa- ter sample was collected using an individually dedicated disposable plastic bailer. Prior to sample a collection three to five times the volume of standing water in the well was removed to provide a sample of formation water in the well for collection. Groundwater samples were than collected into pre-preserved bottles for analysis for Extractable and Volatile Petroleum Hydrocarbons (EPH/VPH) j Volatile Organic Compounds (VOCs) and dissolved lead. The dissolved lead sample was filtered prior u to preservation to remove sediment. The analytical data sheets for the groundwater analyses are also attached in Appendix C. As shown, no contaminants were detected in the groundwater samples. A groundwater sample was also screened in the field for pH and specific conductance. The pH reading was 6.5 and the specific conductance reading was 290. These values are within the range typical for this geographic region. Limited Removal Action Excavation The lead contaminated soils were excavated by CT Environmental, Inc. of Longmeadow, Massachusetts on May 27, 1999. The excavation was observed by Bruce H. Nickelsen of O'Reilly, Talbot & Okun Associates, Inc. The soils were excavated to a depth of 2.5 feet (the depth of fill) and to the lateral limits shown on Figure 2. Excavated soils were placed on top of and covered with plastic sheeting. Approximately 5 cubic yards was excavated from the vicinity of the NOHO-5 sample location, which had been found to be characteristically hazardous based on TCLP testing. The remaining approximately 15 cubic yards of soil were excavated and stockpiled separately. A soil sample was collected from the 15 cubic yard pile (STOCK-1) and analyzed for TCLP lead. A concentration of n 3.23 mg/l of leachable lead'was detected from this sample, indicating the 15 cubic yards pile of soil was J not a characteristically hazardous waste. Page 2 i I ~J O'Reilly, Talbot & Okun A S S 0_ Z- I - A T _E S - 1 - - - Soil Disposal On September 9, 1999, the 15 cubic yard stockpile was transported to the Northampton Landfill for use as daily cover under 'a Massachusetts Bill of Lading. The Bill of Lading is attached-in Appendix D. The 5 cubic yard pile was transported to Chem-Met Services, Inc. of Brownstown, Michigan for disposal in their hazardous waste landfill. A copy of the hazardous waste manifest showing this disposal is attached in Appendix D. Both Bill of Lading and hazardous waste manifest were signed by a representative of the City of Northampton as generator of the waste material. L Conclusions Based on the investigations and analytical test results described in this letter, lead impacted soil has been removed from the vicinity of the TP-1 location to levels below applicable Reportable Concentrations. Given that soils which exceed applicable reportable concentrations have been removed, no further actions are warranted under the MCP, other then maintenance of this documentation report for a period of five years as required under 310 CMR 40.0318. You should sign lJ section M of the last page of the original Bill Of Lading, and keep it with your records. , lJ It has been our pleasure to work with you on this project. Please feel free to call us if you have any questions or comments. Very truly yours, O'Reilly, Talbot & Okun Associates, Inc. 'y Bruce H. Nickelsen Kevin J. Reilly Associate Principal cc Wayne Feiden Attachments: Figures Tables Appendix A - Limitation Appendix B - Test Pit/Boring Logs Appendix C - Analytical Data Appendix D - Bill of Lading, Manifest u Page 3 1 ._J L_J n I "d O ~ J , ~ r i a ~ LJ ~~11 ~.l o. . I~ I y 0 C-1 0 C) O C) C> O ) M O 41 110. ~ r Cd N : 0 r ~ X ~ ~ 4 ` ~ ` 4 ' ~ 4 a o V! f, .J f1 ~ 71 f1 ~ ~J J ~ J ~J ( V ~ J Y 14. I cr, CO) p 41 Y O CD ~I U d N E att' o cd Q) ~i a O Z ' ~ d c N yy p o H o ' \r Z rd~ . r~r~~ ~i ` ~ di N d' , O O cd Y o o H p A J H y y 0 'b F, F+ p o l r 00. O C.i . O c) O p H H 1 ' z z z z z ~ z z a l o z V 'y , I - N Sr ~ry S ma N I7- y Y z :3 o 4 0 C, Ln 1-4 en 140. N l q e q y cc o p 14, - y o % . CC6 ~ ' y 1r d y cj C.1 .Sy Y ,Yi N U a Y _ql a ' z 41 -0 ~ Cd w 1 6 r _a ^y. L ' o. o o U ~ j I V-1 a P-4 C H. N m . H V U U . W Atwood Drive Northampton, Massachusetts Site Locus October 1999 re 1 i 51 ` Lt ~ % 1 u~ ~l lV 11 1l nti N 11~! I O'Reilly, Talbot & Okun Associates, Inc. I P S UNDEVELOPED r- ~-t I I 1 I I 1 L J *NOHO-1 LIMITED REMOVAL ACTION EXCAVATION i A T W O O D D R I V E LEG ND: FARMLAND - • • - PROPERTY LINE SAMPLE LOCATION -d~- MONITORING WELL LOCATION (163) TOTAL LEAD CONCENTRATIONS APPROXIMATE SCALEi V = 10' NOHO-8 (159) + SOIL DISPOSED OF AS HAZARDOUS NOHO_; WASTE 10.9) NOHO-5 (783)1: 4- Ai NOHO-9;=-;ih NON -103 (73.4):'.•`.;:2 (10. NOHp-7 6 :.a;::' (347):':.:::•3 NOHO-3 NOH13-101 (69) (69.0) L TNOHO-105 V (9,26) J j SOIL DISPOSED J AT LANDFILL + f NOHO-2 (163) THE INN AT ` ti', r~ n O'Reilly, Talbot & Okun _L - [ A S S 0 C-I A - T E S T 4-- 41CCMIEMMW LIMITATIONS 1. The observations presented in this report were made under the conditions described herein. The conclusions presented in this report were based solely upon the services described in the report and not on scientific tasks or procedures beyond the scope of the project or the time and budgetary constraints imposed by the client. U 2. In preparing the report O'Reilly, Talbot, Okun & Associates, Inc. relied on certain information provided by state and local officials and other- parties a referenced herein, and on information contained in the files of state or local regulatory agencies. Although there may have been some degree of overlap in the information provided by these sources, O'Reilly, Talbot, Okun & Associates, Inc. did not attempt to independently verify the accuracy or completeness of all information reviewed or received during the course of this assessment. 3. Observations were made of the site and of the structures on the site as indicated within the report. Where access to portions of the 'site or to structures on the site was unavailable or limited, we render no opinion as to the presence or hazardous. materials or oil, or to the presence of indirect information relating to hazardous materials or oil in that portion of the site. In addition, we render no opinion as to the presence. of hazardous materials or oil, where direct observations of portions a of the site where obstructed by objects or coverings on or over these surfaces. .4. Unless otherwise specified in the Report, we did not perform testing or analyses to determine the presence or concentration or concentration- of asbestos or polychlorinated biphenyls (PCBs) at the site or in the environment at the site. a 5. The purpose of this Report was to assess the physical characteristics of the subject site with respect to the presence of oil or hazardous material (OHM) in soil or groundwater at the site, and to assess risks associated with detected OHM, within the meaning of the Massachusetts Contingency Plan, 310 CMR. 40.0000. No specific attempt was made to check on the compliance of present or past owners ..or operators of the site with federal, state, or local laws and regulations, environmental or otherwise. 6. Risk assessment was performed in accordance with generally accepted practices of r government agencies and other consultants conducting similar characterizations. u The findings of the risk characterization are dependent on numerous assumptions and uncertainties inherent in the risk assessment process. Therefore, the findings rl of the risk assessment should not be interpreted as an absolute characterization of actual risks, but as general indicators highlighting potential sources of risk at the site. Although the range of uncertainty in the risk characterization has not (and j~ cannot) be quantified, the use of conservative assumptions throughout the process D D would be expected to err on the side of protection of human health and the L ' environment. D 7. Where analytical data or information regarding site environmental conditions was unavailable or limited, we render no opinion as to risks due to. oil or hazardous D materials in those portions of the site, or to oil or hazardous materials not tested for . 8. Our report was prepared for the exclusive benefit of our client. Reliance upon D the report and its conclusions is not extended to third parties or future property .owners. We acknowledge copies of our report may be submitted to DEP for D MCP compliance purposes. D . D D. _ D D D D _ D - D D D r . i O'Reilly, Talbot & Okun Associates, Inc. -PROJECT Test Pit No. TP-1 293 Bridge Street, Suite 500 Description: Atwood Drive Job No. 084-5-17 Springfield, Massachusetts. 01103 Location: Northhampton, MA Date: 06/23/98 (413)-788-6222 Engineer/Geologist: Bruce Nickelsen Contractor: Gary Guertin Ex. Ground Elev: Weather: Overcast, 70's Backhoe: Case 580 Start: 9:10 Capacity: 1/2 yard cubic yard Finish: 9:30 EXCAV. BOULDER PID DEPTH SOIL DESCRIPTION EFFORT COUNT REMARKS Brown Fine to Medium sand with some brick fragments.(Fill) 1 E None S-1 =ND 2.5' Sample S-1 collected from 0-2.5 feet None E' 5 Natural Brown Fine-Sand, trace silt. S-2, collected from 8' S-2 = ND 8.0 End of Exploration 10 . REMARKS: 1. Samples screened with TEI 580B Photoionization detecto r, referenced to parts per million(PPM) benzene in air. 2. Soil at 8' was moist. PLAN ;LEGEND EFFORT E = Easy M = Moderate i D = Difficult Vol. _ r-, OWEILLY, TALBOT & OKUNASSOCIATES, INC. ENVIRONMENTAL AND GEOTECHNICAL ENGINEERING CONSULTANTS LOG OF BORING NOHO -1 SHEET 1 OF 1 PROJECT Atwood Drive LOCATION Northhampton PROJECT NO. 84-05-17 DRILLING CONTRACTOR Seaboard FOREMAN Jeff N. DATE STARTED DATE FINISHED 12/18198 12/18/98 DRILLING EQUIPMENT B-53 COMPLETION DEPTH GROUND SURFACE ELEV. 24.0 DATUM TYPE BIT H.S.A. SIZE &TYPE OF CORE BARREL NO. SAW. 7 DIST. UNDIST. CASING 3" TIME FIRST COWL. HR. CASING HAMM. WEIGHT DROP WATER LEVEL (FTJ SAMPLER 21/4" Split Spoon BORING North 17 feet South of TP-I SAMPLER WEIGHT 140 pound DROP LOCATION HAMMER 30 inches ENGINEER/GEOLOGIST Melissa Schumacher SAMPLES SAMPLES DEPTH PENETR. REC. TYPE/ DESCRIPTION FIELD SOIL REMARKS FT. RESIST. IN. NO. MEASUREMENTS DESCRIPTION BL/6IN. 4/5/6/8 20" S-1 Medium, dense, brown, fine to medium SAND, trace silt, brick fragments. ND Fill 7/8/618 6" S-2 Medium, dense, brown, fine to medium SAND, trace medium, dense, ND 2.0 brown, silt and trace fine gravel. Fine to Medium 6/7/6/11 12" S-3 Medium, dense, brown, fine to medium SAND, trace medium, dense, ND Sand 5 brown, silt and trace fine gravel. 10/9/7/7 12" S4 Medium, dense, brown, fine to medium SAND, little, medium dense, ND brown, coarse SAND, trace silt, (moist). 10/12/16118 18" S-5 Medium, dense, brown, fine to medium SAND, little, medium, dense, ND brown, coarse SAND, trace silt, (moist). 10 16/14/18/11 18" S-6 Dense, brown, fine to medium SAND, trace dense brown SILT wet ND at 18.5. Bottom 2" wet, dense, brown, silty fine SAND. - 9/7/9111 20" S-7 Top 0.5 feet Medium, dense, little SILTY, fine SAND, (moist). ND (Watertasble 12.511) Bottom 1.5" Medium, dense, dark brown, silty, fine SAND, (saturated) Little, very stiff, dark brown, clay. 15 20 F 25 F Remarks: 1. Samples screened infield using TEI Model 580B referenced to PPM of Benzene in air. Readings in meter units."N.D." indicates none detected 4 2. Well set at 24', 10' of 2" PVC screening (24.0'-14.0'), I2' of filter sand (240-120- 10.0'- Ground Surface) 2' of bentonite (120-10.0'), PVC rising pipe 10' -N2 feet above ground surface, metal rising pi e (N 2 ft below ground surface to N 211 above ground surface). I I~ SPECTI4UNI ANALI'TiCAL, INC. Massachusetts Certification MA 138 L- Connecticut Approval No. PH 0777 New Hampshire ID No. 2538 New York ID No. 11393 Florida HRS87448 O'ReiUy, Talbot & Okun'.Assoc. July 9, 1998 293 Bzidge Street L Springfield, MA 01103 Attn: Bruce Nickelsen a Client Project No.: 784-0520 Location: Atwood Drive - Northampton, MA Lab ID No. Client ID AB10787 TP-1/S-1 Analysis Requeste Extractable 011 d Hydrocarbons Modified SW846 808118082 To tal Arseni c To tal Bari um Total Cadmium Total Chromi um To tal Lead n Total Mercury To to 1 Sel eni um LJ Total Silver AB10788 TP-41S-1 Extractable 011 Hydrocarbons n Modified SW846 • 8081/8082 Total Arsenic To tal Bari um Total Ca dmi um Total Chromi um Total Lead To tat Mercury Total Setenlum To tal S11 ver D AB10789 TP-5/S-1 Extractable 011. Hydrocarbons Modified SW846 808118082 Total Arsenic Total Bari um Total Cadmium Total Chromiurh Total Lead Total Mercury Continued next page i ENVIRONMENTAL ANALYSES - - - - - 1 l Almgren Drive --Agawam-) Massachusetts 01001- -413=789=9018 FAX-413=789-4076 - - - - - SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: TP-I/S-1 Location: Atwood Drive - Northampton, MA Lab ID No: ABI0787 Client Job No: J84-0520 Matrix: Soil Preservative: Refrigeration Collected: 06/23/98 by OTO Container: 1 Glass Soil Jar Received on 07/02/98 by DDR Condition of Sample as Received: Satisfactory QC and Data Review by Delivered by: Courier I~ LJ n Parameter PCB-1016 PCB-1221 PCB-1232 ~J PCB-1242 u PCB-1248 PCB-1254. a PCB-1260 nn Decachlorobiphenyl % ~J Solids, ~J i Polychlorinated Biphenyls (PCB's) Modified SW846 8081/8082 Result (ug/Kg) MI)L Extracted Analyzed Analyst Not detected 250 07/02/98 07/06/98 TO Not detected 250 07/02/98 07/06/98 TO Not detected 250 07/02/98 07/06/98 TG Not detected 250 07/02/98 07/06/98 TO Not detected 250 07/02/98 07/06/98 TO 750 250 07/02/98 07/06/98 TG Not detected 250 07/02/98 07/06/98 TG .73 07/02/98 07/06/98 TG 91.3 0.1 07/02/98 07/02/98 SEC SPECTRUM ANALY TICAL, INC. Laboratory Report Client ID: TP-1/S-1 Location: Atwood Drive - Northampton, MA Lab ID No.: AB10787 Client Job No.: J84-0520 Matrix: Soil Preservative: Refri eration Collected: 06/23/98 by OTO Container: 1 Glass Soil Jar Received on 07/02/98 by DDR Condition of Sample as Received: Satisfactory QC and Data Review by Delivered by: Courier Extractable Petroleum Hydrocarbons MA DEP Modified EPA 8270/8100 Parameter for AB10787 Results Aliphatics/Aromatics (mg/Kg) C9 - C18 Aliphatics Not detected C19- C36 Aliphatics Not detected C11- C22 Aromatics Not detected Targeted PAH's Analytes (ug/Kg) Acenaphthene Not detected Acenaphthylene Not detected Anthracene Not detected Benzo (a) anthracene Not detected Benzo (b) fluoranthene Not detected Benzo (k) fluoranthene Not detected Benzo (a) pyrene Not detected Benzo (g,h.i) perylene Not detected Chrysene Not detected Dlbenz (a,h) anthracene Not detected Fluoranthene Not detected Fluorene Not detected Indeno (1,2,3-cd) pyrene Not detected 2-Methylnaphthalene Not detected Naphthalene Not detected Phenanthrene Not detected Pyrene Not detected Surrogate Recovery(%) 1-Chloro-octadecane(%SR) 43 Ortho-Terphenyl(%SR) 42 % Solids 91.3 AIDL Extracted Analyzed Analyst 33 07/02/98 07/08/98 MB 33 07/02/98 07/08/98 MB 33 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 148.0 07/02/98 07/08/98 MB 07/02/98 07/08/98 MB 07/02/98 07/08/98 MB 0.1 07/02/98 07/02/98 . SEC I SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: TP-1/S-1 Location: Atwood Drive - Northampton, MA Lab ID No: AB10787 Client Job No: J84-0520 n Matrix: Soil Preservative: Refrigeration 1 Gl i1 J i Collected: 06/23/98 by OTO DDR 98 b 02 7 ass S0 ar Conta ner: le as Received: Satisfactor Condition of Sam y / Received on 0 / p y QC and Data Review by Delivered by: Courier Metals Parameter Result (mg/Kg) MDL Method Digested Analyzed . Analyst Total Arsenic nd 0.904 EPA 200.7 07/08/98 07/08/98 CR Total Barium 51.3 0.904 EPA 200.7 07/08/98 07/08/98. CR Total Cadmium nd 0.904 EPA 200.7 07/08%98 07/08/98 CR Total Chromium 13.8 Total Lead 347., 0.904 0.452 EPA 200.7 EPA 200.7 07/08/98 07/08/98 07108/98 07/08/98 CR CR Total Mercury nd 0.225 EPA 245.1 07/08/98 07/07/98 JM Total Selenium nd 0.452 EPA 200.7 07/08/98 07/07/98 CR Total Silver nd 1.81 EPA 200.7 07/08/98 07/07/98 CR LJ r~ u ~I v n CHAIN -T-- RECORD I, Page of SPECTRUM ANALYTICAL kOJECT NO.: REPORTTO: F-o ITE NAME: /zt '77 I` OCATION: STATES ~a ADDRESS: -9EFERENCE QUOTE NUMBER (RQN): CITY STATE ZIP IDURCHASE ORDER NO.: INVOICETO: PROJECT Mgr:f1 3AMPLER(s): CITY STATE ZIP SAMPLE TYPE & MATRIX CODES: C ONT AIN ERS VO C's SVO C's T PH METALS O THER 1 ^I = 40C 2 = HCI 3 = H2SO4 4 = HNO3 5 = OTHER o -Total W o z ~ TCLP h= co CM co o m m __J ¢ o N co o ¢ . COMPOSITE G = GRAB CL W > 2 L.U a M U O ¢ J N N N N W N CL. ¢ a~ D -1 =AQUEOUS 3=SLUDGE 5 =OTHER 9 ¢ Cn . m N = N 2 =SOIL 4=SEDIMENT X w J W m ¢ o r o o N o o ~ v ' CL W M co m co w cn H V) E - ~ co (n W J LAB USE Q Q o- ° o o o cc in Z0 ~ 0 0 c - l az - - ONLY SAMPLE I.D. DATE r - A'A 12 c z t 21 1 -'z ISHED BY: RECEIVED Bl° DATE TIME SPECIAL INSTRUCTIONS: SPECIAL HANDLING' Please El 4 1 Return Sample after Analysis check ~I~, r~ ' •a 1± ~;a iryl I ,i~~i,;fj_1~ ❑ Dispose of Sample after 60 days Standard TAT - 7 to 10 Business days j 61& ❑ Special TAT-24 hr-48 hr-72hr-5b. days ' :TAT begins when sample is received attest facility. ~ . Y ,,/y 1~';.~' bN. 2. ! Y • TAT for samples reed after 3 pm will begin on the next business day. • Ail TAT s are subject to laboratory approval and customer consent. f ❑ Fax results when available to ) DATE RESULTS NEEDED: 11 Almgren Drive -Agawam, Massachusetts 01001 0 413-789-9018 • Fax 413-789-4076 I SPECTRUM ANALYTICAL, DIC, Massachusetts Certification MA 138 Connecticut Approval No. PH 0777 New Hampshire ID No. 2538 New York ID No. 11393 Florida HRS87448 O'Reilly, Talbot & Okun Assoc.. 293 Bridge Street Springfield, MA 01103 Attn: Bruce Nickelsen Client Project No.: J0840517 Tab ID No. AB29056 AB29057 AB29058 AB29059 AB29060 AB29061 Client ID NOHO-2 NOHO-5 NOHO-3 NOHO- 7 NOHO-9 NOHO-10 AB29062 AB290 63 AB290 64 AB29065 AB29066 AB29067 AB29068 NOHO-11 NOHO-12 NOHO-13A NOHO-13B NOHO-14 NOHO-15 NOHO-16 December 30, 1998 Location: Atman - Northampton lvsi Total Lead Total Lead Total Lead Total Lead Total Lead Total Lead Extractable Oil Hydrocarbons Modified SW846.8082 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 Total Leach Extractable Oil Flydrocarbons Modified SW846 8082 Total Lead Extractable Oil Hydrocarbons Modified SW846`8082 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 Total. Lead Extractable Oil Hydrocarbons Modified SW846 8082 Total Lead Extractable Oil Hydrocarbons Continued next page . ENVIRONMENTAL ANALYSES - - 11 AlmgresDrive- Agawam;-Massachusetts-01001--• 413-789-9018 FAX-413-7894070 Lab TD No. Client ID AB290 68 1vOHO-16 AB290 69 NOHO-l 7 a AB290 70 NOHO-l 8 II Analysis Requested Modified SW846 8082 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 Total Lead Extractable Oil Hydrocarbons Modified SW846 8082 uth rized y ani1 ayeh v ENVIRONMENTAL ANALYSES Preside t ry Director f HAImgren-D-rive •-Agawam; Massachusetts-01001---413-789-901-8-•--Fi1X413-789-4076 - - - - SPECTRUM ANALYTICAL, I NC. Laboratory Report I Client ID: NOHO-2 Location: Atman - Northampton Lab ID No: AB29056 Client Job No: J0840517 Matrix: Soil Preservative: Refrigeration Collected: 12/18/98 by OTO Container: 1 Clear Glass Jar Received on 12/21/98 by MBR Condition of Sample as Received: Satisfactory QC and Data Review by Delivered by: Client I Total Lead n EPA Method 6010/200.7 Parameter result (mg/Kg) XML Digested Analyzed Analyst Total Lead 163 0.449 12/29/98 12/30/98 DMM lJ i SPECTRUM ANALYTICA., INC. Laboratory Report Client ID: NOHO-3 Lab ID No: AB29058 Matrix: Soil Collected: 12/18/98 by OTO Received on 12/21/98 by MBR QC and Data Review by l_l Location: Atrnan - Northampton Client Job No: J0840517 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by: Client Total Lead n EPA Method 6010/200.7 L n Parameter Result (mg/Kg) u NII)L Digested Analyzed Analyst 0.464 12/29/98. 12/30/98 DMM SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHO-5 Location: Atman - Northampton Lab ID No: AB29057 Client Job No: J0840517 Matrix: Soil Preservative: Refrigeration Collected: 12/18/98 by OTO Container: 1 Clear Glass Jar Received on 12/21/98 by MBR Condition of Sample as Received: Satisfactory n QC and Data Review by Delivered by: Client L-.l -J Total Lead EPA Method 6010/200.7 Parameter Result (mg/Kg) MDL Digested Total Lead 783 0.455 12/29/98 Analyzed 12/30/98 Analyst DMM SPECTRUM ANALYTICAL, INC. Laboratory Report F1 Client ID: NOHO-7 Lab ID No: AP29059 Matrix: Soil Collected: 12/18%98 by OTO Received on 12/21/98 by MBR ~l QC and Data Review by Location: Ataman - Northampton Client Job No: J0840517 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by: Client Total Lead EPA Method 6010/200.7 n Parameter Result (mg/Kg) MDL 0.558 Digested 12/29/98 Analyzed Analyst 12/30/98 DMM SPECTRUM ANALYTICAL INC. r , Laboratory Report D Client ID: N®H- ®-9 I Location: Atman -Northampton Lab ID No: AB29060 Client Job No: J0840517 Matrix: Soil Preservative: Refrigeration J Collected: 12/18/98 by OTO Container: 1 Clear Glass Jar Received on 12/21/98 b y MBR Condition of Sample as Received: Satisfactory QC and Data Review by Delivered by: Client D Total Lead EPA Method 6010/200.7 Parameter r Result (mg/Kg) M DL Digested Analyzed Analyst D Total Lead . 47.2 0.458 12/29/98 12/30/98 DMM D - D - D D , D D D } D I A ^ y ° rn m o , Z b o E7 U 1 ~ V ' y1 U O ~ "C7 ti O b i~ h G 'd N t( E y 9 O U O a I, o z a Y2d o z o Hdo z a a cis y OWaidJO # sszif) Injo JO #--N U s E~ N U a ~I v Z V W O E~ ~ O rx z , a STIR `dory JO # Hd anr~Sniasa.zd add - s, ~ . O z H o r ~ x Z t 1, Z II 00 ;i t. ~ 'a ; G ~q ~ ...r as ~e b I~ ~4 "Gy I L__I i C F1 L~ Fl I I a ti w° b o ° x °ZC3 O J_. ~ ~ C C o Q; b N Q N O ❑ ❑ o • S~ vOi L." 03 O N z (97 O U % c a n r C-0 V orbs'eid JO # ssalo MID JO # ® ` Z o U ssL'IJ Ia9.uTV'.IO # o sI'gIA VOA JO # Hd ~ anRBnaasaid xilmw ® 0 0CUL E 0 o z a N (D cd ~ x r Q r7 j W ~ o o C z Cd A b M ~ a DO y F Cf) CZ 0 U bu a U ~ r R!v: P-1 qvs te'''a - pw3 N r'c TJ U U R C a SPECTRUIVI,ANALYTICAL, C. i Massachusetts Certification M-MA 138 Connecticut Approval # PH 0777 Rhode Island # 98 & Maine # n/a n New Hampshire ID # 2538 New York ID #11393 Florida HRS87448 ~ O'Reilly, Talbot & Okun Assoc. January 11, 1999 L_] 293 Bridge Street Springfield, MA 01103 Attn: Bruce Xickelsen L_.J Client Project No.: J840517 Location: Atwood Drive LJ Lab ID No. Client ID An ysis Requested AB29697 1VOHO-1 EPA Method 8260 Extractable Oil Hydrocarbons Soluble Lead volatile Petroleum Hydrocarbons ~I AB29698 1VOHO-l0. volatile Petroleum Hydrocarbons U EPA Method 8260 Extractable Oil Hydrocarbons Soluble Lead Ell If V Director I ENVIRONMENTAL ANALYSES i - 11 Alzngren Drive Agawati,-MassachusettsOl001 = 41-3=789-9018 • -FAX 413=789-4076-- - - - - - - E 0 L L~ SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: N0H0-1 Lab ID No: AB29697 Matrix: Ground Water Sampled on12/28/98 by OTO Received on 12/28/98 by MBR QC and Data Review by AM Parameter for AB29697 Location: Atwood Drive Client Job No.: J340517 Preservative: Refrigeration, HCl Container : 2 VOA Vials Condition of Sample as Received: Satisfactory Delivered by: Client Volatile Organics EPA Method 8260 Result (ug/L) N ML Analyzed Analyst Benzene Not detected 1.0 01/09/99 SN Bromobenzene Not detected 1.0 01/09/99 SN Bromochloromethane Not detected 1.0 01/09/99 SN Bromodichloromethane Not detected 1.0 01/09/99 SN Bromoform Not detected 1.0 01/09/99 SN Bromomethane Not detected 1.0 01/09/99 SN n-Butylbenzene Not detected 1.0 01/09/99 SN sec-Butylbenzene Not detected 1.0 01/09/99 SN tert-Butylbenzene Not detected 1.0 01/09/99 SN Carbon tetrachloride Not detected 1.0 01/09/99 SN Chlorobenzene Not detected 1.0 01/09/99 SN Chloroethane Not detected 1.0 01/09/99 SN Chloroform Not detected 1.0 .01/09/99 SN Chloromethane Not detected 1.0 01/09/99 SN 2-Chlorotoluene Not detected 1.0 01/09/99 Sri 4-Chlorotoluene Not detected 1.0 01/09/99 SN 1,2-Dibromo-3-chloropropane Not detected 1.0 01/09/99 SN Dibromochloromethane Not detected 1.0 01/09/99 SN 1,27Dibromoethane (EDB) Not detected .1.0 01109/99 SN Dibromomethane Not detected 1.0 01/09/99 SN 1,2-Dichlotobenzene Not detected 1.0 01/09/99 SN 1,3-Dichlorobenzene Not detected 1.0 01/09/99 SN 1,4-Dichlorobenzene Not detected 1.0 01/09/99 SN Dichlorodifluoromethane Not detected 1.0 01/09/99 SN 1,1-Dichloroethane Not detected 1.0 01/09/99 SN 1,2-Dichloroethane Not detected 1.6 01/09/99 SN 1,1-Dichloroethene Not detected 1.0 01/09/99 SN cis-1,2-Dichloroethene Not detected 1.0 01/09/99 SN trans-1,2-Dichloroethene Not detected 1.0 01/09/99 SN 1,2-Dichloropropane Not detected 1.0 01/09/99 SN 1,3-Dichloropropane Not detected 1.0. 01/09/99 SN 2,2-Dichloropropane Not detected 1.0 01/09/99 SN 01/09/99 SN 1,1-Dichloropropene Not detected 1.0 cis-1,3-Dichloropropene Not detected 1.0 01/09/99 SN Continued next page - - - - - - - - r Volatile Organics EPA Method 8260 Parameter for AB29697 Result (ug/L) M DL Analyzed Analyst trans-1,3-Dichloropropene Not,detected 1.0 01/09/99 sN Ethylbenzene Not detected 2.0 01/09/99 SN Hexachlorobutadiene Not detected 1.0 01/09/99 SN Isopropylbenzene Not detected 1.0 01/09/99 SN 4-Isopropyltoluene Not detected 1.0 01/09/99 SN Methylene chloride Not detected 1.0 01/09/99 sN Naphthalene Not detected 4.0 01/09/99 SN n-Propylbenzene Not detected 1.0 01/09/99 SN Styrene Not detected 1.0 01/09/99 SN 1,1,1,2-Tetrachloroethane Not detected 1.0. 01/09/99 SN 1,1,2,2-Tetrachloroethane Not detected 1.0 01/09/99 SN Tetrachloroethene Not detected 8.0 01/09/99 sN Toluene Not detected 3.0 01/09/99 SN 1,2,3-Trichlorobenzene Not detected 1.0 01/09/99 SN 1,2,4-Trichlorobenzene Not detected 1.0 01/09/99 SN 1,1,1-Trichloroethane Not detected 1.0 01/09/99 SN 1,1,2-Trichloroetharie Not detected 1.0 01/09/99 SN Trichloroethene Not detected 1.0 01/09/99 SN Trichlorofluoromethane Not detected 1.0 01/09/99 SN 1,2,3-Trichloropropane Not detected 1.0 01/09/99 SN 1,2,4-Trimethylbenzene Not detected 4.6 01/09/99 SN 1,3,5-Trimethylbenzene Not detected 2.0 01/09/99 SN m,p-Xylenes Not detected 2.0 01/09/99 SN o-Xylene Not detected .1.0 01/09/99 SN Vinyl chloride Not detected 1.0 01/09/99 SN Methyl-t-butyl ether Not detected 2.0 01/09/99 SN BFB Surrogate Recovery 99 01109/99 SN p-DFB Surrogate Recovery 103 01/09/99 SN CLB-d5 Surrogate Recovery 97 01/09/99 SN Parameter for AB29697 Aliphatics/Aromatics (mg(L) C5-C8 Aliphatic Hydrocarbons C9-C12 Aliphatic Hydrocarbons C9-C10.Aromatic Hydrocarbons Unadjusted C5-C8 Aliphatics Unadjusted C9-C12 Aliphatics n _ Client ID: NOHO-A : AB29697 b ID No L l . a Matrix: Ground Water l Collected: 12/28/98by o'ro Target VPH Analytes (ug/L) Benzene Ethylbenzene Methyl-tert-butylether Naphthalene Toluene M,p-Xylenes ' o-Xylene Received: 12/28/98by MBR Volatile Petroleum Hydrocarbons MADEP VPH 97-12 11 I J H Dilution Factors Carbon Chain Dilution Factor Target Analytes Dilution Factor Location:. Atwood Drive Client Job No.: J840517 Preservative: Refrigeration, HCl Container: 2 VOA Vials Condition of Sample as Received: See Attached Sheet Results MDL Analyzed Analyst Not detected 0.150 01/09/99 SN Not detected 0.050 01/09/99 SN Not detected 0.050 01/09/99 SN Not detected 0.150 01/09/99 SN Not detected 0.050 01/09/99 ISN Not detected 5.0 01/09/99 SN Not detected 5.0 01/09/99 SN Not detected 5.0 01/09/99 SN Not detected . 5.0 01/09/99 SN Not detected 5.0 01/09/99 SN Not detected 5.0 01/09/99 SN Not detected 5.0 01/09/99 SN 1 01/09/99 SN 1 01/09/99 SN NA 01/09/99 SN NA 01/09/99 SN 118 01/09/99 SN 106 01/09/99 SN Surrogate Recoveries 2,5-Dibromotoluene PID (%SR) 2,5-Dibromotoluene FID (%SR) 2,5-Dibromotoluene GCMS (%SR). 4-Bromofluorobenzene GCMS (%SR) D i i_ Were all QA/QC procedures required bythe VPH method followed? Yes No Were all performance/acceptance standards for required QA/QC procedures achieved? Yes -C No Were any significant modifications made to the VPH method, as specified in Section 11.3? Yes* * If yes is answered to above question, then this sample was run via GCMS using all VPH method specified QC criteria. I attest the ma SPECTRUM ANALYTICAL, INC. Laboratory Report of those individuals immediately responsible for obtaining the information, :k-ij, to the best of my knowledge and belief, accurate and complete. 01/11/99 SPECTRUM ANALYTICAL, INC. Client ID: NOHO-1 Location: Atwood Drive I Lab ID No.: AB29697 Client Job No.: J840517 Matrix: Ground Water Preservative: Refrigeration/HN03 Collected: 12/28/98by OTO Container: 1 Amber / 1 Plastic Received: 12/28/98by MBR Condition of Sample as Received: See Attached Sheet Extractable Petroleum Hydrocarbons n MADEP EPH 98-1, SW846 3510C Separatory Funnel Liquid-Liquid Extraction Parameter forAB296.97 L Results lAIDL Extracted Analyzed Analyst ) Aliphatics/Aromatics (mg/ C9-C18 Aliphatic Hydrocarbons Not detected 0.2 12/30/98 01/03/99 KS C19-C36 Aliphatic Hydrocarbons Not detected 0.2 12/30/98. 01/03/99 KS C11-C22 Aromatic Hydrocarbons Not detected 0.2 12/30/98 01/03/99 KS Unadjusted C11-C22 Aromatics Not detected 0.2 12/30/98 01/03/99 KS j LJ Diesel PAH Analytes (ug/L) Naphthalene Not detected 10.0 12/30/98 01/03/99 KS .2-Methylnaphthalene Not detected 10.0 12/30/98 01/03/99 KS Phenanthrene Not detected 10.0 12/30/98 01/03/99 KS a Acenaphthene Not detected 10.0 12/30/98 01/03/99 KS Other Target PAR Analytes (ug/L) Acenaphthylene Not detected 10.0 12/30/98 01/03/99 KS u u Anthracene Not detected. 10.0 12/30/98 01/03/99 KS Benzo (a) anthracene Not detected 10.0 12/30/98 01/03/99 KS Benzo (a) pyrene Not detected 10.0 12/30/98 01/03/99 KS Benzo (b) fluoranthene Not detected 10.0 .12/30/98 01/03/99 KS Benzo (g,h,i) perylene Not detected 10.0. 12/30/98 01/03/99 KS Benzo (k) fluoranthene Not detected 10.0 12/30/98 01/03/99 KS Chrysene - Not detected 10.0 12/30/98 01/03/99 KS Dibenzo (a,h) anthracene Not detected 10.0 12/30/98 01/03/99 KS LJ ~l Fluoranthene Not detected 10.0 12/30/98 01/03/99 KS Fluorene Not detected 10.0 12/30/98 01/03/99 KS Indeno (1,2,3-cd) pyrene Not detected 10.0 12/30/98 01/03/99 KS Pyrene Not detected 10.0 12/30/98 01/03/99 KS J Dilution Factors Carbon Chain Dilution Factor 1 12/30/98 01/03/99 KS l Target Analyte Dilution Factor 1 12/30/98 01/03/99 KS Parameter forA B29697 Results AML Extracted Analyzed Analyst Surrogate Recoveries 1-Chloro-octadecane Aliphatic (%SR) 82 Ortho-Terphenyl Aromatic (%SR) 62 2-Bromonaphthalene Fractionation (%SR) 43 2-Fluorobiphenyl Fractionation (%SR) 51 12/30/98 01/03/99 KS 12/30/98 01/03/99 KS 12/30/98 01/03/99 KS 12/30/98 01/03/99 KS J Were all QA/QC procedures required by the EPH method followed? Yeses No Were all performance/acceptance standards for required QA/QC procedures achieved? Yes C-, No Were any significant modifications made to the EPH method, as specified in Section 11.3? Yes*-C_,-No * If yes answered to above question, the aromatic hydrocarbons from C11- C22 along with target PAH analytes were performed via GC/MS following all EPH method specified QC criteria. I attest that based upf n m inquiry -of those individuals immediately responsible for obtaining the information, J the materi cont ' d in' s repo is to the best of my knowledge and belief, accurate and complete. 01/11/99 l Pres en b to Director I - - i i SPECTRUM ANALYTICAL, INC. l J Laboratory Report Client ID: NOHO-1 Location: Atwood Drive ' Lab ID No: AB29697 Client Job No: J840517 i J Coll cted Ground 28/98at by OTO Container: 1 Amb g/ 1 Plastic Received on 12/28/98 by MBR Condition of Sample as Received: Satisfactory n QC and Data Review by Delivered by: Client U Soluble Lead EPA Method 200.7 Result (mg/L) MDL nd 0.005 Extracted Analyzed Analyst 01/04/99 01/06/99 DMM • ~I 1, I s . a. a 0 N 7y ;c .C a C/1 y d a r 11 6 l mow: vi . . o u r ` 00 . C 00 CD W `'L r-- CD N i "C 77 ~.j 11 1 -;1 d - CD C) V a N N u O ~ x CD ty O N Type o Matrix Preservative pH # Of VOA Vials ~t Z # Of Amber Glass .0 0 # Of Clear Glass # Of Plastic y ® I 1 1 0 w v' 1 V on 0' b 7 0 x 0 w Y o > O 1 I o O O E W N 0. ' Z p •~~-•~-i~ W ~ Cp cau w CD G'• O ¢ a o ~ ~ .q w a 0 Cp . y y co ~ a co y w 0- SPECTRUM ANALY71CAL, VC, massachusetts certif=don M-MA 133 ` Connecticut Approval # PH 0979 Rhodo Island *199 & Maine nAa Igcw Hampshirc ID # 2533 flew York ID # 11393 J Florida. X97448 ®'Rciffy, Talbot & Okun Assoc. .February 3, 1.999 293 Bddsc Street . U Spzingffcld, MA 01103 Arm: Brucc Xickelsezz J Client Project No.: 30840537 Location-, At=an -Northampton TCLP Zeatd Y l ~resi, bosa't®~ igec u ENVIRONMENTii,i+ AMALYSES _ _ii_Almen~~av~ Agawa~a, hiassacbusetts0i001 413-789-X618 ° FA~4f3 799-076 a o---- t,d c~i ZJ 66, d qaj SPECTRUM ANALYTICAL, INC. Laboratory Report (Subcontracted Analysis) Chew M: NOHO-S Lab ID No: AB29057 1Nlatria: Snail ~Ilei1: 12118/98 by e3T0 Rec6vedon12/2119$ by MBR CSC and Data R.-miew by AM Parameter Location: At=aa - Northampton Client Job No: J0840517 Preservative, Refri eration Container: 1 Cleat lass Jar Condition of Saffipie as Received: Satisf=ory ]Delivered icy: Cent TCLP Lead EPA Method 1311/5W846 6010 Result (M) iL UP 0010 n TCLF Lead lJ L L_J u G U L~ ZO'd ~Z;L~ 66b qaj acucj Analyzed Analyst 02/01/99 02103/99 CR 1 I1 fI I D D U 11 0 J I I Spectrum Analytical, Inc, Laborstory Rep®rt Supplement Re ereaise Methods for the Detgimination of Organic Cornpouuds in Drinking Water. EPA-60014-381039. EMSL 1983. Methods for Chemical Analysis 6f Water aridVastes. EPA 60014-79-020. EMI SL 1983_ Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA 60014-92-057. EMSL 19'91 Test Methods for Evaluating Solid Waste. Physical/Chernical Methods. ]EPA SW-846. 1986. standard Methods for the Exam? matinon of Water and Wastes. APRA-AWWA-V4PCP• 16ih- Edidon. 1935. Standard Methods for Comparison of waterborne: Petroleum Oils by Gas Chromatography. ASTM D 3323. 1982. Oil Spill Identification System. U-$. Coast Guard CG-13-52-77. 1977. Handbook for Analytical Quality Control in Water and Wastewater Laboratories. EPA 600/4-79-019_ EMSL 1979. Choosing Cast-Effective QAtQC (Quality Assurance/Quality Control) Programs for Chemical Anslyses. EPA 600/4-35/056. EMSL 1955. Re rt Notations Not Detected, - The compound Was not detected at a concentration equal to or above Not Det, ND or nd, the established method detection limit. NC = Mot Calculated MCI:. . = EPA maximum Contamination Level VOA = VolratileOrganic Analysis BFB _ 4-Bromofluorobeneene (Ara EPA 624 ,Saarrogate) (Ara EPA 624 Surrogate) p_-pFB = 1,4-Difluorobenzene = L:hlorobenzene-d5 (Art EPA 624 Surrogate) CLIP-d5 gCp 2-Promo-1=chloropropeane (An EPA 601 Surrogate) T = a,a,a-Trifluororoluene (An EPA 602 Surrogate) Decachlorobiphenyl - (an EPA 60818080 Surrogate) Defini ns Surrogate Recovery The recovery (expressed as a percent) of a non-method analyte (see surrogates listed above) added to the sample for the purpose of monitoring system performance. Matrix Spike Recovery e The recovery (expressed as a percent) of method analyses added to the sample for the purpose of determining any effect of sample composition on analyte recovery. Laboratory Replicate = Two, sample aliquots taken in the analytical laboratory and analyzed separately with. identical procedures. Analyses of laboratory duplicates give a measure of the preceision associated with laboratory procedures, but not with sample collection, preservation, or storage procedures. d ntifical circumstances measure Field Duplicate = Two separate samples collected at the same time and place treated exactly the same throughout field and laboratory procedures. Analysis of Field P gag of the precision associated with sample collection, preservaton and storage.. as well as with laboratory procedures. Relative Percent Difference RFD) = The precision measurement obtained on duplicate/replicate analyses. %RPD is calculated as: ooPPD va.-lu-e ,+ue2-3lO1000/6 / 20 V qa~ I 'J n 0 LJ 3 j ~a y x S ~1 •da u ~ - s I o 1 u ~ Q4 ~ ~ N N ' Flo ~ q Lf O o n 0 u u x O alive OA Vials ~ fl ear Glass astic o Co Q fd C CCD ti b 1 I N PC O Q a O ~ m -v ° CD y y Vl (0 Po 'd 97l : LZ 66, V Qaj J Mamaohuwtts Cortifieation M-MA 131 Cosnwticbat Approval # PH 0777 Rhode Island # 98 & Maine a n/a 14ow Hampshire ID 2539 New York M ##11393 Florida HRS87448 O'Reilly, Taalbof & ®kun Assoc. January S, 15999 295 1 zidgs: ,S'imvi . S,,zsdngfield, MA 01193 Attn: Bruce Nickelson Client Project No.: 30840517 Location: Atwood AB29860 NOHO-8 Wiabo 'r Presiarce, ENS'IRONKFN7AL ANALYSES I1 AlmgnnUriec ^ Agawam,Aiassacfiusefisi}TOiiT-~ 413=789=90f8-°-FfiX-41:3'=7tsiJ=40'tb- TO' d .200* ON TS: VT 66, SO u*et :-131 I SPECTRUM ANALYTIC.,, INC. Laboratory Report Client ID: NOM-8 Lab III No: 29860 Matrix: Soil 1 Collected: 12118/98 by OTO Received on 12/31 j98 by MMBR QC and Data Review by L_1 Location: Atwood Cheidt Job No: JUS40517 Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Satisfactory Delivered by: Client Total Lead EPA Method 50101200.7 Parameter Result (mom) Total bead 159 LJ u J ZO' d 200 * oN ZS:17T 66, SO uet MUL 0.470 Digested Analyzed Analyst 01/04/98 0.1/05/99 DMM f :-131 i Spectrum Anslydcal, Inc. Laboratory Report Saapplea'eaat Methods for the Determination of Organic Compounds in Drinking Water. EPA-600/4-1351039. EMSL 1988. !Methods for Chemical Analysis of Water and Wastes. FPA 60014-79-020. EMSL 1953. Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA 64014.82-057. EMSL 19112. qL Test Methods for Evaluating Solid Waste. PhysicaliChermical Methods. EPA SW 546. 1956. Standard Methods for the Examinatinon of Water and Wastes. APIA-AWWA-WPCF. 16th Edition_ 1935. Standard Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography. ASTM D 3328. 1982. ~J Oil Spill Identification System. U.S. Coast Guard CCs-D-52-77. 1977. Handbook for Analytical Quality Control in `'Mater and Wastewater Laboratories- EPA 60014.79-019. EMSL 1979. a Choosing Cost Effective QA/QC (Quality Assura=JQuality Control) Programs for Chemical Analyses. EPA 60014-351056. EMSL 1985. n ~nrt Notations Ll Not Detected, = The compound was not defected at a concentration equal to or above Not Det, ND or nd the established method detection limit. NC Nos Calculated MCL EPA 1bl=imum Contamination Level VOA = Volatile Organic Analysis 13F33 m 4-Br°omofluorobenzene (An EPA 624 Surrogate) p-DFl3 1,4,Diffuorobenzene (An EPA 624 Surrogate) CLB-d5 = Chlorobenzene-dS (An .SPA. 624 Surrogate) I~ 13CP _ 2-.Eromo-l-chloropropane (An EPA 601 Surrogate) u TFT a ga-Tri uarotoluene (An EPA 602 Surrogate) Decachlerobiphenyl = (an EPA 60818080 Surrogate) Surrogate Recover, = The recovery (expressed as a percent) of a non-method analyte (see surrogates listed J above) added to the sample for the purpose of monitoring system performance. Matrix Spike Recovery The recovery (expressed as a percent) of method analytes added to the sample for the purpose of determining any effect of sample composition on analyte recovery. Laboratory Replicate = Two sample aliquots taken. in the analytical laboratory and analyzed separately with J identical procedures. Analyses of laboratory duplicates give a measure of the precession associated with laboratory procedures, but not with sample collection, preservation, or storage procedures. Field Duplicate _ Two separate samples collected at the same time and place under identifrcal circumstances and J treated exactly the same throughout Reid and laboratory procedures. Analysis of Field duplicates give a measure of the precision associated with sample collection, prcgervaton and storage, as well as with laboratory procedures. Relative Percent Difference IUD) =The precision measurement obtained on duplicate/replicate anatlyses. J %RPD is calculated as: %R]?D Umlmcl -uhL 0 300% ave. value - 10'd 200 ON ZS: VT 66,S0 uPf :-131 i IiI ca e~. a a~ w O G se W V L 1.V ~r I oil -n d? c . r, r e w M o p ~ 6 ae 9 I M. ' w A ~ 0 r9 o pA i Typo C Q, Matn Presmative pH # Of VOA Vials ~ # Of Amber Glass # Of Clear Glass . # Of Plastic 40 6 ® ~1 j n ~ 0 61 R ~ 3: V/ ~ Q 1 z y , V0'd 200 ON 2S: VT 66,S0 upr :-131 I 1~ SPECTRUM ANALYTICAL, INC. Massachusetts Certification M-MA 138 Connecticut Approval # PH 0777 Rhode Island 98 & Maine # n/a New Hampshire ID # 2538 LJI New York ID # 11393 Florida HRS87448 O'Reilly, Talbot & Okun Assoc. L_1 293 Bridge Street Springfield, MA 01103 Attn: Bruce Nickelsen Client Project No.: J084 Location: Atwood Lab ID No. Client ID AB32346 NOHO-101 AB32348 NOHO-103 - AB32350 NOHO-105 AB32353 NOHO-108 AB32356 NOHO-11 [U-1 AB32390 u I Li `J NOHOCOMP Analysis Rec Total Lead Total Lead Total Lead Total Lead February 3, 1999 Conductance . 'EPA Method 8260 TPH by GC EPA Method 8270 Conductance EPA Method 8260 TPH by GC EPA Method 8270 tho ed b aniba ` h Preside L a or Director ENVIRONMENTAL ANALYSES - i~ - - -11 Almgren Drive Agawam, Massachusetts` 01001 -4-1-3489=9018 • TAX-413=789-4076- SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHO-101 Location: Atwood Lab ID No: AB32346 Client Job No: J084 l_l Matrix: Soil Preservative: Refrigeration Collected: 01/29/99 by OTO Container: 1 Clear Glass Jar. Received on 01/29/99 by MBR Condition of Sample as Received: Satisfactory QC and Data Review by Delivered by: Client lJ n L 1 7 i L_ Parameter Total Lead D ~J H n n ~l i F-1 U . IJ Total Lead EPA Method 6010/200.7 Result (mg/Kg) MDL Digested Analyzed Analyst 69.9 0.454 02/02/99 02/03/99 CR r~ SPECTRUM ANALYTICAL, INC. Laboratory Report n Client ID: NOHO-103 Location: Atwood Lab ID No: AB32348 Client Job No: J084 I__ 1 Matrix: Soil Preservative: Refrigeration Collected: 01/29/99 by OTO Container: 1 Clear Glass Jar Received on 01/29/99 by MBR Condition of Sample as Received: Satisfactory QC and Data Review by Delivered by: Client l_ L1 -1 Parameter u Total Lead L~ I L L~ u Total Lead EPA Method 6010/200.7 Result (mg/Kg) XML 10.2 0.454 Digested Analyzed Analyst 02/02/99 02/03/99 CR SPECTRUM ANALYTICAL, INC. Laboratory Report ~J Client ID: NOHO-105 Location: Atwood. Lab ID No: AB32350 Client Job No: J084 L ..l Matrix: Soil Preservative: Refrigeration Collected: 01/29/99 by OTO Container: 1 Clear Glass Jar Received on 01/29/99 by MBR Condition of Sample as Received: Satisfactory n QC and Data Review by Delivered by: Client SPECTRUM ANALYTICAL, INC. J Laboratory Report n l Client ID: NOHO-108 Location: Atwood n Lab ID No: AP32353 Client Job No: J084 `---I Matrix: Soil Preservative: Refrigeration Collected: 01/29/99 by OTO Container: 1 Clear Glass Jar Received on 01/29/99 by MBR Condition of Sample as Received: Satisfactory QC and Data Review by Delivered by: Client l1 l~ 1 Parameter Total Lead LJ J Total Lead EPA Method 6010/200.7 Result (mg/Kg) MDL Digested Analyzed 10.9 0.447 02/02/99 02/03/99 Analyst CR n SPECTRUM ANALYTICAL, INC. Laboratory Report J Client ID: NOHO-11 Location: Atwood Lab ID No.. AB32356 Client Job No.: J084 Matrix: Soil Collected: 01/29/99 b OTO Received on 01/29/99 by NOR QC and Data Review by Preservative: Refrigeration Container : 3 Clear Glass Jars Condition of Sample as Received: Satisfactory Delivered by: Client Semivolatile Organics EPA Method 8270 Parameter for AB32356 Result (ug/Kg) MDL Extracted Analyzed Analyst Acenaphthene Not detected 151.0 02/02/99 02/03/99 KS Acenaphthylene Not detected 151.0 02/02/99 02/03/99 KS Anthracene Not detected 151.0 02/02/99 .02/03/99 KS Benzidine Not detected 151.0 02/02/99 02/03/99 KS Benzoic acid Not detected 755.0 02/02/99 02/03/99 KS Benzo (a) athracene Not detected 151.0 02/02/99 02/03/99 KS Benzo (b) fluoranthene , Not detected 151.0 02/02/99 02/03/99 KS Benzo (k) fluoranthene Not detected 151.0 02/02/99 02/03/99 KS Benzo (g,h,i) perylene Not detected 151.0 02/02/99 02/03/99 KS Benzo (a) pyrene Not detected 151.0 02/02/99 02/03/99 KS Benzyl alcohol Not detected 302.0 02/02/99 02/03/99 KS Bis (2-chloroethoxy) methane Not detected 151.0 02/02/99 02/03/99 KS Bis (2-chloroethyl) ether Not detected 151.0 02/02/99 02/03/99 KS Bis (2-chloroisopropyl) ether Not detected 151.0 02/02/99 02/03/99 KS Bis (2-ethylhexyl) phthalate Not detected 1510.0 02/02/99 02/03/99 KS 4-Bromophenyl phenyl ether Not detected 151.0 02/02/99 02/03/99 KS Butyl benzyl phthalate Not detected 151.0 02/02/99 02/03/99 KS 4-Chloroaniline Not detected 302.0 02/02/99 02/03/99 KS 2-Chloronaphthalene Not detected 151.0 02/02/99 02/03/99 KS 4-Chloro-3-methylphenol Not detected 302.0, 02/02/99 02/03/99 KS 2-Chlorophenol Not detected 151.0 02/02/99 02/03/99 KS 4-Chlorophenyl phenyl ether Not detected 151.0 02/02/99 02/03/99 KS Chrysene Not detected 151.0 02/02/99 02/03/99 KS Dibenz (a,h) anthracene Not detected 151.0 02/02/99 02/03/99 KS Dibenzofuran Not detected 151.0 02/02/99 02/03/99 KS Di-n-butylphthalate Not detected 151.0 02/02/99 02/03/99 KS 1,3-Dichlorobenzene Not detected 151.0 02/02/99 02/03/99 KS 1,4-Dichlorobenzene Not detected 151.0 02/02/99 02/03/99 KS 1,2-Dichlorobenzene Not detected 151.0 02/02/99 02/03/99 KS 3,3'-Dichlorobenzidine Not detected 302.0 02/02/99 02/03/99 KS Continued next page.. Parameter for AB32356 Result (ugWg) MDI. . Extracted. Analyzed Analyst. 2,4-Dichlorophenol Not detected 151.0 02/02/99 02/03/99 KS 2,6-Dichlorophenol Not detected 151.0 02/02/99 02/03/99 KS Diethyl phthalate Not detected 151.0 02/02/99 02/03/99 KS 2,4-Dimethlylphenol Not detected 151.0 02/02/99 02/03/99 KS 4,6-Dinitro-2-methylphenol Not detected 755.0 02/02/99 02/03/99 KS 2,4-Dinitrophenol Not detected 755.0 02/02/99 02/03/99 KS 2,4-Dinitrotoluene Not detected 151.0 02/02/99 02/03/99 KS 2,6-Dinitrotoluene Not detected 151.0 02/02/99 02/03/99 KS 1,2-Diphenylhydrazine Not detected 151.0 02/02/99 02/03/99 KS Di-n-Propylnitrosoamine Not detected 151.0 02/02/99 02/03/99 KS Fluoranthene Not detected 151.0 02/02/99 02/03/99 KS Fluorene Not detected 151.0 02/02/99 02/03/99 KS Hexachlorobenzene Not detected 151.0 02/02/99 02/03/99 KS Hexachlorobutadiene Not detected 151.0 02/02/99 02/03/99 KS Hexachlorocyclopentadiene Not detected 151.0 02/02/99 02/03/99 KS Hexachloroethane Not detected 151.0 02/02/99 02/03/99 KS Indeno (1,2,3-cd) pyrene Not detected 151.0 02/02/99 02/03/99 KS Isophorone Not detected 151.0 02/02/99 02/03/99 KS 2-Methylnaphthalene Not detected 151.0 02/02/99 02/03/99 KS 2-Methylphenol (0-cresol) Not detected 151.0 02/02/99 02/03/99 KS 4-Methylphenol (p-cresol) Not detected 151.0 02/02/99 02/03/99 KS Naphthalene Not detected 151.0 02/02/99 02/03/99 KS 2-Nitroaniline Not detected 755.0 02/02/99 02/03/99 KS 3-Nitroaniline Not detected 755.0 02/02/99 02/03/99 KS 4-Nitroaniline Not detected 755.0 02/02/99 02/03/99 KS Nitrobenzene Not detected 151.0 02/02/99 02/03/99 KS 2-Nitrophenol Not detected 151.0 02/02/99 02/03/99 KS 4-Nitrophenol Not detected 755.0 02/02/99 02/03/99 KS N-Nitrosodimethylamine Not detected 151.0 02/02/99 02/03/99 KS N-Nitrosodiphenylamine Not detected 151.0 02/02/99 02/03/99 KS Pentachlorophenol Not detected 755.0 02/02/99 02/03/99 KS Phenanthrene Not detected 151.0 02/02/99 02/03/99 KS Phenol Not detected 151.0 02/02/99 02/03/99 KS Pyrene Not detected 302.0 02/02/99 .02/03/99 KS 1,2,4-Trichlorobenzene Not detected 151.0 02/02/99 02/03/99 KS 2,4,5-Trichlorophenol Not detected 151.0 02/02/99 02/03/99 KS 2,4,6-Trichlorophenol Not detected 151.0 02/02/99 02/03/99 KS Pyridine Not detected 151.0 02/02/99 02/03/99 KS Dimethyl phthalate Not detected 151.0 02/02/99 02/03/99 KS Di-n-octyl phthalate Not detected 151.0 02/02/99 02/03/99 KS n SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHO-11 Location: Atwood Lab ID No.: AB32356 Client'Job No.: J084 Matrix: Soil Collected: 01/29/99 by OTO Received on 01/29/99 by MBR n QC and Data Review by Preservative: Refrigeration Container: 1 Clear Glass Jar Condition of Sample as Received: Delivered by: Client Satisfactory Volatile Organics EPA Method 8260 Parameter for AB32356 Result (ug/Kg) MDL Extracted Analyzed Analyst Benzene Not detected 31.8 02/02/99 02/02/99 CD Bromobenzene Not detected 31.8 02/02/99 02/02/99 CD Bromochloromethane Not detected 31.8 02/02/99 02/02/99 CD Bromodichloromethane Not detected 31.8 02/02/99 02/02/99 CD Bromoform Not detected 31.8 02/02/99 02/02/99 CD n-Butylbenzene Not detected 31.8 02/02/99 02/02/99 CD sec-Butylbenzene Not detected 31.8 02/02/99 02/02/99 CD tert-Butylbenzene Not detected 31.8 02/02/99 02/02/99 CD Carbon tetrachloride Not detected 31.8 02/02/99 02/02/99 CD Chlorobenzene Not detected .31.8 02/02/99 02/02/99 CD Chloroform Not detected 31.8 02/02/99 02/02/99 CD 2-Chlorotoluene Not detected 31.8 02/02/99 02/02/99 CD 4-Chlorotoluene Not detected 31.8 02/02/99 02/02/99 CD 1,2-Dibromo-3-chloropropane Not detected 31.8 02/02/99 02/02/99 CD Dibromochloromethane Not detected 31.8 02/02/99 02%02/99 CD 1,2-Dibromoethane (EDB) Not detected 31.8 02/02/99 02/02/99 CD Dibromomethane Not detected 31.8 02/02/99 02/02/99 CD 1,2-Dichlorobenzene Not detected 31.8 02/02/99 02/02/99 CD 1,3-Dichlorobenzene Not detected 31.8 02/02/99 02/02/99 CD 1,4-Dichlorobenzene Not detected 31.8 02/02/99 02/02/99 CD 1,1-Dichloroethane Not detected 31.8 02/02/99 02/02/99 CD 1,2-Dichloroethane Not detected 31.8 02/02/99 02/02/99 CD 1,1-Dichloroethene Not detected 31.8 02/02/99 02/02/99 CD cis- 1,2-Dichloroethene Not detected 31.8 02/02/99 02/02/99 CD trans-1,2-Dichloroethene Not detected 31.8 02/02/99 02/02/99 CD 1,2-Dichloropropane Not detected ` 31.8 02/02/99 02/02/99 CD 1,3-Dichloropropane Not detected 31.8 02/02/99 02/02/99 CD 2,2-Dichloropropane Not detected 31.8 02/02/99 02/02/99 CD -l Continued next page.. Parameter for AB32356 result (ug/Kg) MDL Extracted Analyzed ' Analyst n l 1,1-Dichloro ro ene P p Di hl i Not detected N t d t t d 31,8 31 8 02/02/99 02/02/99 CD ~l oropropene c c s-1,3- e ec e o . 02/02/99 02/02/99 CD trans-1,3-Dichloropropene Not detected 31.8 02/02/99 02/02/99 CD Ethylbenzene Not detected 31.8 02/02/99 02/02/99 CD Hexachlorobutadiene Not detected 63.6 02/02/99 02/02/99 CD n Isopropylbenzene Not detected 31.8 02/02/99 02/02/99 CD 4-Isopropyltoluene Not detected 31.8 02/02/99 02/02/99 CD Methylene chloride l h h Not detected t N t d t d 31.8 63 6 02/02/99 02/02/99 CD ene t a Nap ec e e o . 02/02/99 02/02/99 CD n-Propylbenzene Not detected 31.8 02/02/99 02/02/99 CD Styrene Not detected 31.8 02/02/99 02/02/99 CD 1,1,1,2-Tetrachloroethane Not detected 31.8 02/02/99 02/02/99 CD n 1,1,2,2-Tetrachloroethane Not detected 31.8 02/02/99 02/02/99 CD l J Tetrachloroethene Not detected 31.8 02/02/99 02/02/99 CD Toluene z b Not detected N d t t d 31.8 63 6 02/02/99 02/02/99 CD en ene 1,2,3-Trichloro e ec e ot . 02/02/99 02/02/99 CD 1,2,4-Trichlorobenzene Not detected 63.6 02/02/99 02/02/99 CD 1,1,1-Trichloroethane Not detected 31.8 02/02/99 02/02/99 CD 1,1,2-Trichloroethane Not detected 31.8 02/02/99 02/02/99 CD Trichloroethene Not detected 31.8 02/02/99 02/02/99 CD Trichlorofluoromethane Not detected 31.8 02/02/99 02/02/99 CD a 1,2,3-Trichloropropane h lb Not detected d N d t t . 31.8 31 8 02/02/99 02/02/99 CD enzene y 1,2,4-Trimet ot e ec e . 02/02/99 02/02/99 CD 1,3,5-Trimethylbenzene Not detected 31.8 02/02/99 02/02/99 CD m,p-Xylenes Not detected 63.6 02/02/99 02/02/99 CD o-Xylene Not detected 31.8 02/02/99 02/02/99 CD Methyl-t-butyl ether Not detected 31.8 02/02/99 02/02/99 CD BFB Surrogate Recovery % 104 104 02/02/99 02/02/99 CD ) p-DFB Surrogate Recovery ( 02/02/99 02/02/99 CD CLB-d5 Surrogate Recovery 100 02/02/99 02/02/99 CD J % Solids 86.4 0.1 02/03/99 02/03/99 CD J r 1 SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHO-11 Location: Atwood Lab ID No.: AB32356 Client Job No.: J084 Matrix: Soil Preservative: Refrigeration Collected: 01/29%99 by OTO Container: 3 Clear Glass Jars Received on 01/29/99 by NOR Condition of Sample as Received: Satisfactory f j QC and Data Review by Delivered by: Client Total Hydrocarbons by GC Modified EPA Method 8100 LLI Parameter Result (mg/Kg) AML Extracted Analyzed Analyst Total Hydrocarbons (GC) Not detected 02/02/99 02/02/99 LR i L - _ Fingerprint based quantiiicaton: Gasoline Not detected 40 02/02/99 02/02/99 LR Fuel Oil #2 Not detected 40 02/02/99 02/02/99 LR l Fuel Oil #4 Not detected 40 02/02/99 02/02/99 LR J Fuel Oil #6 Not detected 80 02/02/99 02%02/99 LR Motor Oil Not detected 80 02/02/99 02/02/99 LR M Ligroin Not detected 40 02/02/99 02/02/99 LR Aviation Fuel Not detected 40 .02/02/99 02/02/99 LR ~F Other Oil Not detected N d t d t 80 02/02/99 02/02/99 02/02/99 02/02/99 LR LR Unidentified e ec e ot ~Ll % Solids , 86.4 0.1 02/03/99 02/03/99 CD Petroleum identification is determined by comparing the GC fingerprint obtained from the sample with a library of GC fingerprints obtained from petroleum products. Possible match categories are as follows; Gasoline - includes regular, unleaded, premium, etc. Fuel Oil #2 - includes home heating oil, #2 fuel oil and diesel. Fuel Oil #4 - Includes #4 Fuel Oil. Fuel Oil #6 - includes #6 oil and bunker "C" oil. Motor Oil - includes virgin and waste automobile. Ligroin - includes mineral spirits, petroleum naphtha, vm&p naphtha. Aviation Fuels - includes Kerosene, Jet A and JP-4. Other Oil - includes lubricating and cutting oil and silicon oil. n Factors such as microbial degradation, weathering and solubility generally prevent specific identification J within a petroleum category. A finding of "unidentified" means that the sample fingerprint was characteristic of a petroleum product, but could not be matched to a fingerprint in the library. After fingerprint identification, the amount present in the sample is quantified using a calibration curve prepared from a petroleum product of the same category as the identified petroleum. Unidentified petroleum is quantified using a petroleum calibration that approximates the distribution of compounds in the sample. A * in the results column indicates the petroleum calibration used to quantify unidentified samples. n !I l _I SPECTRUM ANALYTICAL, INC. Laboratory Report (Subcontracted Analyses) Client ID: N0110-11 Lab ID No: AB32356 Matrix: Soil Collected: 01/29%99 by OTO Received on 01/29/99 by MBR QC and Data Review by Location: Atwood Client Job No: J084, Preservative: Refrigeration Container: 3 Clear Glass Jars Condition of Sample as Received: Satisfactory Delivered by: Client ~J Parameter Conductance L_J L_ J II LJ J I j~II Wet Chemistry Analyses . Result 1VIDL Units 20 1.0 umhos/cm Method S205/E120.1 Start Date Analyst 02/01/99 PX i SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHOCOMP Location: Atwood Lab ID No: AB32390 Client Job No.: J084 J Matrix: Soil Preservative: Refrigeration Collected: 01/29/99 b OTO Container : 2 Amber Glass Jars Received on 01/29/99 by MBR Condition of Sample as Received: Satisfactory n QC and Data Review by Delivered by: Client LI Semivolatile Organics EPA Method 8270 Parameter for AB32390 Result (ug/Kg) MDL Extracted Analyzed Analyst Acenaphthene Not detected 144.0 02/02/99 02/03/99 KS L Acenaphthylene Not detected 144.0 02/02/99 02/03/99 KS Anthracene Not detected. 144.0 02/02/99 02/03/99 KS Benzidine Not detected 144.0 02/02/99 02/03/99 KS Benzoic acid . Not detected 720.0 02/02/99 02/03/99 KS Benzo (a) anthracene Not detected 144.0 02/02/99 02/03/99 KS Benzo (b) fluoranthene Not detected 144.0 02/02/99 02/03/99 KS Benzo (k) fluoranthene Not detected 144.0 02/02/99 02/03/99 KS Benzo (g,h,i) perylene Not detected 144.0 02/02/99 02/03/99 KS Benzo (a) pyrene Not detected 144.0 02/02/99 02/03/99 KS Benzyl alcohol Not detected 288.0 02/02/99 02/03/99 KS Bis (2-chloroethoxy) methane Not detected 144.0 02/02/99 02/03/99 KS Bis (2-chloroethyl) ether Not detected 144.0- 02/02/99 02/03/99 KS Bis (2-chloroisopropyl) ether Not detected 144.0 02/02/99 02/03/99 KS Bis (2-ethylhexyl) phthalate Not detected 144.0 02/02/99 02/03/99 KS 4-Bromophenyl phenyl ether Not detected 144.0 02/02/99 02/03/99 KS Butyl benzyl phthalate Not detected 144.0 02/02/99 02/03/99 KS 4-Chloroaniline Not detected 288.0 02/02/99 02/03/99 KS 2-Chloronaphthalene Not detected 144.0 02/02/99 02/03/99 KS 4-Chloro-3-methylphenol Not detected 288.0 02/02/99 02103/99 KS 2-Chlorophenol Not detected 144.0 02/02/99 02/03/99 KS 4-Chlorophenyl phenyl ether Not detected 144.0 02/02/99 02/03/99 KS ~J Chrysene Not detected 144.0 02/02/99 02/03/99 KS Dibenz (a,h) anthracene Not detected 144.0 02/02/99 02/03/99 KS Dibenzofuran Not detected 144 .0 02/02/99 02/03/99 KS Di-n-butylphthalate Not detected 144.0 02/02/99 02/03/99 KS 1,3-Dichlorobenzene Not detected 144.0 02/02/99 02/03/99 KS J 1,4-Dichlorobenzene Not detected 144.0 02/02/99 02/03/99 KS 1,2-Dichlorobenzene Not detected 144.0 02/02/99 02/03/99 KS 3,3'-Dichlorobenzidine Not detected 288.0 02/02/99 02/03/99 KS Continued next page.. Parameter for AB32390 Result (uWKg) AML Extracted Analyzed Analyst 2,4-Dichlorophenol Not detected 144.0 02/02/99 02/03/99 KS 2,6-Dichlorophenol Not detected 144.0 02/02/99 02/03/99 KS Diethyl phthalate Not detected 144.0 02/02/99 02/03/99 KS 2,4-Dimethlylphenol Not detected 144.0 02/02/99 02/03/99 KS 4,6-Dinitro-2-methylphenol Not detected 720.0 02/02/99 02/03/99 KS 2,4-Dinitrophenol Not detected 720.0 02/02/99 02/03/99 KS 2,4-Dinitrotoluene Not detected 144.0 02/02/99 02/03/99 KS 2,6-Dinitrotoluene Not detected 144.0 02/02/99 02/03/99 KS 1,2-Diphenylhydrazine Not detected 144.0 02/02/99 02/03/99 KS Di-n-Propylnitrosoamine Not detected 144.0 02/02/99 02/03/99 KS Fluoranthene Not detected 144.0 02/02/99 02/03/99 KS Fluorene Not detected 144.0 02/02/99 02/03/99 KS Hexachlorobenzene Not detected 144.0 02/02/99 02/03/99 KS Hexachlorobutadiene Not detected 144.0 02/02/99 02/03/99 KS Hexachlorocyclopentadiene Not detected 144.0 02/02/99 02/03/99 KS Hexachloroethane Not detected 144.0 02/02/99 02/03/99 KS .Indeno (1,2,3-cd) pyrene Not detected 144.0 02/02/99 02/03/99 KS Isophorone Not detected 144.0 02/02/99 02/03/99 KS 2-Methylnaphthalene Not detected. 144.0 02/02/99 02/03/99 KS 2-Methylphenol (0-cresol) Not detected 144.0 02/02/99 02/03/99 KS 4-Methylphenol (p-cresol) Not detected 144.0 02/02/99 02/03/99 KS Naphthalene Not detected. 144.0 02/02/99 02/03/99 KS 2-Nitroaniline Not detected 720.0 02/02/99 02/03/99 KS 3-Nitroaniline Not detected 720.0 02/02/99 02/03/99 KS 4-Nitroaniline Not detected 720.0 02/02/99 02/03/99 KS Nitrobenzene Not detected 144.0 02/02/99 02/03/99 KS 2-Nitrophenol Not detected 144.0 02/02/99 02/03/99 KS .4-Nitrophenol Not detected 720.0 02/02/99 02/03/99 KS N-Nitrosodimethylamine Not detected. 144.0 02/02/99 02/03/99 KS N-Nitrosodiphenylamine Not detected 144.0 02/02/99 02/03/99 KS Pentachlorophenol Not detected 720.0 02/02/99 02/03/99 KS Phenanthrene Not detected 144.0 02/02/99 02/03/99 KS Phenol Not detected 144.0 02/02/99 02/03/99 KS Pyrene Not detected 288.0 02/02/99 02/03/99 KS 1,2,4-Trichlorobenzene Not detected 144.0 02/02/99 02/03/99, KS 2,4,5-Trichlorophenol Not detected 144.0 02/02/99 02/03/99 KS 2,4,6-Trichlorophenol Not detected 144.0 02/02/99 02/03/99 KS Pyridine Not detected 144.0 02/02/99 02/03/99 KS Dimethyl phthalate Not detected 144.0 02/02/99 02/03/99 KS Di-n-octyl phthalate Not detected 144.0 02/02/99 02/03/99 KS SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHOCOMP Location: Atwood Lab ID No.: AB32390 Client Job No.: J084 Matrix: Soil Preservative: Collected: 01/29/99 by OTO Container: Received on 01/29/99 by MBR Condition of Sample as Received: Satisfactory n QC and Data Review by Delivered by: Client Volatile Organics EPA Method 8260 Parameter for AB32390 Result (ug/Kg) AML Extracted Analyzed Analyst Benzene Not detected 6.1 02/02/99 02/02/99 CD Bromobenzene Not detected 6.1 02/02/99 02/02/99 CD Bromochloromethane Not detected 6.1 02/02/99 02/02/99 CD Bromodichloromethane Not detected 6.1 02/02/99 02/02/99 CD Bromoform Not detected 6.1 02/02/99 02/02/99 CD n-Butylbenzene Not detected 6.1 02/02/99 02/02/99 CD sec-Butylbenzene Not detected 6.1 02/02/99 02/02/99 CD tert-Butylbenzene Not detected 6.1 02/02/99 02/02/99 CD Carbon tetrachloride Not detected 6.1 02/02/99 02/02/99 CD Chlorobenzene Not detected . 6.1 02/02/99 02/02/99 CD Chloroform Not detected 6.1 02/02/99 02/02/99 CD 2-Chlorotoluene Not detected 6.1 02/02/99 02/02/99 CD 4-Chlorotoluene Not detected 6.1 02/02/99 02/02/99 CD 1,2-Dibromo-3-chloropropane Not detected 6.1 02/02/99 02/02/99 CD Dibromochloromethane Not detected 6.1 02/02/99 02/02/99 CD 1,2-Dibromoethane (EDB) Not detected 6.1 02/02/99 .02/02/99 CD Dibromomethane Not detected 6.1 02/02/99 02/02/99 CD 1,2-Dichlorobenzene Not detected 6.1 02/02/99 02/02/99 CD 1,3-Dichlorobenzene Not detected 6.1 02/02/99 02/02/99 CD 1,4-Dichlorobenzene Not detected 6.1 02/02/99 02/02/99 CD 1,1-Dichloroethane Not detected 6.1 02/02/99 02/02/99 CD 1,2-Dichloroethane Not detected 6.1 02/02/99 02/02/99 CD 1,1-Dichloroethene Not detected 6.1 02/02/99 02/02/99 CD cis-1,2-Dichloroethene Not detected 6.1 02/02/99 02/02/99 i CD trans-l,2-Dichloroethene Not detected 6.1 02/02/99 02/02/99 CD 1,2-Dichloropropane Not detected 6.1 02/02/99 02/02/99 CD j 1,3-Dichloropropane Not detected 6.1 02/02/99 02/02/99 CD 2,2-Dichloropropane Not detected 6.1 02/02/99 02/02/99 CD 4 Continued next page.. Parameter for AB32390 Result (ug/Kg) MDL Extracted Analyzed Analyst 1,1-Dichloropropene Not detected 6.1 02/02/99 02/02/99 CD cis-1,3-Dichloropropene Not detected 6.1 02/02/99 02/02/99 CD trans-1,3-Dichloropropene Not detected 6.1 02/02/99 02/02/99 CD Ethylbenzene Not detected 6.1 02/02/99 02/02/99 CD Hexachlorobutadiene Not detected 6.1 02/02/99 02/02/99 CD Isopropylbenzene Not detected 6.1 02/02/99 02/02/99 CD 4-Isopropyltoluene Not detected 6.1 02/02/99 02/02/99 CD Methylene chloride Not detected 6.1 02/02/99 02/02/99 CD Naphthalene Not detected 6.1 02/02/99 02/02/99 CD n-Propylbenzene Not detected 6.1 02/02/99 02/02/99 CD Styrene Not detected 6.1 02/02/99 02/02/99 CD 1,1,1,2-Tetrachloroethane Not detected 6.1 02/02/99 02/02/99 CD 1,1,2,2-Tetrachloroethane Not detected 6.1 02/02/99 02/02/99 CD Tetrachloroethene Not detected 6.1 02/02/99 02/02/99 CD Toluene Not detected 6.1 02/02/99 02/02/99 CD 1,2,3-Trichlorobenzene Not detected 6.1 02/02/99 02/02/99 CD 1,2,4-Trichlorobenzene ' Not detected 6.1 02/02/99 02/02/99 CD 1,1,1-Trichloroethane Not detected 6.1 02/02/99 02/02/99 CD 1,1,2-Trichloroethane Not detected_ 6.1 02/02/99- - - 02/02/99 CD Trichloroethene Not detected 6.1 02/02/99 02/02/99 CD Trichlorofluoromethane Not detected 6.1 02/02/99 .02/02/99 CD 1,2,3-Trichloropropane Not detected . 6.1 02/02/99 02/02/99 CD 1,2,4-Trimethylbenzene. Not detected 6.1 02/02/99 02/02/99 CD 1,3,5-Trimethylbenzene Not detected 6.1 02/02/99 02/02/99 CD m,p-Xylenes Not detected 12.2 02/02/99 02/02/99 CD o-Xylene Not detected 6.1 02/02/99 02/02/99 CD Methyl-t-butyl ether Not detected 6.1 02/02/99 02/02/99 CD BFB Surrogate Recovery % 101 105 02/02/99 02/02/99 CD ) p-DFB Surrogate Recovery ( 02/02/99 02/02/99 CD CLB-d5 Surrogate Recovery 98 02/02/99 02/02/99 CD % Solids 89.7 01 02/03/99 02/03/99 GMM U n J - - - - SPECTRUM ANALYTICAL, INC. Laboratory Report Client ID: NOHOCOMP Location: Atwood Lab ID No.: AB32390 Client Job No.: J084 Matrix: Soil Preservative: Refrigeration Collected: 01/29%99 by OTO Container: 2 Amber Glass Jars Received on 01/29/99 by MBR Condition of Sample as Received: Satisfactory QC and Data Review by Delivered by: Client Total Hydrocarbons by GC L-A Modified EPA Method 8100 Parameter Result (mg/Kg) MDL Extracted Analyzed Analyst Total Hydrocarbons (GC) Not detected 02/02/99 02/02/99 LR Fingerprint based quantificaton: a Gasoline Not detected 40 02/02/99 02/02/99 LR Fuel Oil #2 Not detected 40 02/02/99 02/02/99 LR I~1 Fuel Oil #4 Not detected 40 02/02/99 02/02/99 LR I~ Fuel Oil #6 Not detected 80 02/02/99 02/02/99 LR Motor Oil Not detected 80 02/02/99 02/02/99 LR Ligroin Not detected 40 02/02/99 02/02/99 LR ~J . Aviation Fuel Not detected 40 02/02/99 02/02/99 LR Other Oil Not detected 80 02/02/99 02/02/99 LR Unidentified Not detected 02/02/99 02/02/99 LR 1 % Solids 89.7 0.1 02/03/99 02/03/99 GMM Petroleum identification is determined by comparing the GC fingerprint obtained from the sample with a library of GC fingerprints obtained from petroleum products. Possible match categories are as follows; 11 Gasoline - includes regular, unleaded, premium, etc. L Fuel Oil #2 - includes home heating oil, #2 fuel oil and diesel. Fuel Oil #4 - Includes #4 Fuel Oil. Fuel Oil #6 - includes #6 oil and bunker "C" oil. u Motor Oil - includes virgin and waste automobile. Ligroin - includes mineral spirits, petroleum naphtha, vm&p naphtha. Aviation Fuels - includes Kerosene, Jet A and JP-4. Other Oil - includes lubricating and cutting oil and silicon oil. Factors such as microbial degradation, weathering and solubility generally prevent specific identification within a petroleum category. A finding of "unidentified" means that the sample fingerprint was characteristic of a petroleum product, but could not be matched to a fingerprint in the library. After fingerprint identification, the amount present in the sample is quantified using a calibration curve prepared from a petroleum product of the same category as the identified petroleum. Unidentified petroleum is quantified using a petroleum calibration that approximates the distribution of compounds in the sample. A * in the results column indicates the petroleum calibration used to quantify unidentified samples. SPECTRUM ANALYTICAL, INC. l Laboratory Report (Subcontracted Analyses) Client ID: NOHOCOMP Location: Atwood Lab ID No: AB32390 Client Job No: J084 Matrix: Soil Preservative: Refrigeration Collected: 01/29%99 by OTO Container: 2 Amber Glass Jars Received on 01/29/99 by MBR Condition of Sample as Received: Satisfactory r~ QC and Data Review by Delivered by: Client Wet Chemistry Analyses Parameter Result MDL Units Method Start Date Analyst n Conductance 56 1.0 umhos/cm S205/E120.1 02/01/99 PX LJ U J D f Spectrum Analytical, Inc. Laboratory Report Supplement - References Methods for the Determination of Organic Compounds in Drinking Water. EPA-600/4-88/039. EMSL 1988. Methods for Chemical "Analysis of Water arid Wastes. EPA 600/4-79-020. EMSL 1983. i Methods for Organic Chemical Analysis of Municipal and Industrial Wastewater. EPA 600/4-82-057. EMSL 1982. Test Methods for Evaluating Solid Waste. Physical/Chemical Methods. EPA SW-846. 1986. Standard Methods for the Examinatinon of Water and Wastes. APHA-AWWA-WPCF. 16fh-Edition. 1985. Standard Methods for Comparison of Waterborne Petroleum Oils by Gas Chromatography. ASTM D 3328. 1982. u Oil Spill Identification System. U.S. Coast Guard CG-D-52-77. 1977. _J Handbook for Analytical Quality Control in Water and Wastewater Laboratories. EPA 600/4-79-019. EMSL 1979. Choosing Cost-Effective QA/QC (Quality Assurance/Quality Control) Programs for Chemical Anslyses. EPA 600/4-85/056. a EMSL 1985. Report Notations D Not Detected, = The compound was not detected at a concentration equal to or above Not Det, ND or nd the established method detection limit. NC = Not Calculated MCL EPA Maximum Contamination Level VOA Volatile Organic Analysis BFB 4-Bromofluorobenzene : (An EPA 624 Surrogate) p-DFB _ 1,4-Diuorobenzene (An EPA 624 Surrogate) CLB-d5 Chlorobenzene-di (An EPA 624 Surrogate) BCP = 2-Bromo-l-chloropropane (An EPA 601 Surrogate) TFT = a,a,a-Triuorotoluene (An EPA 602 Surrogate) Decachlorobiphenyl (an EPA 60818080 Surrogate) Definitions U Surrogate Recovery = The recovery (expressed as a percent) of a non-method analyte (see surrogates listed above) added to the sample for the purpose of monitoring system performance. Matrix Spike Recovery = The recovery (expressed as a percent) of method analytes added to the sample for the I~ purpose of determining any effect of sample composition on analyte recovery. Laboratory Replicate = Two sample aliquots taken in the analytical laboratory and analyzed separately with identical procedures. Analyses of laboratory duplicates give a measure of the preceision associated with laboratory procedures, but not with sample collection, preservation, or storage procedures. Field Duplicate = Two separate samples collected at the same time and place under identifical circumstances and treated exactly the same throughout field and laboratory procedures. Analysis of Field duplicates give a measure of the precision associated with sample collection, preservaton and storage, as well as with laboratory procedures. r-1 Relative Percent Difference RPD) = The precision measurement obtained on duplicate/replicate analyses. %RPD is calculated as: .%RPD (valuel - value2) * 100° o aver value_ i ❑ ~~ss lb yy t!I yy td w GI G7 vi ty O II II o d `"o CD 7y co o moo - CD " Ch Z CD ua < m ) o rn 7 v C ( 1 .a CD Y CD O cn a r u. - z o - cr% x o _ z o CD - Type o - cr Matrix. i P i ~ rese vat ve o - I A pH # Of VOA Vials _ p ~ o F # Of Amber Glass Z o 6-1 Gl O ass f Clear # # Of Plastic ; Z C 0 y y 104 ~ ~a g0CCrlS~3 ~ i • ❑ OO tQ y 2 1, r 0. > Y a 'C, w 0 d H n ? v O N J ° C CCD o 'rI, fD . . . . tom. a s a. o r ...y. ..FQ. . ..r . ~.p1.. . 3~.. . ?~j.. . r r` : . . Z w ° y _ 4, E G r _ i Z r 9 /0 OJ O vcu, CrD y c dCD UQ o rv co ` ^ CD w p, - y a 1114 v v v p d b 7y o ~ 1Cd W 0 g 0- W pppp CD pp o 0 p O A C l cu O p .A. 1 0 H~ ~ p W II ma y. N 0 t•4 H ° Type o ® Matrix p ~ Preservative ro pH # Of VOA Vials o # Of Amber Glass z o e ar Glass # Of Cl . y # Of Plastic Cn 17' C. `C Z C 0 z yd rC• f ~ ! ~ 1 - .C ~ ~ CAD ~ • e ❑ ❑ _ ~ - T 0 > 1 F+ a y C8 g t > e 1, H y• a u y CD ° , 4 c~'o w. ~ d . o I ION C D a CD . . . . . . a o CD - A' En r:3 Co QA T En h I i l __1 l_1 a 0 SPECTRUM ANALYTICAL, INC. Massachusetts Certification M-MA 138 Connecticut Approval # PH 0777 Rhode Island # 98 & Maine n/a New Hampshire ID # 2538 New York ID #11393 Florida HRS87448 O'Reilly, Talbot & Okun 293 Bridge Street, Suite 500 Springfield, MA 01103 June 2, 1999 Client Project No.: 84-05-17 Location: Atwood Drive - Northampton, MA Lab ID No. Client ID AB44666 STOCK-1 J Analysis Requested TCLP Lead ENVIRONMENTAL ANALYSES Almgren Drive Agawam; Massachusetts 01001-c,-413--789-9018----FA-X-413-789-4076- - - - - - - SPECTRUM ANALYTICAL, INC. Laboratory Report (Subcontracted Analysis) Location: Atwood Drive - Northampton, MA Client Job No: 84-05-17 L_ Client-ID: STOCK-1 n Lab ID No: AP44666 J Matrix: Soil Collected: 05/27/99 by OTO Received on 05/27/99 by KC j QC and Data Review by MD Lll Parameter 1 TCLP Lead 1 IJ n. !I Preservative: Refrigeration Container: 1 Amber Glass Condition of Sample as Received: Satisfactory Delivered by: Client TCLP Lead EPA Method 1311/SW846 6010 Result (mg/L) 3.23 MDL Extracted Analyzed 0.010 06/01/99 06/02/99 Analyst CR J II X ~t i CD y e=t C o . ■ ~c- c: , a O W 5 N ~ ~ {c 0 - C C D V~~ `.C I y ~ a (~l v z ~ ~ ~ O ~ t7 b 04 II n rt H O''' d ~ N y 4 CI) Cf R, C 0 N CD C ) 0 3 a ~ ; O G A Cp, II ` ~ \ A+ CD• ~ w O G II CD O C3 C ~ x b J p z O Type Matrix Preservative pH # Of VOA Vials # Of Amber Glass o Z # Of Clear Glass 9. # Of Plastic a m CD ...1.......1....... 0 0 n Z I ~J n o ~d CD o ~n C/) o C4 -d 0 CD 0 . 0 z 0 ry D W .gyp z o I All ' ❑ - ~ C) N ~ ~r ( , r - b , ,y C I I 0 y y ` ~ y 0 ~6' - 2 t ID R ~ O O J O (D CD 0 O r'~' ' SD ~J ~ y p CD 0 c i - CD & i ~ CD K 1, 0 ° a. 0 a I:r a CD c CD < a Massachusetts Department of Environmental Pratectlon Bureau of Waste Site Cleanup SILL OF LADING (Pursuant to ago cMR ao.aoao) >JRA A. LOCATION OF SITE OR DISPOSAL SITE WHERE. REMEDIATION WASTE WAS GENERATED: Release Name (optional): Street: Atwood Driye ...Location Aid: End of Cul-de-sac City/Town: Northampton Zip Coder ' 01060 rl - Date/Period-of Generation:. 5 / 2 7 / 9 9 to _ Additional Release Tracking Numbers Associated with this Bill of Lading: Note: if this Bill of Lading Is the result of a Limited RemovafAction (LRA) taken prior to-Madflcation, a Release Tracking . Number is not needed . I B. PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH BILL OF LADING: Name of Organization: City of Northcim:oton J Name of Contact: Via= n e F P i ci r--n Title: I Street. r-i i-~ Ha 11 , 21 n' Ma inStreet _ 1 City/Town: Northampton State: MA 'Zip Code: 01060 l Telephone: 413 -5 8 7 - 1 2 6 5 Ext. C. RELATIONSHIP TO RELEASE OR THREAT OF RELEASE OF PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH BILL OF,LADING:. (check one/specify) I ❑ RP ,Specify (circle one): Owner Operator ...Generator. ..Transporter Other. RP:. 1 ® PRP Specify (circle one): Owner Operator, • Generator Transporter. Other PRP: J Fiduciary/Secured Lender ❑ Agency/Public Utility on a Right of Way J ❑ Other Person: ; fJ If an owner and/or operator is not conducting the response action associated with the Bill of Lading, provide on an attachment the name, contact person. address and telephone number, including any area-code and extension, for each,"If known. ' D-TRANSPORTER/COMMON CARRIER INFORMATION: . 1 rs~, C . J Transporter/Common Carrier Name: J. ~ ~ te;`5 S A Contact Person: ~~~t i~ J s of ~`_c' Title: Street City/Town: 1--. i~ State: Zap Code: 0 ,,tiJ Z 0 _ Telephone: Ext. E. RECEIVING FACILITYITEMPORARY STORAGE LOCATION: I . Operator/FacilttyName: City :of Northampton Landfill : Contact Person: Peter McErlail Titie Health Aaent - street: Board of Health ; 210 MIN-.Street. " I City/Town' Northamptoft' MA ° State: 01060 Zip Code: _ Telephone:`/; _545' - % lye .ExL Type of Facifty'. ❑ Asphalt Batoh/Cold Mix. ❑ Landfill/Disposal ❑ incinerator . (check one) ❑ Asphalt Batah/Hot Mix ® Landfill/Daily Cover ❑ Temporary ❑ Thermal Processing ❑ Landfill/Structural Fill ❑ Storage _ Other: Division of Hazardous ' Division of Solid Waste. Waste/Class A Permit Management Permit 96-214-002 EPA Identification Actual/Anticipated Period of Temporary Storage (specify dates if applicable): NA to NA Reason for Temporary Storage (if applicable): Massachusetts Department of.iEnvironrnenta9 Protection BWSC-012A Bureau of Waste Site Cleanup Reim. rl ~ i _ LRA l , 9 BILL OF LADING'(pursuant to 310 CZAR 40.0030) H. CERTIFICATION OF PERSON CONDUCTING RESPONSE ACTION ASSOCIATED WITH THIS BILL OF LADING: I certify under penalties of law that I have personally examined and am familiar with the information contained in this submittal, Including-any and I all documents accompanying this certification, and that, based on my inquiry of those Individuals immediately responsible -for obtaining the information, the material information dontained herein is, to the best of my knowledge and belief, true, accurate and-complete. I am aware that there are significant penalties, Including, but not limited. to, possible. fines. arid. imprisonment, for wilfully submitting false, inaccurate, or incomplete information. r F Signature: ?r'~ y'r~'A.-~* Gate: ~ I l I Name of Person (print):~~`iG * As Agent for the City of Northampton evts Tins form is printed on racy-cled paper. 1-age ;s or i Massachusetts Department of Environm M ental Protection BWSC-012B Bureau of Waste Site Cleanup . . Rele"e Tr=Wnq Nunjbw H O DILL OF LADING (pursuant to 310 CMR 40.0030) LRA LOG SHEET OF 1. LOAD INFORMATION: LOAD 1: Signature of Transporter Representative: Receivin Facillty/Temporary Storage Representative: g Date of Shipment: Time of'Shipment: Date of Receipt:. Time of Receipt: (circle one) am/pm : s . i /4- Truckfrractor Registration: Trailer Registration (if any): . " (circle one) am/pm .i_ i - ; Load Size (cu. yds./tons): LOAD 2: Signature of Transporter Representative: Receiving Facility/Temporary Storage Representative: Date of Shipment: Time of Shipment: t i Date of Receipt: Time of Receipt: (circle one) am/pm Truck/Tractor Registration : Trailer Registration Cif any): i (circle one) am/pm Load Size (cu. ydsJtons): LOAD 3: Signature of Transporter Representative: Receiving Facility/Temporary Storage Representative: i Date of Shipment: Time of Shipment: i Date of Receipt: Time of Receipt: (circle one) am/pm It Truck/Tractor Registration: Trailer Registration (if any): (circle one) am/pm Load Size (cu. ydsJtons): LOAD 4: Signature of Transporter Representative: i Receiving Facility/Temporary Storage Representative: Date of Shipment: Time of Shipment: • ` i i Date of Receipt: Time of Receipt: (circle one) am/pm Truck/Tractor Registration: Trailer Registration (if any): (circle one) am/pm t Load Size (cu. ydsJtons): LOAD 5: Signature of Transporter Representative:, i Receiving Facifity/Temporary Storage Representative: Date of Shipment: Time.of Shipment: i Date of Receipt: Time of Receipt: . (circle one) am/pm 1 i Truck/Tractor Registration:.- Trailer Registration (if.any): I . (circle one) am/pm 'Load Size (cu. ydsJfons-j: LOAD 6: Signature of Transporter Representative: Receiving Facllity/Temporary Storage Representative: Date of Shipment: Time of Shipment i i Date of Receipt: Mme of Receipt: _ (circle one) am/pm:' TruckR ractor Registration: Trailer Registration, (if any):. (circle one) am/pm Load Size (cu. ydsJtons): LOAD 7: Signature of Transporter Representative: Receiving Facility/Temporary Storage Representative: Date of Shipment: Time of Shipment - i Date of Receipt: Time of Receipt: (circle one) aMpm` 1 _ / -T-ruck/Tractor Registration: Trailer Registration (f any): (circle one) am/pm r j Load Size (cu. ydsJtons): J J. LOG SHEET VOLUME INFORMATION: Total Volume This Page (cu.ydsAons): l Y Total Carried Forward (cu.ydsAons): Total Carried Forward and This Page(cu.yds.ttons): lrS evise 10/1/94 1 tits r is nn paper. Page 1 of 1 Massachusetts Department of Environmental Protection BWSC-012C Bureau of Waste Site Cleanup BILL OF LADING (pursuant 10 310 CMR 40.0030) a TiadHnp tdumber SUMMARY SHEET OF -LRA. K -''SUMMARY'OF SH IPMENTS:. DATE OF SHIPMENT: DATE OF RECEIPT: NUMBER OF LOADS SHIPPED: DAILY VOLUME SHIPPED (CU, YDS,/TONS): - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - SUMMARY SHEET TOTAL SHIPPED: BILL OF LADING TOTALSHIPPED (only if different): R ' ed° 10/1194 - eves u ~m s pn _ - n paper. rage 1 01 z n i G 0 ON co 't CO :t OD t"l (0 co N y-; ++t 3j &3 Q 0) 63 0 y 0 O S- 4-3 O ~ ffj L (TJ Q) $ - Q) r, a) Q) 03 (D F- Z 0 U F= E 7 0 O Q z z \0 4j I CSC ~ 7 Z - Q (f) O 0- z 0- :f Q Q Z ? ~ W LIJ W <z (D I if i l 0 0 U U U U D co _ N rs 0 0 0 0 lam. ~ UUUUC> .x Di p #LI 114 <1 UOfL00 cL Q) _j fs€ 1- tr TEf)?D1- Q) E L D? C n o U .C~ z 0 0 WASTE MANAGEMENT [ `310N MICHIGAN DEPARTMEN-f OF ENVIRONMENTAL QUALITY F1 Please print or type. _ cyuucu uuue, euuwrny u1 tart i anu art 121 of Act 451, 1994, as amended. Failure to file may subject you to DO NO-OWRITE IN THIS t.OE criminal and/or civil penalties under 'ATT. ❑ DIS. El REJ. El PR. El Sections 324.11151 or 324.12116 MCL. Form Approved.- OMB No. 2050-0039 UNIFORM HAZARDOUS 1 G n~e atrgr's U EXA ID No. Manifest D ~ t 1 ~ 2. Page 1 Information in the shaded areas WASTE MANIFEST f t Ei wit No. st i ~J of isawnot. required by Federal 3. Generator's Name and Mailing Addr ss - CITY OF NORTRAHPi N ~„~~y A .State ManlfestDocur 'hent Number . NORT'HAXPTOB 210 MAIN ST MA 01060 ~ ' , :,B'.1 State Generator's ID'-.- .ATWOO?2 DR~ 4. Generator's Phone ( 413 1 587--1265 INORTHA 'SON hA 5. Transporter 1 Company Name 6. US EPA ID Number 1 AD 985 294 693 OIL RECOVERY CORP E.; State ,Transporter s !D . , . D.;Transporters Flione4i3 737-2949 7. Transporter 2 Company Name 8. US EPA ID Number 'E_State Transporters ID F. Jrarisporter!s' Phone 9. Designated Facility Name and Site Address 10. US EPA ID Number G. State Facility's ID CHFA-MT SERVICES INC. 18550 ALLEN B RO _ . ~ . HC I aclli 's Phone"" SRGvt STC , 48192 KID 096 563 194 ' 734-2~2-925 3 11. US DOT Description (including Proper Shipping Name, Hazard Class, and 12. Containers 13. Total 14. Unit i. Waste No J ID NUMBER). HM No. T e Quanti Wt(Vol . sLL a. R.Q,RAZA OUS WASTE SOLID, N.,O. S. s (I)€ 0,5 ,LEAD) s 9 s 39A3077 PC Ili 00 0iio 1171% I1003 E b. a N E _ A T C R ~ d. y J.' Additwnal scriptlons for{Wterials Li'st_d Above` fL Handling Codes a - c d` 15. Special Handling Instructions and Additional Information t ERG #171 24 HR. FEO11E:517--523--7740 SEND COPY OF qIF. WWI V' 16. GENERATOR'S CERTIFICATION: Thereby declare that the contents of this consignment are fully and accurately described above by propel'shipping name and are classified, packed, marked, and labeled, and are in all respects in proper condition for transport by, Ighway according to applicable international and national government regulations. If I am a large quantity generator, I certify that I have a program in place to reduce the volume and toxicity of waste generated to the degree l .have determined to be economically practicable and that I have selected the practicable method of treatment,' storage, or disposal currently available to me which minimizes the present and'future threat to humah health and the environment;, OR; if I am a small-quantity generator, I have made a good faith effort to minimize my waste generation and select the best waste management method that is available to me and that I .can afford. F Date Printed/Typed Name Signature Month Day Year / r. / T 17. Transporter 1 Acknbwle ement of Receipt of Mat ' Is v r. Date q' Prihted/Typ ! , f r'1 V !J Signa "tiT°%/ 1 IN > S P 18. Transporter 2 Acknowledgement of Receipt of Materials - Date T Printed/Typed Name Signature Month Day Year E R 19. Discrepancy Indication Space F A C L 20. Facility Owner or Operator: Certification of receipt of hazardous materials covered by this manifest except as noted in I Item 19. Date' y Pripted(ryped Name i Signature Month Day Year rq 010 s UQ ~O ~a 00 ¢ I.- ~ 0 w 0 = X09 wQ ~ m w m N F ~ ~ O mom ~r aLu N fw- ~~Q U U J } CHEM-MET SEkVICES 046142 ME= 18550 ALLEN ROAD Phone -925 .734-282 0 BROWNSTOWN, M1 48192 EPA # MID096963194 CERTIFICATE OF DISPOSAL This certifies that the waste(s) specified on MANIFEST NUMBER : M17404681 FOR GENERATOR: MA RC10001051 c AND TRANSPORTER: MAD985294693 NORTHHAMPTION, CITY OF OIL RECOVERY CORPORATION 201 MAIN ST. ATWOOD DR. NORTHHAMPTON, MA 010FIO has been properly disposed of under the authority of all required and applicable permits and licenses, to my best knowledge and belief based on my inquiry of individuals immediately responsible for the waste disposal. The waste identified above has been handled -in compliance with one or more of the applicable performance standards specified in 40 CFR, part 268, subpart D and all applicable prohibitions set forth in 40 CFR 268.32 or RCRA section 3004 (d).